DE60305070D1 - Mikrowellenbehandlung von granulaten in einem wirbelbett - Google Patents

Mikrowellenbehandlung von granulaten in einem wirbelbett

Info

Publication number
DE60305070D1
DE60305070D1 DE60305070T DE60305070T DE60305070D1 DE 60305070 D1 DE60305070 D1 DE 60305070D1 DE 60305070 T DE60305070 T DE 60305070T DE 60305070 T DE60305070 T DE 60305070T DE 60305070 D1 DE60305070 D1 DE 60305070D1
Authority
DE
Germany
Prior art keywords
fluidized
granules
microwave treatment
bed
bed reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60305070T
Other languages
English (en)
Inventor
Michael Stroeder
Nikola Anastasijevic
Thorsten Gerdes
Monika Willert-Porada
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Outokumpu Oyj
Metso Outotec Oyj
Original Assignee
Outokumpu Oyj
Outokumpu Technology Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outokumpu Oyj, Outokumpu Technology Oyj filed Critical Outokumpu Oyj
Priority to DE60305070T priority Critical patent/DE60305070D1/de
Application granted granted Critical
Publication of DE60305070D1 publication Critical patent/DE60305070D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B6/00—Heating by electric, magnetic or electromagnetic fields
    • H05B6/64—Heating using microwaves
    • H05B6/80—Apparatus for specific applications
    • H05B6/806—Apparatus for specific applications for laboratory use
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1872—Details of the fluidised bed reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B01J8/36—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed through which there is an essentially horizontal flow of particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B01J8/38—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed containing a rotatable device or being subject to rotation or to a circulatory movement, i.e. leaving a vessel and subsequently re-entering it
    • B01J8/384—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed containing a rotatable device or being subject to rotation or to a circulatory movement, i.e. leaving a vessel and subsequently re-entering it being subject to a circulatory movement only
    • B01J8/388—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed containing a rotatable device or being subject to rotation or to a circulatory movement, i.e. leaving a vessel and subsequently re-entering it being subject to a circulatory movement only externally, i.e. the particles leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B01J8/42—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed subjected to electric current or to radiations this sub-group includes the fluidised bed subjected to electric or magnetic fields
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00—Preliminary treatment of ores or scrap
    • C22B1/02—Roasting processes
    • C22B1/10—Roasting processes in fluidised form
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B11/00—Obtaining noble metals
    • C22B11/02—Obtaining noble metals by dry processes
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00—Drying solid materials or objects by processes involving the application of heat
    • F26B3/02—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
    • F26B3/06—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried
    • F26B3/08—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried so as to loosen them, e.g. to form a fluidised bed
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00—Drying solid materials or objects by processes involving the application of heat
    • F26B3/02—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
    • F26B3/06—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried
    • F26B3/08—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried so as to loosen them, e.g. to form a fluidised bed
    • F26B3/084—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried so as to loosen them, e.g. to form a fluidised bed with heat exchange taking place in the fluidised bed, e.g. combined direct and indirect heat exchange
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00—Drying solid materials or objects by processes involving the application of heat
    • F26B3/32—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action
    • F26B3/34—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action by using electrical effects
    • F26B3/343—Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action by using electrical effects in combination with convection
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/00141—Coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00433—Controlling the temperature using electromagnetic heating
    • B01J2208/00442—Microwaves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12—Processes employing electromagnetic waves
    • B01J2219/1203—Incoherent waves
    • B01J2219/1206—Microwaves
    • B01J2219/1287—Features relating to the microwave source
    • B01J2219/129—Arrangements thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00—General methods of reducing to metals
    • C22B5/02—Dry methods smelting of sulfides or formation of mattes
    • C22B5/12—Dry methods smelting of sulfides or formation of mattes by gases
    • C22B5/14—Dry methods smelting of sulfides or formation of mattes by gases fluidised material

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Microbiology (AREA)
  • Combustion & Propulsion (AREA)
  • General Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Health & Medical Sciences (AREA)
  • Biotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Biomedical Technology (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Clinical Laboratory Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Geology (AREA)
  • Electromagnetism (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Drying Of Solid Materials (AREA)
  • Medicinal Preparation (AREA)
  • Glanulating (AREA)
  • Apparatuses For Bulk Treatment Of Fruits And Vegetables And Apparatuses For Preparing Feeds (AREA)
  • Constitution Of High-Frequency Heating (AREA)
  • Crucibles And Fluidized-Bed Furnaces (AREA)
  • Furnace Details (AREA)
DE60305070T 2002-12-23 2003-11-25 Mikrowellenbehandlung von granulaten in einem wirbelbett Expired - Lifetime DE60305070D1 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE60305070T DE60305070D1 (de) 2002-12-23 2003-11-25 Mikrowellenbehandlung von granulaten in einem wirbelbett

