DE69130101D1 - Verfahren zur Fraktionierung einer Reaktionsmischung, die methylenverbrückte Polyphenylenpolyisocyanate enthält - Google Patents
Verfahren zur Fraktionierung einer Reaktionsmischung, die methylenverbrückte Polyphenylenpolyisocyanate enthältInfo
- Publication number
- DE69130101D1 DE69130101D1 DE69130101T DE69130101T DE69130101D1 DE 69130101 D1 DE69130101 D1 DE 69130101D1 DE 69130101 T DE69130101 T DE 69130101T DE 69130101 T DE69130101 T DE 69130101T DE 69130101 D1 DE69130101 D1 DE 69130101D1
- Authority
- DE
- Germany
- Prior art keywords
- fractionation
- reaction mixture
- mixture containing
- containing methylene
- polyphenylene polyisocyanates
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 229920000265 Polyparaphenylene Polymers 0.000 title 1
- 238000005194 fractionation Methods 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 229920001228 polyisocyanate Polymers 0.000 title 1
- 239000005056 polyisocyanate Substances 0.000 title 1
- -1 polyphenylene Polymers 0.000 title 1
- 239000011541 reaction mixture Substances 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C07C263/20—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyurethanes Or Polyureas (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2283515A JP2875877B2 (ja) | 1990-10-23 | 1990-10-23 | メチレン架橋ポリフェニレンポリイソシアネートの製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69130101D1 true DE69130101D1 (de) | 1998-10-08 |
DE69130101T2 DE69130101T2 (de) | 1999-02-18 |
Family
ID=17666538
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69130101T Expired - Fee Related DE69130101T2 (de) | 1990-10-23 | 1991-10-16 | Verfahren zur Fraktionierung einer Reaktionsmischung, die methylenverbrückte Polyphenylenpolyisocyanate enthält |
Country Status (8)
Country | Link |
---|---|
US (1) | US5179227A (de) |
EP (1) | EP0482490B1 (de) |
JP (1) | JP2875877B2 (de) |
KR (1) | KR950008204B1 (de) |
CN (1) | CN1045003C (de) |
BR (1) | BR9104556A (de) |
DE (1) | DE69130101T2 (de) |
HU (1) | HU208984B (de) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5179222A (en) * | 1991-09-13 | 1993-01-12 | International Flavors & Fragrances Inc. | Process for preparing phenyl butyronitriles and perfumery use of 2,2-dimethyl-4-phenyl valeronitrile |
KR970001071B1 (ko) * | 1992-06-23 | 1997-01-25 | 미쓰이도오아쓰가가꾸 가부시끼가이샤 | 메틸렌 가교 폴리페닐렌 폴리이소시아네이트의 제조방법 |
DE10333929A1 (de) * | 2003-07-25 | 2005-02-24 | Bayer Materialscience Ag | Herstellung von Mischungen von Di- und Polyisocyanaten der Diphenylmethanreihe mit hohen Gehalten an 4,4'-Methylendiphenyldiisocyanat und 2,4'-Methylendiphenyldiisocyanat |
DE102004005319A1 (de) * | 2004-02-04 | 2005-08-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von hochreinem 2,4'-Methylendiphenyldiisocyanat |
BRPI0519528A2 (pt) * | 2004-12-22 | 2009-02-17 | Lanxess Deutschand Gmbh | processo para reduÇço do teor de cloro hodrolisÁvel em isocianatos orgÂnicos ou em misturas de isocianatos orgÂnicos, emprego de isocianatos |
DE102005026864A1 (de) * | 2005-06-10 | 2006-12-14 | Bayer Materialscience Ag | Verfahren zur Herstellung von 4,4'-Diphenylmethandiisocyanat |
DE102005055189A1 (de) * | 2005-11-19 | 2007-05-24 | Bayer Materialscience Ag | Verfahren zur Herstellung von 4,4'-Diphenylmethandiisocyanat |
EP2042485A1 (de) * | 2007-09-28 | 2009-04-01 | Huntsman International Llc | Verfahren zur Fraktionierung einer Mischung von Polyisocyanaten |
JP2010120870A (ja) * | 2008-11-18 | 2010-06-03 | Nippon Polyurethane Ind Co Ltd | メチレン架橋ポリフェニルポリイソシアネートの製造方法 |
CN104326941B (zh) * | 2014-11-05 | 2016-07-13 | 华玉叶 | 一种浓缩粗多异氰酸酯的方法 |
KR102618935B1 (ko) | 2015-01-30 | 2023-12-27 | 바스프 에스이 | 낮은 부산물 함량의 폴리페닐렌 폴리메틸렌 폴리이소시아네이트 |
CN111069203B (zh) * | 2019-12-06 | 2021-07-23 | 万华化学集团股份有限公司 | 一种光气化法异氰酸酯生产装置中酸性固体物的安全清理方法 |
US20240034831A1 (en) * | 2020-09-18 | 2024-02-01 | Keun Sik Kim | Process of preparing isocyanate compounds comprising non-chlorinated derivative and composition thereof |
CN115650880B (zh) * | 2022-11-03 | 2024-08-20 | 万华化学(宁波)有限公司 | 一种过保质期mdi的回收处理方法及由其制备碳化二亚胺改性异氰酸酯的方法和产品 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4014914A (en) * | 1970-01-12 | 1977-03-29 | Badische Anilin- & Soda-Fabrik Aktiengesellschaft | Manufacture of 4,4'-diphenylmethane diisocyanate and a mixture of diisocyanates and polyisocyanates |
GB1398975A (en) * | 1971-08-16 | 1975-06-25 | Ici Ltd | Heat treatment and distillation of methylene bridged polyphenyl polyisocyanates |
GB1384065A (en) * | 1971-11-30 | 1975-02-19 | Ici Ltd | Process for the purification of organic isocyanates |
GB1417087A (en) * | 1973-05-29 | 1975-12-10 | Ici Ltd | Polyisocyanates |
US3925437A (en) * | 1974-07-18 | 1975-12-09 | Jefferson Chem Co Inc | Reduction of acidity of organic polymeric isocyanates |
DE2624285C2 (de) * | 1976-05-31 | 1987-03-12 | Basf Ag, 6700 Ludwigshafen | Verfahren zur kontinuierlichen Herstellung von organischen Isocyanaten |
DE2631168B2 (de) * | 1976-07-10 | 1979-03-08 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Diisocyanatodiphenylmethan-Isomeren mit einem eingestellten Gehalt an Chlorverbindungen |
DE2844591A1 (de) * | 1978-10-13 | 1980-04-24 | Texaco Development Corp | Verfahren zur reinigung und verminderung der aziditaet von polymethylen-polyphenylpolyisocyanat-gemischen |
JPS5826337A (ja) * | 1981-07-16 | 1983-02-16 | Clarion Co Ltd | 保持プランジヤ−機構 |
DE3145010A1 (de) * | 1981-11-12 | 1983-05-19 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von 4,4'-diisocyanatodiphenylmethan |
DD257827A1 (de) * | 1987-02-20 | 1988-06-29 | Schwarzheide Synthesewerk Veb | Verfahren zur gewinnung von isocyanatkomponenten aus verfahrensprodukten der toluylendiisocyanatherstellung |
DE3714439A1 (de) * | 1987-04-30 | 1988-11-10 | Bayer Ag | Verfahren zur herstellung von (cyclo)aliphatischen diisocyanaten |
-
1990
- 1990-10-23 JP JP2283515A patent/JP2875877B2/ja not_active Expired - Fee Related
-
1991
- 1991-10-16 EP EP91117622A patent/EP0482490B1/de not_active Expired - Lifetime
- 1991-10-16 DE DE69130101T patent/DE69130101T2/de not_active Expired - Fee Related
- 1991-10-22 HU HU913325A patent/HU208984B/hu unknown
- 1991-10-22 BR BR919104556A patent/BR9104556A/pt not_active IP Right Cessation
- 1991-10-23 CN CN91108082A patent/CN1045003C/zh not_active Expired - Lifetime
- 1991-10-23 KR KR1019910018688A patent/KR950008204B1/ko not_active IP Right Cessation
- 1991-10-23 US US07/779,733 patent/US5179227A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
BR9104556A (pt) | 1992-06-09 |
HUT60305A (en) | 1992-08-28 |
JPH04159259A (ja) | 1992-06-02 |
CN1060836A (zh) | 1992-05-06 |
CN1045003C (zh) | 1999-09-08 |
US5179227A (en) | 1993-01-12 |
JP2875877B2 (ja) | 1999-03-31 |
EP0482490A2 (de) | 1992-04-29 |
KR920008098A (ko) | 1992-05-27 |
EP0482490B1 (de) | 1998-09-02 |
HU913325D0 (en) | 1992-01-28 |
KR950008204B1 (ko) | 1995-07-26 |
DE69130101T2 (de) | 1999-02-18 |
HU208984B (en) | 1994-02-28 |
EP0482490A3 (en) | 1993-03-31 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8339 | Ceased/non-payment of the annual fee |