DE60315684T2 - Glasfüllmaterial und Verfahren zur Herstellung - Google Patents
Glasfüllmaterial und Verfahren zur Herstellung Download PDFInfo
- Publication number
- DE60315684T2 DE60315684T2 DE60315684T DE60315684T DE60315684T2 DE 60315684 T2 DE60315684 T2 DE 60315684T2 DE 60315684 T DE60315684 T DE 60315684T DE 60315684 T DE60315684 T DE 60315684T DE 60315684 T2 DE60315684 T2 DE 60315684T2
- Authority
- DE
- Germany
- Prior art keywords
- mol
- glass
- dental
- glass filler
- metal oxides
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000011521 glass Substances 0.000 title claims abstract description 88
- 239000000463 material Substances 0.000 title claims abstract description 59
- 238000000034 method Methods 0.000 title claims description 23
- 238000011049 filling Methods 0.000 title claims description 19
- 238000004519 manufacturing process Methods 0.000 title abstract description 8
- 239000000945 filler Substances 0.000 claims abstract description 62
- 239000002245 particle Substances 0.000 claims abstract description 57
- 150000002500 ions Chemical class 0.000 claims abstract description 30
- 239000003513 alkali Substances 0.000 claims abstract description 27
- 229910000272 alkali metal oxide Inorganic materials 0.000 claims abstract description 17
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000011350 dental composite resin Substances 0.000 claims abstract description 10
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052810 boron oxide Inorganic materials 0.000 claims abstract description 4
- WIHZLLGSGQNAGK-UHFFFAOYSA-N hafnium(4+);oxygen(2-) Chemical compound [O-2].[O-2].[Hf+4] WIHZLLGSGQNAGK-UHFFFAOYSA-N 0.000 claims abstract description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 3
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910000449 hafnium oxide Inorganic materials 0.000 claims abstract description 3
- 239000010936 titanium Substances 0.000 claims abstract description 3
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 3
- 239000000843 powder Substances 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 31
- 239000000178 monomer Substances 0.000 claims description 16
- 239000005548 dental material Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 11
- 238000002844 melting Methods 0.000 claims description 11
- 230000008018 melting Effects 0.000 claims description 11
- 239000003999 initiator Substances 0.000 claims description 8
- 238000003801 milling Methods 0.000 claims description 8
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- 239000002798 polar solvent Substances 0.000 claims description 7
- 229910021193 La 2 O 3 Inorganic materials 0.000 claims description 6
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 6
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 6
- 230000002378 acidificating effect Effects 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 230000008569 process Effects 0.000 claims description 6
- 229910018068 Li 2 O Inorganic materials 0.000 claims description 5
- 229910000287 alkaline earth metal oxide Inorganic materials 0.000 claims description 4
- 239000003479 dental cement Substances 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 229910000311 lanthanide oxide Inorganic materials 0.000 claims description 4
- 229910052792 caesium Inorganic materials 0.000 claims description 3
- 239000008187 granular material Substances 0.000 claims description 3
