DE69130066T2 - Verfahren und vorrichtung zum wiedergewinnen von chemischen verbindungen aus dem ausfluss einer überkritischen flüssigkeitsextraktion - Google Patents

Verfahren und vorrichtung zum wiedergewinnen von chemischen verbindungen aus dem ausfluss einer überkritischen flüssigkeitsextraktion

Info

Publication number
DE69130066T2
DE69130066T2 DE69130066T DE69130066T DE69130066T2 DE 69130066 T2 DE69130066 T2 DE 69130066T2 DE 69130066 T DE69130066 T DE 69130066T DE 69130066 T DE69130066 T DE 69130066T DE 69130066 T2 DE69130066 T2 DE 69130066T2
Authority
DE
Germany
Prior art keywords
chemical compounds
outflow
liquid extraction
supercritical liquid
recovering chemical
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69130066T
Other languages
English (en)
Other versions
DE69130066D1 (de
Inventor
Kevin Durst
Nathan Porter
Ross Riches
Gary Gleave
R Nielsen
Bruce Richter
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dionex Corp
Original Assignee
Dionex Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dionex Corp filed Critical Dionex Corp
Publication of DE69130066D1 publication Critical patent/DE69130066D1/de
Application granted granted Critical
Publication of DE69130066T2 publication Critical patent/DE69130066T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/34Purifying; Cleaning
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0203Solvent extraction of solids with a supercritical fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L5/00Gas handling apparatus
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/04Preparation or injection of sample to be analysed
    • G01N30/06Preparation
    • G01N2030/062Preparation extracting sample from raw material
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N35/00Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
    • G01N35/10Devices for transferring samples or any liquids to, in, or from, the analysis apparatus, e.g. suction devices, injection devices
    • G01N35/1079Devices for transferring samples or any liquids to, in, or from, the analysis apparatus, e.g. suction devices, injection devices with means for piercing stoppers or septums

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Physics & Mathematics (AREA)
  • Biomedical Technology (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Sampling And Sample Adjustment (AREA)
DE69130066T 1990-10-02 1991-09-19 Verfahren und vorrichtung zum wiedergewinnen von chemischen verbindungen aus dem ausfluss einer überkritischen flüssigkeitsextraktion Expired - Fee Related DE69130066T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/591,612 US5271903A (en) 1990-10-02 1990-10-02 Supercritical fluid extraction restrictor and collection system
PCT/US1991/006700 WO1992006058A1 (en) 1990-10-02 1991-09-19 Supercritical fluid extraction restrictor and collection system

Publications (2)

Publication Number Publication Date
DE69130066D1 DE69130066D1 (de) 1998-10-01
DE69130066T2 true DE69130066T2 (de) 1999-04-01

Family

ID=24367158

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69130066T Expired - Fee Related DE69130066T2 (de) 1990-10-02 1991-09-19 Verfahren und vorrichtung zum wiedergewinnen von chemischen verbindungen aus dem ausfluss einer überkritischen flüssigkeitsextraktion

Country Status (8)