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10260743A DE10260743B4 (de) 2002-12-23 2002-12-23 Verfahren und Anlage zum thermischen Behandeln von körnigen Feststoffen in einem Wirbelbett
PCT/EP2003/013209 WO2004056468A1 (en) 2002-12-23 2003-11-25 Treatment of granular solids in a fluidized bed with microwaves
DE60305070T DE60305070D1 (de) 2002-12-23 2003-11-25 Mikrowellenbehandlung von granulaten in einem wirbelbett

Publications (1)

Publication Number Publication Date
DE60305070D1 true DE60305070D1 (de) 2006-06-08

Family

ID=32477942

Family Applications (2)

Application Number Title Priority Date Filing Date
DE10260743A Expired - Fee Related DE10260743B4 (de) 2002-12-23 2002-12-23 Verfahren und Anlage zum thermischen Behandeln von körnigen Feststoffen in einem Wirbelbett
DE60305070T Expired - Lifetime DE60305070D1 (de) 2002-12-23 2003-11-25 Mikrowellenbehandlung von granulaten in einem wirbelbett

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DE10260743A Expired - Fee Related DE10260743B4 (de) 2002-12-23 2002-12-23 Verfahren und Anlage zum thermischen Behandeln von körnigen Feststoffen in einem Wirbelbett

Country Status (14)

Country Link
US (1) US20060237300A1 (de)
EP (1) EP1575702B1 (de)
JP (1) JP2006511775A (de)
CN (1) CN1729047A (de)
AT (1) ATE324940T1 (de)
AU (1) AU2003288160A1 (de)
BR (1) BR0317686A (de)
CA (1) CA2510013A1 (de)
DE (2) DE10260743B4 (de)
EA (1) EA200501037A1 (de)
NO (1) NO20053289L (de)
PE (1) PE20040454A1 (de)
WO (1) WO2004056468A1 (de)
ZA (1) ZA200505909B (de)

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DE10260738A1 (de) 2002-12-23 2004-07-15 Outokumpu Oyj Verfahren und Anlage zur Förderung von feinkörnigen Feststoffen
DE10260739B3 (de) 2002-12-23 2004-09-16 Outokumpu Oy Verfahren und Anlage zur Herstellung von Metalloxid aus Metallverbindungen
DE10260741A1 (de) 2002-12-23 2004-07-08 Outokumpu Oyj Verfahren und Anlage zur Wärmebehandlung von feinkörnigen Feststoffen
DE10260737B4 (de) 2002-12-23 2005-06-30 Outokumpu Oyj Verfahren und Anlage zur Wärmebehandlung von titanhaltigen Feststoffen
DE102004042430A1 (de) * 2004-08-31 2006-03-16 Outokumpu Oyj Wirbelschichtreaktor zum thermischen Behandeln von wirbelfähigen Substanzen in einem mikrowellenbeheizten Wirbelbett
DE102006005382A1 (de) * 2006-02-03 2007-08-16 Glatt Gmbh Messung, Überwachung und Regelung gerichteter Produktbewegungen in Wirbel- oder Strahlschichtanlagen und geeignete Anlagen
CN101842504B (zh) 2007-05-21 2012-11-14 奥贝特铝业有限公司 从铝土矿石中提取铝和铁的工艺
DE202010001027U1 (de) * 2009-01-20 2010-06-02 Ettenberger Gmbh & Co. Kg Vorrichtung zur Erzeugung eines brennbaren Synthesegases
DE102009003441B4 (de) * 2009-02-05 2011-04-07 Native Power Solutions Gmbh Verfahren zum Betrieb einer Einkoppeleinheit eines Mikrowellenreaktors für die Pyrolyse von kohlenstoffhaltigem Material
DE102010022400B4 (de) * 2010-06-01 2013-04-25 Outotec Oyj Verfahren und Anlage zur Absenkung des Rest-Kohlenstoffgehaltes von Asche
JP5901519B2 (ja) 2010-06-30 2016-04-13 マイクロ波化学株式会社 油状物質の製造方法、及び油状物質の製造装置
JP2014508863A (ja) 2011-03-18 2014-04-10 オーバイト アルミナ インコーポレイテッド アルミニウム含有材料から希土類元素を回収する方法
US9410227B2 (en) 2011-05-04 2016-08-09 Orbite Technologies Inc. Processes for recovering rare earth elements from various ores
EP2714594A4 (de) 2011-06-03 2015-05-20 Orbite Aluminae Inc Verfahren zur herstellung von hämatit
KR101838330B1 (ko) 2011-06-29 2018-04-26 마이크로파 화학 주식회사 화학 반응 장치 및 화학 반응 방법
US9382600B2 (en) 2011-09-16 2016-07-05 Orbite Technologies Inc. Processes for preparing alumina and various other products
US11229895B2 (en) 2011-11-11 2022-01-25 Microwave Chemical Co., Ltd. Chemical reaction method using chemical reaction apparatus
JP5109004B1 (ja) * 2011-11-11 2012-12-26 マイクロ波化学株式会社 化学反応装置
JP5114616B1 (ja) * 2011-11-11 2013-01-09 マイクロ波化学株式会社 化学反応装置
WO2013071324A2 (de) * 2011-11-17 2013-05-23 Horst Wustinger Verfahren für das herstellen von porösen körnern aus wasserglas
JP6025868B2 (ja) 2012-01-10 2016-11-16 オーバイト アルミナ インコーポレイテッドＯｒｂｉｔｅ Ａｌｕｍｉｎａｅ Ｉｎｃ． 赤泥を処理するプロセス
WO2013138455A1 (en) * 2012-03-14 2013-09-19 Microwave Materials Technologies, Inc. Enhanced microwave heating systems and methods of using the same
US9271338B2 (en) 2012-03-14 2016-02-23 Microwave Materials Technologies, Inc. Pressurized heating system with enhanced pressure locks
AU2013203808B2 (en) 2012-03-29 2016-07-28 Aem Technologies Inc. Processes for treating fly ashes
RU2597096C2 (ru) 2012-07-12 2016-09-10 Орбит Алюминэ Инк. Способы получения оксида титана и различных других продуктов
BR112015006536A2 (pt) 2012-09-26 2017-08-08 Orbite Aluminae Inc processos para preparar alumina e cloreto de magnésio por lixiviação com hcl de vários materiais.
BR112015011049A2 (pt) 2012-11-14 2017-07-11 Orbite Aluminae Inc métodos para purificação de íons de alumínio
JP6136338B2 (ja) * 2013-02-18 2017-05-31 株式会社Ihi ボイラ装置
CN103884011A (zh) * 2014-04-11 2014-06-25 成都曙光光纤网络有限责任公司 锅炉
JP5702016B1 (ja) 2014-06-24 2015-04-15 マイクロ波化学株式会社 化学反応装置
CN105928323B (zh) * 2016-04-28 2018-10-16 华中农业大学 一种粮食微波流态化联合干燥设备、干燥方法及应用
CA3056407A1 (en) 2017-03-15 2018-09-20 915 Labs, LLC Multi-pass microwave heating system
BR112019019114A2 (pt) 2017-03-15 2020-04-14 915 Labs Llc elementos de controle de energia para aquecimento melhorado por micro-ondas de artigos embalados
SG11201908588QA (en) 2017-04-17 2019-10-30 915 Labs Llc Microwave-assisted sterilization and pasteurization system using synergistic packaging, carrier and launcher configurations
IT201800010563A1 (it) * 2018-11-26 2020-05-26 Levi Dancona Pier Lorenzo Forni fusori potenziati al plasma convogliato nel camino
CN210183589U (zh) * 2019-01-22 2020-03-24 南京先欧仪器制造有限公司 连续式液态物料微波处理设备
CN111530591B (zh) * 2020-05-09 2021-05-25 东北大学 一种重力式双管可控矿石厚度的微波助磨装置及使用方法
CN111693411A (zh) * 2020-07-24 2020-09-22 中国石油化工股份有限公司 一种移动床径向反应器状态检测及故障诊断的方法及装置
DE102020127374A1 (de) 2020-10-16 2022-04-21 Technische Universität Bergakademie Freiberg Verfahren zur Zersetzung eines Metall-Carbonats und/oder Metall-Hydroxids zu deren Metall-Oxid mittels Mikrowellen
CN113606872B (zh) * 2021-08-02 2022-06-21 农业农村部南京农业机械化研究所 一种基于石墨烯远红外加热的流化床干燥机及其干燥方法
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Also Published As

Publication number Publication date
CN1729047A (zh) 2006-02-01
ATE324940T1 (de) 2006-06-15
PE20040454A1 (es) 2004-09-10
US20060237300A1 (en) 2006-10-26
ZA200505909B (en) 2006-11-29
EP1575702A1 (de) 2005-09-21
AU2003288160A1 (en) 2004-07-14
WO2004056468A1 (en) 2004-07-08
BR0317686A (pt) 2005-11-22
EP1575702B1 (de) 2006-05-03
NO20053289L (no) 2005-09-06
DE10260743B4 (de) 2008-05-15
NO20053289D0 (no) 2005-07-05
CA2510013A1 (en) 2004-07-08
JP2006511775A (ja) 2006-04-06
EA200501037A1 (ru) 2006-02-24
DE10260743A1 (de) 2004-07-08

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