- 229910052701 rubidium Inorganic materials 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 2
- 150000007522 mineralic acids Chemical class 0.000 claims description 2
- 150000007524 organic acids Chemical class 0.000 claims description 2
- 239000004593 Epoxy Substances 0.000 claims 1
- 239000002131 composite material Substances 0.000 abstract description 32
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 abstract description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract description 6
- 239000000377 silicon dioxide Substances 0.000 abstract description 5
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 abstract description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract description 4
- FUJCRWPEOMXPAD-UHFFFAOYSA-N Li2O Inorganic materials [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 abstract description 3
- 229910052593 corundum Inorganic materials 0.000 abstract description 3
- CJNBYAVZURUTKZ-UHFFFAOYSA-N hafnium(IV) oxide Inorganic materials O=[Hf]=O CJNBYAVZURUTKZ-UHFFFAOYSA-N 0.000 abstract description 3
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum oxide Inorganic materials [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 abstract description 3
- KTUFCUMIWABKDW-UHFFFAOYSA-N oxo(oxolanthaniooxy)lanthanum Chemical compound O=[La]O[La]=O KTUFCUMIWABKDW-UHFFFAOYSA-N 0.000 abstract description 3
- HYXGAEYDKFCVMU-UHFFFAOYSA-N scandium(III) oxide Inorganic materials O=[Sc]O[Sc]=O HYXGAEYDKFCVMU-UHFFFAOYSA-N 0.000 abstract description 3
- 229910001845 yogo sapphire Inorganic materials 0.000 abstract description 3
- KOPBYBDAPCDYFK-UHFFFAOYSA-N Cs2O Inorganic materials [O-2].[Cs+].[Cs+] KOPBYBDAPCDYFK-UHFFFAOYSA-N 0.000 abstract description 2
- CETPSERCERDGAM-UHFFFAOYSA-N ceric oxide Chemical compound O=[Ce]=O CETPSERCERDGAM-UHFFFAOYSA-N 0.000 abstract description 2
- 229910000422 cerium(IV) oxide Inorganic materials 0.000 abstract description 2
- AKUNKIJLSDQFLS-UHFFFAOYSA-M dicesium;hydroxide Chemical compound [OH-].[Cs+].[Cs+] AKUNKIJLSDQFLS-UHFFFAOYSA-M 0.000 abstract description 2
- XUCJHNOBJLKZNU-UHFFFAOYSA-M dilithium;hydroxide Chemical compound [Li+].[Li+].[OH-] XUCJHNOBJLKZNU-UHFFFAOYSA-M 0.000 abstract description 2
- NOTVAPJNGZMVSD-UHFFFAOYSA-N potassium monoxide Inorganic materials [K]O[K] NOTVAPJNGZMVSD-UHFFFAOYSA-N 0.000 abstract description 2
- 229910001953 rubidium(I) oxide Inorganic materials 0.000 abstract description 2
- 235000012239 silicon dioxide Nutrition 0.000 abstract 2
- 239000011347 resin Substances 0.000 description 15
- 229920005989 resin Polymers 0.000 description 15
- 229920000642 polymer Polymers 0.000 description 14
- 239000004033 plastic Substances 0.000 description 13
- 229920003023 plastic Polymers 0.000 description 13
- 238000003860 storage Methods 0.000 description 10
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 8
- -1 polysiloxanes Polymers 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 7
- 230000005012 migration Effects 0.000 description 7
- 238000013508 migration Methods 0.000 description 7
- 239000002253 acid Substances 0.000 description 6
- 125000002091 cationic group Chemical group 0.000 description 6
- 238000006116 polymerization reaction Methods 0.000 description 6
- 150000007513 acids Chemical class 0.000 description 5
- 239000010410 layer Substances 0.000 description 5
- 239000006060 molten glass Substances 0.000 description 5