Country Link
US (1) US5271903A (de)
EP (1) EP0551352B1 (de)
JP (1) JP3042881B2 (de)
AT (1) ATE170166T1 (de)
AU (1) AU661974B2 (de)
CA (1) CA2093220A1 (de)
DE (1) DE69130066T2 (de)
WO (1) WO1992006058A1 (de)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5269930A (en) * 1990-07-13 1993-12-14 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5690828A (en) * 1990-07-13 1997-11-25 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5614089A (en) * 1990-07-13 1997-03-25 Isco, Inc. Apparatus and method for supercritical fluid extraction or supercritical fluid chromatography
US5268103A (en) * 1990-07-13 1993-12-07 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5635070A (en) * 1990-07-13 1997-06-03 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5653885A (en) * 1990-07-13 1997-08-05 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5250195A (en) 1990-07-13 1993-10-05 Isco, Inc. Apparatus and method for supercritical fluid extraction
US5932095A (en) 1990-07-13 1999-08-03 Isco, Inc. Multi-chambered supercritical fluid extraction cartridge
US5601707A (en) * 1990-07-13 1997-02-11 Isco, Inc. Apparatus and method for supercritical fluid extraction or supercritical fluid chromatography
NO175834C (no) * 1992-09-02 1994-12-14 Norsk Hydro As Utstyr for prövetakning og opparbeiding til analyse av PAH og andre organiske forbindelser, samt hydrogenfluorid og svoveloksider
DE69332946T2 (de) * 1992-10-16 2004-05-19 Suprex Corp. Automatisierte extrakion mittels eines superkritischen fluidum
US5750029A (en) * 1992-10-16 1998-05-12 Suprex Corporation Method and apparatus for determination of analyte concentration
US5472612A (en) * 1993-08-16 1995-12-05 The United States Of America As Represented By The Secretary Of Agriculture Supercritical fluid extraction system and method of operation
GB9413875D0 (en) 1994-07-09 1994-08-31 British Nuclear Fuels Plc Separating solutes from solutions
DE4447116A1 (de) * 1994-12-29 1996-07-04 Sueddeutsche Kalkstickstoff Verfahren zur Fraktionierung bzw. Raffination von lipiden Naturstoffen
US5561066A (en) * 1995-04-20 1996-10-01 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Analysis of supercritical-extracted chelated metal ions from mixed organic-inorganic samples
GB9600461D0 (en) 1996-01-08 1996-03-13 Ugcs University Of Glamorgan C Analytical apparatus
US5945070A (en) * 1996-10-31 1999-08-31 Merck & Co., Inc. Reaction vessel filter for combinatorial chemistry or biological use
US6106783A (en) * 1998-06-30 2000-08-22 Microliter Analytical Supplies, Inc. Microplate assembly and closure
US6632353B2 (en) * 2000-06-26 2003-10-14 Berger Instruments, Inc. Rapid sample collection in supercritical fluid chromatography
US10182884B2 (en) 2012-04-26 2019-01-22 Ormco Corporation Systems and methods for manufacturing orthodontic appliances
WO2014143419A1 (en) * 2013-03-12 2014-09-18 Waters Technologies Corporation Thermally modulated variable restrictor
US20160018367A1 (en) 2013-03-12 2016-01-21 Waters Technologies Corporation Matching thermally modulated variable restrictors to chromatography separation columns
AU2013202778A1 (en) 2013-03-14 2014-10-02 Gen-Probe Incorporated Systems, methods, and apparatuses for performing automated reagent-based assays
JP2019533809A (ja) 2016-10-10 2019-11-21 パーキンエルマー・ヘルス・サイエンシーズ・インコーポレイテッドPerkinelmer Health Sciences, Inc. サンプリングポンプ、及びトラップに充填するためのサンプリングポンプの閉ループ制御
US11015142B1 (en) * 2016-10-20 2021-05-25 Unified Science, LLC Extraction system and methods for preparing a botanical oil

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4479380A (en) * 1982-02-26 1984-10-30 Brigham Young University Open-tubular supercritical fluid chromatography
US5087360A (en) * 1990-04-19 1992-02-11 Electric Power Research Institute, Inc. Field-portable apparatus and method for analytical supercritical fluid extraction of sorbent materials
US4962275A (en) * 1990-02-21 1990-10-09 United States Of America As Represented By The Secretary Of Commerce Method and apparatus for supercritical fluid extraction solution separation

Also Published As

Publication number Publication date
EP0551352A1 (de) 1993-07-21
EP0551352B1 (de) 1998-08-26
JPH06501936A (ja) 1994-03-03
JP3042881B2 (ja) 2000-05-22
DE69130066D1 (de) 1998-10-01
AU8627891A (en) 1992-04-28
EP0551352A4 (en) 1993-11-18
AU661974B2 (en) 1995-08-17
CA2093220A1 (en) 1992-04-03
WO1992006058A1 (en) 1992-04-16
US5271903A (en) 1993-12-21
ATE170166T1 (de) 1998-09-15

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee