DE69026590D1 - Nitrierungsverfahren - Google Patents

Nitrierungsverfahren

Info

Publication number
DE69026590D1
DE69026590D1 DE69026590T DE69026590T DE69026590D1 DE 69026590 D1 DE69026590 D1 DE 69026590D1 DE 69026590 T DE69026590 T DE 69026590T DE 69026590 T DE69026590 T DE 69026590T DE 69026590 D1 DE69026590 D1 DE 69026590D1
Authority
DE
Germany
Prior art keywords
nitriding process
nitriding
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69026590T
Other languages
English (en)
Other versions
DE69026590T2 (de
Inventor
Alfred A Guenkel
John M Rae
Edward G Hauptmann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NRM INTERNATIONAL TECHNOLOGY C.V., AMSTERDAM, NL
Original Assignee
Nrm Int Tech
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nrm Int Tech filed Critical Nrm Int Tech
Publication of DE69026590D1 publication Critical patent/DE69026590D1/de
Application granted granted Critical
Publication of DE69026590T2 publication Critical patent/DE69026590T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00186—Controlling or regulating processes controlling the composition of the reactive mixture

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE1990626590 1990-01-04 1990-12-31 Nitrierungsverfahren Expired - Lifetime DE69026590T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US46114290A 1990-01-04 1990-01-04

Publications (2)

Publication Number Publication Date
DE69026590D1 true DE69026590D1 (de) 1996-05-23
DE69026590T2 DE69026590T2 (de) 1996-10-31

Family

ID=23831389

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1990626590 Expired - Lifetime DE69026590T2 (de) 1990-01-04 1990-12-31 Nitrierungsverfahren

Country Status (3)

Country Link
EP (1) EP0436443B1 (de)
DE (1) DE69026590T2 (de)
ES (1) ES2087139T3 (de)

Families Citing this family (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4309140C2 (de) * 1993-03-22 2001-09-20 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4411064A1 (de) * 1994-03-30 1995-10-05 Bayer Ag Verfahren zur adiabatischen Herstellung von Mononitrohalogenbenzolen
DE4428459A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4428462A1 (de) * 1994-08-11 1996-02-15 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE4437047A1 (de) 1994-10-17 1996-04-18 Bayer Ag Verfahren zur Dinitrierung von aromatischen Verbindungen
DE19521614A1 (de) * 1995-06-14 1996-12-19 Bayer Ag Verfahren zur Herstellung von Dinitrotoluol
DE19539205A1 (de) * 1995-10-22 1997-04-24 Meissner Gmbh & Co Kg Josef Verfahren zur Aromatennitrierung
US6969490B2 (en) * 2003-06-26 2005-11-29 3M Innovative Properties Company Device for the continuous process for the production of controlled architecture materials
CN101679200A (zh) * 2007-06-27 2010-03-24 Hrd有限公司 生产硝基苯的方法和系统
DE102007059513A1 (de) 2007-12-11 2009-06-18 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol durch adiabate Nitrierung
DE102008048713A1 (de) 2008-09-24 2010-03-25 Bayer Materialscience Ag Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
WO2010054462A1 (en) * 2008-11-14 2010-05-20 Noram International Limited Method for reducing the formation of by-product dinitrobenzene in the production of mononitrobenzene
DE102009005324B4 (de) 2009-01-16 2014-04-03 Plinke Gmbh Verfahren zur adiabatischen Nitrierung von Benzol
WO2010145914A1 (en) 2009-06-17 2010-12-23 Huntsman International Llc Chemical installation
DE102010006984A1 (de) 2010-02-05 2011-08-11 Bayer MaterialScience AG, 51373 Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
KR20130041145A (ko) 2010-07-30 2013-04-24 바이엘 인텔렉쳐 프로퍼티 게엠베하 니트로벤젠의 연속 제조 방법
EP2418176A1 (de) 2010-08-12 2012-02-15 Basf Se Verfahren zur Aufreinigung von Abwässern aus der Aufarbeitung vom rohem Mononitrobenzol
KR102029504B1 (ko) 2011-08-09 2019-10-07 바스프 에스이 미정제 방향족 니트로 화합물의 재처리로부터의 폐수 정제 방법
US8697921B2 (en) 2011-08-09 2014-04-15 Basf Se Process for purifying wastewaters from the workup of crude aromatic nitro compounds
WO2013020798A1 (de) 2011-08-09 2013-02-14 Basf Se Verfahren zur aufreinigung von abwässern aus der aufarbeitung von rohen aromatischen nitroverbindungen
DE102011081898A1 (de) 2011-08-31 2013-02-28 Bayer Materialscience Aktiengesellschaft Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
WO2013054181A1 (en) 2011-10-14 2013-04-18 Council Of Scientific & Industrial Research Continuous two step flow synthesis of m-amino acetophenone
KR102066763B1 (ko) 2012-07-27 2020-01-15 코베스트로 도이칠란드 아게 단열 질화에 의한 니트로벤젠의 제조방법
WO2014016289A1 (de) 2012-07-27 2014-01-30 Bayer Materialscience Ag Verfahren zur herstellung von nitrobenzol durch adiabate nitrierung
WO2014016290A1 (de) 2012-07-27 2014-01-30 Bayer Materialscience Ag Verfahren zur herstellung von nitrobenzol durch adiabate nitrierung
US9227909B2 (en) 2012-10-10 2016-01-05 Covestro Deutschland Ag Method for the continuous production of nitrobenzene
PT2986562T (pt) 2013-04-18 2017-04-24 Covestro Deutschland Ag Método para o processamento de água residual a partir da produção de nitro-benzeno
PT2986563T (pt) 2013-04-18 2017-04-06 Covestro Deutschland Ag Processo para tratamento de efluentes da produção de nitrobenzeno
JP6661555B2 (ja) 2014-06-24 2020-03-11 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ ニトロベンゼンの製造方法
JP6640125B2 (ja) 2014-06-24 2020-02-05 コベストロ、ドイチュラント、アクチエンゲゼルシャフトＣｏｖｅｓｔｒｏ Ｄｅｕｔｓｃｈｌａｎｄ Ａｇ 運転の中断を伴う化学製品の製造方法
HUE055741T2 (hu) 2016-08-17 2021-12-28 Covestro Intellectual Property Gmbh & Co Kg Eljárás és berendezés különféle vegyi termékek elõállítására
DE102017110084B4 (de) 2017-02-03 2019-07-04 Josef Meissner Gmbh & Co. Kg Verfahren und Anlage zur adiabatischen Nitrierung von Aromaten
HUE067029T2 (hu) 2017-03-07 2024-09-28 Covestro Deutschland Ag Eljárás nitrobenzol elõállítására
CN112939781B (zh) * 2019-12-11 2022-07-12 万华化学（宁波）有限公司 一种通过苯的硝化制备硝基苯的连续运行的绝热方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE515328A (de) * 1951-11-06 1900-01-01
US3780116A (en) * 1972-06-15 1973-12-18 Zaverchand & Co Method for nitration of aromatic hydrocarbon compounds
US4331819A (en) * 1980-04-24 1982-05-25 E. I. Du Pont De Nemours And Company Water removal in nitration of aromatic hydrocarbons
US4973770A (en) * 1988-12-15 1990-11-27 C-I-L, Inc. Manufacture of organic nitro compounds

Also Published As

Publication number Publication date
EP0436443B1 (de) 1996-04-17
DE69026590T2 (de) 1996-10-31
ES2087139T3 (es) 1996-07-16
EP0436443A3 (en) 1992-01-02
EP0436443A2 (de) 1991-07-10

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Legal Events

Date Code Title Description
8327 Change in the person/name/address of the patent owner

Owner name: NRM INTERNATIONAL TECHNOLOGY C.V., AMSTERDAM, NL

8364 No opposition during term of opposition