- IATRAKWUXMZMIY-UHFFFAOYSA-N strontium oxide Chemical compound [O-2].[Sr+2] IATRAKWUXMZMIY-UHFFFAOYSA-N 0.000 description 5
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 description 4
- 239000000292 calcium oxide Substances 0.000 description 4
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 4
- 239000003822 epoxy resin Substances 0.000 description 4
- 239000002657 fibrous material Substances 0.000 description 4
- 239000003365 glass fiber Substances 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- 229920000647 polyepoxide Polymers 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Inorganic materials [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 3
- 239000011575 calcium Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 125000005520 diaryliodonium group Chemical group 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 239000000975 dye Substances 0.000 description 3
- 229910052731 fluorine Inorganic materials 0.000 description 3
- 239000011737 fluorine Substances 0.000 description 3
- 230000004907 flux Effects 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 239000000156 glass melt Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 150000004679 hydroxides Chemical class 0.000 description 3
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000010703 silicon Substances 0.000 description 3
- LWNGJAHMBMVCJR-UHFFFAOYSA-N (2,3,4,5,6-pentafluorophenoxy)boronic acid Chemical compound OB(O)OC1=C(F)C(F)=C(F)C(F)=C1F LWNGJAHMBMVCJR-UHFFFAOYSA-N 0.000 description 2
- VNQXSTWCDUXYEZ-UHFFFAOYSA-N 1,7,7-trimethylbicyclo[2.2.1]heptane-2,3-dione Chemical compound C1CC2(C)C(=O)C(=O)C1C2(C)C VNQXSTWCDUXYEZ-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N Formic acid Chemical compound OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 229930006711 bornane-2,3-dione Natural products 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- ZYGHJZDHTFUPRJ-UHFFFAOYSA-N coumarin Chemical compound C1=CC=C2OC(=O)C=CC2=C1 ZYGHJZDHTFUPRJ-UHFFFAOYSA-N 0.000 description 2
- 239000012955 diaryliodonium Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 150000002118 epoxides Chemical class 0.000 description 2
- 235000019253 formic acid Nutrition 0.000 description 2
- 239000003178 glass ionomer cement Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical class I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 2
- 239000011256 inorganic filler Substances 0.000 description 2
- 229910003475 inorganic filler Inorganic materials 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 238000010309 melting process Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000012552 review Methods 0.000 description 2
- 239000000565 sealant Substances 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 229910001948 sodium oxide Inorganic materials 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- QKAIFCSOWIMRJG-UHFFFAOYSA-N (4-methylphenyl)-(4-propan-2-ylphenyl)iodanium Chemical compound C1=CC(C(C)C)=CC=C1[I+]C1=CC=C(C)C=C1 QKAIFCSOWIMRJG-UHFFFAOYSA-N 0.000 description 1
- PAAVDLDRAZEFGW-UHFFFAOYSA-N 2-butoxyethyl 4-(dimethylamino)benzoate Chemical compound CCCCOCCOC(=O)C1=CC=C(N(C)C)C=C1 PAAVDLDRAZEFGW-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 229910004116 SrO 2 Inorganic materials 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 229910000421 cerium(III) oxide Inorganic materials 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- 239000002521 compomer Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000001671 coumarin Nutrition 0.000 description 1
