DE69511028T2 - Kryogenes Rektifikationssystem mit Seitenkolonne zur Herstellung von niedrigreinem Sauerstoff - Google Patents

Kryogenes Rektifikationssystem mit Seitenkolonne zur Herstellung von niedrigreinem Sauerstoff

Info

Publication number
DE69511028T2
DE69511028T2 DE69511028T DE69511028T DE69511028T2 DE 69511028 T2 DE69511028 T2 DE 69511028T2 DE 69511028 T DE69511028 T DE 69511028T DE 69511028 T DE69511028 T DE 69511028T DE 69511028 T2 DE69511028 T2 DE 69511028T2
Authority
DE
Germany
Prior art keywords
production
low
side column
purity oxygen
rectification system
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Revoked
Application number
DE69511028T
Other languages
English (en)
Other versions
DE69511028D1 (de
Inventor
Harry Cheung
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Praxair Technology Inc
Original Assignee
Praxair Technology Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=23236076&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69511028(T2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Praxair Technology Inc filed Critical Praxair Technology Inc
Application granted granted Critical
Publication of DE69511028D1 publication Critical patent/DE69511028D1/de
Publication of DE69511028T2 publication Critical patent/DE69511028T2/de
Anticipated expiration legal-status Critical
Revoked legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04151Purification and (pre-)cooling of the feed air; recuperative heat-exchange with product streams
    • F25J3/04187Cooling of the purified feed air by recuperative heat-exchange; Heat-exchange with product streams
    • F25J3/04193Division of the main heat exchange line in consecutive sections having different functions
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04078Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression
    • F25J3/0409Providing pressurised feed air or process streams within or from the air fractionation unit providing pressurized products by liquid compression and vaporisation with cold recovery, i.e. so-called internal compression of oxygen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/0429Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of feed air, e.g. used as waste or product air or expanded into an auxiliary column
    • F25J3/04303Lachmann expansion, i.e. expanded into oxygen producing or low pressure column
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04418Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system with thermally overlapping high and low pressure columns
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00Processes or apparatus using separation by rectification
    • F25J2200/34Processes or apparatus using separation by rectification using a side column fed by a stream from the low pressure column
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00Processes or apparatus using separation by rectification
    • F25J2200/50Processes or apparatus using separation by rectification using multiple (re-)boiler-condensers at different heights of the column
    • F25J2200/54Processes or apparatus using separation by rectification using multiple (re-)boiler-condensers at different heights of the column in the low pressure column of a double pressure main column system
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2215/00Processes characterised by the type or other details of the product stream
    • F25J2215/50Oxygen or special cases, e.g. isotope-mixtures or low purity O2
    • F25J2215/52Oxygen production with multiple purity O2
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00Details related to the use of reboiler-condensers
    • F25J2250/02Bath type boiler-condenser using thermo-siphon effect, e.g. with natural or forced circulation or pool boiling, i.e. core-in-kettle heat exchanger
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00Details related to the use of reboiler-condensers
    • F25J2250/04Down-flowing type boiler-condenser, i.e. with evaporation of a falling liquid film

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Separation By Low-Temperature Treatments (AREA)
DE69511028T 1994-10-04 1995-10-03 Kryogenes Rektifikationssystem mit Seitenkolonne zur Herstellung von niedrigreinem Sauerstoff Revoked DE69511028T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/317,973 US5463871A (en) 1994-10-04 1994-10-04 Side column cryogenic rectification system for producing lower purity oxygen

Publications (2)

Publication Number Publication Date
DE69511028D1 DE69511028D1 (de) 1999-09-02
DE69511028T2 true DE69511028T2 (de) 2000-01-27

Family

ID=23236076

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69511028T Revoked DE69511028T2 (de) 1994-10-04 1995-10-03 Kryogenes Rektifikationssystem mit Seitenkolonne zur Herstellung von niedrigreinem Sauerstoff

Country Status (9)

Country Link
US (1) US5463871A (de)
EP (1) EP0706020B1 (de)
JP (1) JP3182326B2 (de)
KR (1) KR100261915B1 (de)
CN (1) CN1103041C (de)
BR (1) BR9504263A (de)
CA (1) CA2159751C (de)
DE (1) DE69511028T2 (de)
ES (1) ES2134391T3 (de)

Families Citing this family (38)