- 229960000956 coumarin Drugs 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- GNBHRKFJIUUOQI-UHFFFAOYSA-N fluorescein Chemical compound O1C(=O)C2=CC=CC=C2C21C1=CC=C(O)C=C1OC1=CC(O)=CC=C21 GNBHRKFJIUUOQI-UHFFFAOYSA-N 0.000 description 1
- 239000006112 glass ceramic composition Substances 0.000 description 1
- QWPPOHNGKGFGJK-UHFFFAOYSA-N hypochlorous acid Chemical compound ClO QWPPOHNGKGFGJK-UHFFFAOYSA-N 0.000 description 1
- 239000007943 implant Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 229910052747 lanthanoid Inorganic materials 0.000 description 1
- 150000002602 lanthanoids Chemical class 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 229910001947 lithium oxide Inorganic materials 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- AHHWIHXENZJRFG-UHFFFAOYSA-N oxetane Chemical compound C1COC1 AHHWIHXENZJRFG-UHFFFAOYSA-N 0.000 description 1
- 150000002921 oxetanes Chemical class 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- 238000002047 photoemission electron microscopy Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 229910001950 potassium oxide Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 239000011342 resin composition Substances 0.000 description 1
- 239000003340 retarding agent Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000005361 soda-lime glass Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- 239000001018 xanthene dye Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C12/00—Powdered glass; Bead compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K6/00—Preparations for dentistry
- A61K6/70—Preparations for dentistry comprising inorganic additives
- A61K6/71—Fillers
- A61K6/76—Fillers comprising silicon-containing compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K6/00—Preparations for dentistry
- A61K6/70—Preparations for dentistry comprising inorganic additives
- A61K6/71—Fillers
- A61K6/77—Glass
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K6/00—Preparations for dentistry
- A61K6/80—Preparations for artificial teeth, for filling teeth or for capping teeth
- A61K6/884—Preparations for artificial teeth, for filling teeth or for capping teeth comprising natural or synthetic resins
- A61K6/891—Compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C03C23/0085—Drying; Dehydroxylation
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Organic Chemistry (AREA)
- Plastic & Reconstructive Surgery (AREA)
- Birds (AREA)
- Dental Preparations (AREA)
- Glass Compositions (AREA)
- Dental Tools And Instruments Or Auxiliary Dental Instruments (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP03029538A EP1547572B1 (en) | 2003-12-22 | 2003-12-22 | Glass filler material and method of production |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE60315684D1 DE60315684D1 (de) | 2007-09-27 |
| DE60315684T2 true DE60315684T2 (de) | 2008-06-05 |
Family
ID=34530683
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE60315684T Expired - Lifetime DE60315684T2 (de) | 2003-12-22 | 2003-12-22 | Glasfüllmaterial und Verfahren zur Herstellung |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20080255265A1 (enExample) |
| EP (1) | EP1547572B1 (enExample) |
| JP (1) | JP2007515450A (enExample) |
| KR (1) | KR20060129288A (enExample) |
| AT (1) | ATE369829T1 (enExample) |
| AU (1) | AU2004305250B2 (enExample) |
| CA (1) | CA2551180A1 (enExample) |
| DE (1) | DE60315684T2 (enExample) |
| WO (1) | WO2005060921A1 (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102009008954A1 (de) * | 2009-02-13 | 2010-10-07 | Schott Ag | Röntgenopakes bariumfreies Glas und dessen Verwendung |
| DE102010007796B3 (de) * | 2010-02-12 | 2011-04-14 | Schott Ag | Röntgenopakes bariumfreies Glas und dessen Verwendung |
| US8268065B2 (en) | 2009-02-13 | 2012-09-18 | Schott Ag | X-ray opaque barium-free glasses and uses thereof |
| US8268739B2 (en) | 2009-02-13 | 2012-09-18 | Schott Ag | X-ray opaque barium-free glasses and uses thereof |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100616677B1 (ko) | 2005-04-11 | 2006-08-28 | 삼성전기주식회사 | 유전체용 글라스 프릿트, 유전체 자기조성물, 적층세라믹커패시터 및 그 제조방법 |
| JP5054321B2 (ja) * | 2006-03-28 | 2012-10-24 | 日揮触媒化成株式会社 | 歯科用充填材、その製造方法および歯科用複合材料 |
| RU2320562C1 (ru) * | 2006-12-12 | 2008-03-27 | Юлия Алексеевна Щепочкина | Стекло |
| DE102007032391B3 (de) * | 2007-07-12 | 2009-01-22 | Belchem Fiber Materials Gmbh | Hochtemperaturbeständige anorganische Faser auf Kieselsäurebasis sowie Verfahren zur Herstellung und Verwendung derselben |
| KR101026853B1 (ko) * | 2008-02-27 | 2011-04-06 | 전북대학교산학협력단 | 붕규산 유리 조성물, 이를 이용한 인공 치아 및 인공 치아제조 방법 |
| KR101228694B1 (ko) * | 2010-12-03 | 2013-02-01 | 삼성전기주식회사 | 소결 조제용 나노 사이즈 글라스 분말 및 그 제조 방법 |
| US9757480B2 (en) | 2011-01-28 | 2017-09-12 | Abk Biomedical Incorporated | Radiopaque embolic particles |
| KR101395862B1 (ko) * | 2011-07-21 | 2014-05-16 | (주) 메덴트솔루션 | 치과용 글래스 조성물 및 글래스 침투 세라믹 수복재 |
| DE102011084501B3 (de) * | 2011-10-14 | 2013-03-21 | Schott Ag | Röntgenopakes bariumfreies Glas und dessen Verwendung |
| RU2606999C2 (ru) * | 2011-10-14 | 2017-01-10 | Ивоклар Вивадент Аг | Литиево-силикатные стеклокерамика и стекло с оксидом одновалентного металла |
| CN102976618B (zh) * | 2012-12-11 | 2015-09-23 | 安泰科技股份有限公司 | 水基玻璃离子水门汀的玻璃粉体及其制备方法 |
| US20150013568A1 (en) * | 2013-07-15 | 2015-01-15 | Sukgyung AT Co., Ltd. | Glass Fillers Having Acid Resistance |
| EP3215473A1 (en) * | 2014-11-05 | 2017-09-13 | Corning Incorporated | Glass articles with non-planar features and alkali-free glass elements |
| WO2016082045A1 (en) * | 2014-11-26 | 2016-06-02 | Abk Biomedical Inc. | Radioembolic particles |
| US11136260B2 (en) | 2016-07-29 | 2021-10-05 | Schott Ag | Radiopaque glass and use thereof |
| US10301212B2 (en) | 2016-07-29 | 2019-05-28 | Schott Ag | Radiopaque glass and uses thereof |
| CN109790061B (zh) * | 2016-11-10 | 2022-06-28 | 日本板硝子株式会社 | 玻璃填料及其制造方法 |
| DE102018102301B4 (de) | 2018-02-01 | 2019-08-14 | Schott Ag | Röntgenopakes Glas und dessen Verwendung |
| DE102018010246B4 (de) | 2018-02-01 | 2024-05-16 | Schott Ag | Röntgenopakes Glas und dessen Verwendung |
| JP7530352B2 (ja) | 2018-09-05 | 2024-08-07 | アイアール サイエンティフィック インコーポレイティド | ガラス組成物 |
| CA3136355A1 (en) * | 2019-05-31 | 2020-12-03 | Abk Biomedical Incorporated | Radiopaque glass material |
| US20230024895A1 (en) * | 2019-09-10 | 2023-01-26 | Nippon Sheet Glass Company, Limited | Glass filler and method for producing the same, and resin-containing composition including glass filler |
| CN111517642B (zh) * | 2020-04-30 | 2022-09-20 | 中国建筑材料科学研究总院有限公司 | 一种耐碱玻璃及其制备方法和应用 |
| CN116322598A (zh) * | 2020-10-06 | 2023-06-23 | 日本电气硝子株式会社 | 管玻璃、医药品一次包装容器及碱硅酸盐玻璃 |
| WO2022115940A1 (en) * | 2020-12-01 | 2022-06-09 | Abk Biomedical Incorporated | Radiopaque glass material |