* Cited by examiner, † Cited by third party
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US5628207A (en) * 1996-04-05 1997-05-13 Praxair Technology, Inc. Cryogenic Rectification system for producing lower purity gaseous oxygen and high purity oxygen
US5596886A (en) * 1996-04-05 1997-01-28 Praxair Technology, Inc. Cryogenic rectification system for producing gaseous oxygen and high purity nitrogen
US5669236A (en) * 1996-08-05 1997-09-23 Praxair Technology, Inc. Cryogenic rectification system for producing low purity oxygen and high purity oxygen
US5697229A (en) * 1996-08-07 1997-12-16 Air Products And Chemicals, Inc. Process to produce nitrogen using a double column plus an auxiliary low pressure separation zone
US5675977A (en) * 1996-11-07 1997-10-14 Praxair Technology, Inc. Cryogenic rectification system with kettle liquid column
US5682766A (en) * 1996-12-12 1997-11-04 Praxair Technology, Inc. Cryogenic rectification system for producing lower purity oxygen and higher purity oxygen
US5836174A (en) * 1997-05-30 1998-11-17 Praxair Technology, Inc. Cryogenic rectification system for producing multi-purity oxygen
US5873264A (en) * 1997-09-18 1999-02-23 Praxair Technology, Inc. Cryogenic rectification system with intermediate third column reboil
US5881570A (en) * 1998-04-06 1999-03-16 Praxair Technology, Inc. Cryogenic rectification apparatus for producing high purity oxygen or low purity oxygen
US5934104A (en) * 1998-06-02 1999-08-10 Air Products And Chemicals, Inc. Multiple column nitrogen generators with oxygen coproduction
US5916262A (en) * 1998-09-08 1999-06-29 Praxair Technology, Inc. Cryogenic rectification system for producing low purity oxygen and high purity oxygen
FR2787559A1 (fr) * 1998-12-22 2000-06-23 Air Liquide Procede et installation de separation d'air par distillation cryogenique
FR2787561A1 (fr) * 1998-12-22 2000-06-23 Air Liquide Procede de separation d'air par distillation cryogenique
US6134915A (en) * 1999-03-30 2000-10-24 The Boc Group, Inc. Distillation column arrangement for air separation plant
US6295836B1 (en) 2000-04-14 2001-10-02 Praxair Technology, Inc. Cryogenic air separation system with integrated mass and heat transfer
US6237366B1 (en) 2000-04-14 2001-05-29 Praxair Technology, Inc. Cryogenic air separation system using an integrated core
US6279344B1 (en) 2000-06-01 2001-08-28 Praxair Technology, Inc. Cryogenic air separation system for producing oxygen
US6536234B1 (en) 2002-02-05 2003-03-25 Praxair Technology, Inc. Three column cryogenic air separation system with dual pressure air feeds
US20040020239A1 (en) * 2002-03-08 2004-02-05 Laforce Craig Steven Method of producing an oxygen-enriched air stream
JP2005522629A (ja) * 2002-04-11 2005-07-28 エイ. ハーゼ,リチャード 水燃焼技術−水素と酸素を燃焼させる方法、プロセス、システム及び装置
US6626008B1 (en) 2002-12-11 2003-09-30 Praxair Technology, Inc. Cold compression cryogenic rectification system for producing low purity oxygen
US6622520B1 (en) 2002-12-11 2003-09-23 Praxair Technology, Inc. Cryogenic rectification system for producing low purity oxygen using shelf vapor turboexpansion
US8268269B2 (en) 2006-01-24 2012-09-18 Clearvalue Technologies, Inc. Manufacture of water chemistries
US8429933B2 (en) 2007-11-14 2013-04-30 Praxair Technology, Inc. Method for varying liquid production in an air separation plant with use of a variable speed turboexpander
US20090139263A1 (en) * 2007-12-04 2009-06-04 Air Products And Chemicals, Inc. Thermosyphon reboiler for the denitrogenation of liquid natural gas
FR2930331B1 (fr) * 2008-04-22 2013-09-13 Air Liquide Procede et appareil de separation d'air par distillation cryogenique
JP5032407B2 (ja) * 2008-07-24 2012-09-26 大陽日酸株式会社 窒素製造方法及び装置
FR2946735B1 (fr) * 2009-06-12 2012-07-13 Air Liquide Appareil et procede de separation d'air par distillation cryogenique.
CN102003867A (zh) * 2010-11-09 2011-04-06 上海启元科技发展有限公司 一种生产高纯氮和低纯氧的方法
US8899075B2 (en) * 2010-11-18 2014-12-02 Praxair Technology, Inc. Air separation method and apparatus
US20120125044A1 (en) * 2010-11-19 2012-05-24 Neil Mark Prosser Feed compression method and apparatus for air separation process
CN102080921B (zh) * 2010-12-23 2013-09-04 上海启元科技发展有限公司 一种高压氮和低压氧的生产方法及装置
CN102052821A (zh) * 2011-01-07 2011-05-11 苏州市兴鲁空分设备科技发展有限公司 一种空气分离方法
CN102538397A (zh) * 2012-01-18 2012-07-04 开封黄河空分集团有限公司 一种由空气分离制取氮气或制取氮气同时附产氧气的工艺
CN102721263A (zh) * 2012-07-12 2012-10-10 杭州杭氧股份有限公司 一种利用深冷技术分离空气的系统及方法
CN103438663A (zh) * 2013-07-11 2013-12-11 开封黄河空分集团有限公司 超低压制取高纯氧气和氮气装置及工艺
CN103453314A (zh) * 2013-08-15 2013-12-18 湖北和远气体股份有限公司 一种废液处理过程中加入富氧的方法
CN109737691B (zh) * 2019-01-31 2020-05-19 东北大学 一种钢铁企业空气分离系统

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Also Published As

Publication number Publication date
KR100261915B1 (ko) 2000-07-15
KR960013411A (ko) 1996-05-22
JP3182326B2 (ja) 2001-07-03
ES2134391T3 (es) 1999-10-01
CN1103041C (zh) 2003-03-12
CA2159751A1 (en) 1996-04-05
CN1126305A (zh) 1996-07-10
EP0706020A3 (de) 1996-07-03
US5463871A (en) 1995-11-07
CA2159751C (en) 1997-11-25
DE69511028D1 (de) 1999-09-02
JPH08210769A (ja) 1996-08-20
EP0706020B1 (de) 1999-07-28
BR9504263A (pt) 1998-10-27
EP0706020A2 (de) 1996-04-10

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