| JP7622939B2 (ja) * | 2021-01-07 | 2025-01-28 | 株式会社トクヤマデンタル | カチオン重合性硬化性組成物 |
| AU2023234349A1 (en) * | 2022-03-15 | 2024-10-24 | The Penn State Research Foundation | Low-melting glass compositions, articles, and methods of making the same. |
| CN115028986B (zh) * | 2022-06-27 | 2023-06-23 | 重庆泰山电缆有限公司 | 电缆护套材料及制备方法 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2929121A1 (de) * | 1979-07-18 | 1981-02-12 | Espe Pharm Praep | Calciumaluminiumfluorosilikatglas- pulver und seine verwendung |
| NZ204975A (en) * | 1982-08-02 | 1985-10-11 | Johnson & Johnson Dental Prod | Polymerisable dental restorative compositions having improved mechanical properties and hydrolytic stability |
| DE3502594A1 (de) * | 1985-01-26 | 1986-07-31 | Etablissement Dentaire Ivoclar, Schaan | Roentgenopaker dentalwerkstoff |
| DE3609038A1 (de) * | 1986-03-18 | 1987-09-24 | Espe Stiftung | Roentgenopake polymerisierbare dentalmassen |
| US5292354A (en) * | 1986-12-04 | 1994-03-08 | Glaverbel, Societe Anonyme | Method of producing dealkalized sheet glass |
| GB2199318B (en) * | 1986-12-04 | 1990-11-14 | Glaverbel | Dealkalised sheet glass and method of producing same |
| JPH0755882B2 (ja) * | 1987-02-13 | 1995-06-14 | 而至歯科工業株式会社 | 歯科用グラスアイオノマーセメント用ガラス粉末 |
| JPH0651735B2 (ja) * | 1988-07-04 | 1994-07-06 | 徳山曹達株式会社 | 硬化性組成物 |
| US5147904A (en) * | 1989-08-24 | 1992-09-15 | Thera Patent Gmbh & Co. Kg | Open-pored moldings, a process for their production and use thereof |
| GB9012533D0 (en) * | 1990-06-05 | 1990-07-25 | Johnson Matthey Plc | Glass composition |
| DE4443173C2 (de) * | 1994-12-05 | 1997-04-10 | Schott Glaswerke | Bariumfreies Dentalglas mit guter Röntgenabsorption |
| US5747003A (en) * | 1995-03-22 | 1998-05-05 | Ppg Industries, Inc. | Amorphous precipitated silica abrasive |
| FR2744440B1 (fr) * | 1996-02-07 | 1998-03-20 | Saint Gobain Vitrage | Procede de traitement de substrats en verre |
| DE19648283A1 (de) * | 1996-11-21 | 1998-05-28 | Thera Ges Fuer Patente | Polymerisierbare Massen auf der Basis von Epoxiden |
| US6270562B1 (en) * | 1998-06-11 | 2001-08-07 | Jeneric/Pentron, Inc. | Filler material for dental composites |
| US6022819A (en) * | 1998-07-17 | 2000-02-08 | Jeneric/Pentron Incorporated | Dental porcelain compositions |
| US6306926B1 (en) * | 1998-10-07 | 2001-10-23 | 3M Innovative Properties Company | Radiopaque cationically polymerizable compositions comprising a radiopacifying filler, and method for polymerizing same |
| DE19846556A1 (de) * | 1998-10-09 | 2000-04-13 | Degussa | Dentalwerkstoff aufweisend poröse Glaskeramiken, poröse Glaskeramiken, Verfahren und Verwendung |
| DE19849388C2 (de) * | 1998-10-27 | 2001-05-17 | Schott Glas | Bariumfreies röntgenopakes Dentalglas sowie dessen Verwendung |
| DE10001228B4 (de) * | 2000-01-13 | 2007-01-04 | 3M Espe Ag | Polymerisierbare Zubereitungen auf der Basis von siliziumhaltigen Epoxiden |
| DE10100680B4 (de) * | 2001-01-09 | 2005-10-27 | 3M Espe Ag | Kationisch härtbare Dentalmassen |
-
2003
- 2003-12-22 AT AT03029538T patent/ATE369829T1/de active
- 2003-12-22 DE DE60315684T patent/DE60315684T2/de not_active Expired - Lifetime
- 2003-12-22 EP EP03029538A patent/EP1547572B1/en not_active Expired - Lifetime
-
2004
- 2004-12-22 AU AU2004305250A patent/AU2004305250B2/en not_active Ceased
- 2004-12-22 JP JP2006546060A patent/JP2007515450A/ja active Pending
- 2004-12-22 KR KR1020067014796A patent/KR20060129288A/ko not_active Ceased
- 2004-12-22 WO PCT/EP2004/014614 patent/WO2005060921A1/en not_active Ceased
- 2004-12-22 US US10/596,722 patent/US20080255265A1/en not_active Abandoned
- 2004-12-22 CA CA002551180A patent/CA2551180A1/en not_active Abandoned
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102009008954A1 (de) * | 2009-02-13 | 2010-10-07 | Schott Ag | Röntgenopakes bariumfreies Glas und dessen Verwendung |
| DE102009008954B4 (de) * | 2009-02-13 | 2010-12-23 | Schott Ag | Röntgenopakes bariumfreies Glas und dessen Verwendung |
| US8178595B2 (en) | 2009-02-13 | 2012-05-15 | Schott Ag | X-ray opaque barium-free glasses and uses thereof |
| US8268065B2 (en) | 2009-02-13 | 2012-09-18 | Schott Ag | X-ray opaque barium-free glasses and uses thereof |
| US8268739B2 (en) | 2009-02-13 | 2012-09-18 | Schott Ag | X-ray opaque barium-free glasses and uses thereof |
| DE102010007796B3 (de) * | 2010-02-12 | 2011-04-14 | Schott Ag | Röntgenopakes bariumfreies Glas und dessen Verwendung |
| US8168693B2 (en) | 2010-02-12 | 2012-05-01 | Schott Ag | X-ray opaque barium-free glasses and uses thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| ATE369829T1 (de) | 2007-09-15 |
| CA2551180A1 (en) | 2005-07-07 |
| KR20060129288A (ko) | 2006-12-15 |
| WO2005060921A1 (en) | 2005-07-07 |
| EP1547572B1 (en) | 2007-08-15 |
| DE60315684D1 (de) | 2007-09-27 |
| AU2004305250A1 (en) | 2005-07-07 |
| AU2004305250B2 (en) | 2010-02-25 |
| EP1547572A1 (en) | 2005-06-29 |
| US20080255265A1 (en) | 2008-10-16 |
| JP2007515450A (ja) | 2007-06-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE60315684T2 (de) | Glasfüllmaterial und Verfahren zur Herstellung | |
| EP2765977B1 (de) | Lithiumsilikat-glaskeramik und -glas mit einwertigem metalloxid | |
| EP2765979B1 (de) | Lithiumsilikat-glaskeramik und -glas mit fünfwertigem metalloxid | |
| EP2765974B1 (de) | Lithiumsilikat-glaskeramik und -glas mit zweiwertigem metalloxid | |
| EP2868634B1 (de) | Lithiumdisilikat-Apatit-Glaskeramik mit Übergangsmetalloxid | |
| EP2844213B1 (de) | Lithiumdisilikat-apatit-glaskeramik | |
| EP2765976B1 (de) | Lithiumsilikat-glaskeramik und -glas mit vierwertigem metalloxid | |
| EP2765975B1 (de) | Lithiumsilikat-glaskeramik und -glas mit dreiwertigem metalloxid | |
| EP2765978B1 (de) | Lithiumsilikat-glaskeramik und -glas mit sechswertigem metalloxid | |
| JPH02233605A (ja) | 放射線不透過性、フッ化物放出性、可視光線硬化性歯科用複合体並びに該複合体中での特定充填材の使用 | |
| CH700386B1 (de) | Röntgenopakes bariumfreies Glas und dessen Verwendung. | |
| CH702657A2 (de) | Röntgenopakes bariumfreies Glas und dessen Verwendung. | |
| EP0634373A1 (de) | Bariumfreies Dentalglas mit guter Röntgenabsorption | |
| CH705618A2 (de) | Röntgenopakes bariumfreies Glas und dessen Verwendung. | |
| EP0802221A1 (de) | Füllstoff auf Siliciumdioxid-Basis, Verfahren zu seiner Herstellung und seine Verwendung | |
| EP1940341B1 (de) | Dentalglas | |
| EP1357883B1 (de) | Kationisch härtbare dentalmassen | |
| EP1560557B1 (de) | Kompositmaterial und verwendung eines kompositmaterials | |
| EP1905412B1 (de) | Glas für dentale Anwendungen | |
| EP3824913A1 (de) | Glasgefüllte paek-formmassen | |
| WO2023008122A1 (ja) | Ｘ線不透過性ガラス、ガラスフィラー及び樹脂組成物 | |
| SE436245B (sv) | Rontgenstraleabsorberande sammansatt komposition for tandrestaurering samt derfor avsedd partikelformig fyllnadsmedelskomposition |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition |