DE602005025861D1 - Verfahren zur herstellung von fettsäurealkylestern aus fettsäureabfall- oder -rezyklatmaterial - Google Patents

Verfahren zur herstellung von fettsäurealkylestern aus fettsäureabfall- oder -rezyklatmaterial

Info

Publication number
DE602005025861D1
DE602005025861D1 DE200560025861 DE602005025861T DE602005025861D1 DE 602005025861 D1 DE602005025861 D1 DE 602005025861D1 DE 200560025861 DE200560025861 DE 200560025861 DE 602005025861 T DE602005025861 T DE 602005025861T DE 602005025861 D1 DE602005025861 D1 DE 602005025861D1
Authority
DE
Germany
Prior art keywords
fatty acid
fatty
acidal
cylinders
present method
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
DE200560025861
Other languages
English (en)
Inventor
Douglas F Geier
Ahmad K Hilaly
John G Soper
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Archer Daniels Midland Co
Original Assignee
Archer Daniels Midland Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Archer Daniels Midland Co filed Critical Archer Daniels Midland Co
Publication of DE602005025861D1 publication Critical patent/DE602005025861D1/de
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10LFUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00Liquid carbonaceous fuels
    • C10L1/02Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00Recovery of fats, fatty oils or fatty acids from waste materials
    • C11B13/02Recovery of fats, fatty oils or fatty acids from waste materials from soap stock
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/02Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08Refining
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08Refining
    • C11C1/10Refining by distillation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/74Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Microbiology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
DE200560025861 2004-04-09 2005-04-11 Verfahren zur herstellung von fettsäurealkylestern aus fettsäureabfall- oder -rezyklatmaterial Active DE602005025861D1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US56061904P 2004-04-09 2004-04-09
PCT/US2005/012208 WO2005100519A1 (en) 2004-04-09 2005-04-11 Method of preparing fatty acid alkyl esters from waste or recycled fatty acid stock

Publications (1)

Publication Number Publication Date
DE602005025861D1 true DE602005025861D1 (de) 2011-02-24

Family

ID=34965539

Family Applications (1)

Application Number Title Priority Date Filing Date
DE200560025861 Active DE602005025861D1 (de) 2004-04-09 2005-04-11 Verfahren zur herstellung von fettsäurealkylestern aus fettsäureabfall- oder -rezyklatmaterial

Country Status (10)

Country Link
US (1) US7705170B2 (de)
EP (1) EP1749079B1 (de)
AT (1) ATE495234T1 (de)
AU (1) AU2005233615B2 (de)
BR (1) BRPI0509742A (de)
CA (1) CA2563301C (de)
DE (1) DE602005025861D1 (de)
MX (1) MXPA06011666A (de)
MY (1) MY150129A (de)
WO (1) WO2005100519A1 (de)

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ATE331776T1 (de) 2003-08-06 2006-07-15 Smet Engineering N V De Verfahren und vorrichtung zum vakuumstripping
ES2271776T3 (es) 2004-08-06 2007-04-16 De Smet Engineering N.V. Proceso de recuperacion de aceite.
EP1637201B1 (de) 2004-09-15 2007-08-15 De Smet Engineering N.V. Gaswaschverfahren und -vorrichtung
US7582777B2 (en) 2004-10-15 2009-09-01 Archer-Daniels-Midland Company Long chain (C22-C50) polyunsaturated hydrocarbons, derivatives, synthesis and uses thereof
US7828978B2 (en) * 2006-01-11 2010-11-09 Doug Geier Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel
EP1818088A1 (de) 2006-01-20 2007-08-15 De Smet Engineering N.V. Kristallisatoren für Fraktionierungsverfahren von Ölen und Fetten
AU2007363151B2 (en) * 2006-06-28 2014-12-11 Cibus Europe B.V. Alkylester fatty acid blends and uses therefor
WO2008016330A2 (en) * 2006-08-01 2008-02-07 Sie Hendery @ Hendery Bio formula to substitute diesel fuel
EP1894913A1 (de) * 2006-08-21 2008-03-05 Desmet Ballestra Oleo s.p.a. Herstellung von Fettsäureestern und niederen Alkoholen
EP1892232A1 (de) * 2006-08-21 2008-02-27 Desmet Ballestra Oleo s.p.a. Produktion von Estern aus Fettsäuren und Niedrigalkoholen
EP1905815A1 (de) 2006-09-28 2008-04-02 De Smet Engineering S.A. Vorrichtung und Verfahren zur Phasenabtrennung
CN101641429B (zh) * 2007-03-14 2013-07-17 恩迪科特生物燃料Ⅱ有限责任公司 低甘油低硫生物柴油燃料的生产
US20080228011A1 (en) * 2007-03-14 2008-09-18 Endicott Biofuels Ii, Llc Methods for Producing Triol Ethers by Reactive Distillation
US20090031618A1 (en) * 2007-07-31 2009-02-05 Endicott Biofuels Ii, Llc Vacuum Distillation Process
US8105399B2 (en) 2007-07-31 2012-01-31 Endicott Biofuels Ii, Llc Production of renewable diesel by pyrolysis and esterification
US20090036705A1 (en) * 2007-07-31 2009-02-05 Endicott Biofuels Ii, Llc Production of Alkyl Esters from High Fatty Acid Feedstocks
EP2028258A1 (de) 2007-08-01 2009-02-25 N.V. Desmet Ballestra Engineering S.A. Verfahren für eine Vorrichtung zur Desolventisierung unter vermindertem Druck
US8105398B2 (en) * 2007-08-27 2012-01-31 Endicott Biofuels Ii, Llc Production of ester-based fuels such as biodiesel from renewable starting materials
US8097049B2 (en) * 2008-02-07 2012-01-17 The Dallas Group Of America, Inc. Biodiesel purification by a continuous regenerable adsorbent process
US20090247785A1 (en) * 2008-03-31 2009-10-01 The University Of Connecticut Methods and systems for pretreatment of an oil stream
CN104974030A (zh) 2009-12-30 2015-10-14 巴斯夫制药(卡兰尼什)公司 用于纯化多不饱和脂肪酸的模拟移动床色谱分离方法
GB201111595D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Improved process
GB201111589D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New modified process
GB201111594D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New improved process
GB201111601D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New process
GB201111591D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Further new process
GB201300354D0 (en) 2013-01-09 2013-02-20 Basf Pharma Callanish Ltd Multi-step separation process
US9428711B2 (en) 2013-05-07 2016-08-30 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
US8802880B1 (en) 2013-05-07 2014-08-12 Group Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
EP2801604B1 (de) * 2013-05-07 2017-04-12 Groupe Novasep Chromatographisches Verfahren zur Herstellung von hochreinen, mehrfach ungesättigten Fettsäuren
KR102263760B1 (ko) * 2013-05-07 2021-06-11 그룹 노바셉 고도 정제된 다가 불포화 지방산의 제조를 위한 크로마토그래피 방법
US9328054B1 (en) 2013-09-27 2016-05-03 Travis Danner Method of alcoholisis of fatty acids and fatty acid gyicerides
EP3118186B1 (de) 2013-12-11 2022-02-09 Novasep Process Chromatografische anlage zur herstellung von mehrfach ungesättigten fettsäuren
BR112016015718B1 (pt) 2014-01-07 2021-12-07 Novasep Process Solutions Processo de purificação de aminoácidos aromáticos
US10131862B2 (en) 2015-03-19 2018-11-20 Inventure Renewables Inc. Complete saponification and acidulation of natural oil processing byproducts and treatment of reaction products
US9745541B1 (en) 2016-09-09 2017-08-29 Inventure Renewables, Inc. Methods for making free fatty acids from soaps using thermal hydrolysis followed by acidification
WO2020097256A1 (en) 2018-11-06 2020-05-14 Inventure Renewables, Inc. Methods for making free fatty acids and fatty acid derivatives from mixed lipid feedstocks or soapstocks

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US2812343A (en) * 1953-04-06 1957-11-05 Archer Daniels Midland Co Method of making refined fatty acids from soap stocks
US3010977A (en) * 1959-01-14 1961-11-28 Paul H Eaves Process for the methylation of vegetable oil soapstocks
US4100181A (en) * 1977-05-10 1978-07-11 Scm Corporation Process for obtaining free fatty acids from soap stock
US4454329A (en) * 1980-07-04 1984-06-12 The Nisshin Oil Mills, Ltd. Process for preparation of tocopherol concentrates
JPS6042495A (ja) 1983-08-17 1985-03-06 日清製油株式会社 油脂脱臭留出物のメチルエステル化法
US4678580A (en) * 1986-01-27 1987-07-07 Akzo America Inc. Hydrolysis of fats
EP0454719B1 (de) 1989-01-17 1996-06-05 Davy Process Technology Limited Kontinuierliches Verfahren zur Herstellung von Carbonsäureestern
EP0560121A3 (en) * 1992-03-09 1994-07-27 Vandemoortele Int Nv Method for refining glyceride oil
US5405992A (en) * 1994-04-28 1995-04-11 Uop Process for concurrent esterification and separation using a simulated moving bed
US5859270A (en) * 1996-03-13 1999-01-12 Cargill, Incorporated Method for preparation of purified monoglycerides; and, products
US6166231A (en) * 1998-12-15 2000-12-26 Martek Biosciences Corporation Two phase extraction of oil from biomass
US6399802B2 (en) * 2000-03-24 2002-06-04 Kru Feed Energy Company Method for soapstock acidulation
US6623604B1 (en) * 2000-06-05 2003-09-23 Cognis Corporation Method of recovering free fatty acids having low ester content and high acid value
US6797753B2 (en) * 2000-06-20 2004-09-28 Battelle Memorial Institute Plasticizers derived from vegetable oils
MY137733A (en) * 2000-11-22 2009-03-31 Kao Corp Process for producing lower alkyl fatty esters
EP1339817B1 (de) * 2000-12-04 2007-06-13 Westfalia Separator AG Verfahren zur herstellung von fettsaüreestern
US6723863B2 (en) * 2001-08-09 2004-04-20 Archer-Daniels-Midland Company Methods for the preparation of propylene glycol fatty acid esters
US6573396B2 (en) * 2001-10-12 2003-06-03 Exxonmobil Chemical Patents Inc. Co-production of dialkyl carbonates and diols with treatment of hydroxy alkyl carbonate
CA2360986A1 (en) * 2001-11-01 2003-05-01 Nicole Cadoret Method for fractionating grease trap waste and uses of fractions therefrom
US6855838B2 (en) * 2002-01-09 2005-02-15 The United States Of America, As Represented By The Secretary Of Agriculture Lipid rich compositions, production of lipid rich compositions, production of fatty acid alkyl esters from heterogeneous lipid mixtures
EA007328B1 (ru) * 2002-03-28 2006-08-25 Апплайд Резеч Системз Арс Холдинг Н. В. Тиазолидинкарбоксамидные производные как модуляторы рецептора простагландина f
AT504727A1 (de) * 2002-04-12 2008-07-15 Energea Umwelttechnologie Gmbh Verfahren und anlage zur veresterung von fettsäuren
US6768015B1 (en) * 2003-05-16 2004-07-27 Stepan Company Method of making alkyl esters using pressure
US7126018B2 (en) * 2004-01-16 2006-10-24 Archer-Daniels-Midland Company Methods for the preparation of polyol esters that are light in color
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Also Published As

Publication number Publication date
MY150129A (en) 2013-11-29
ATE495234T1 (de) 2011-01-15
CA2563301A1 (en) 2005-10-27
MXPA06011666A (es) 2007-01-23
EP1749079A1 (de) 2007-02-07
BRPI0509742A (pt) 2007-09-25
CA2563301C (en) 2013-04-02
EP1749079B1 (de) 2011-01-12
US20050245405A1 (en) 2005-11-03
WO2005100519A1 (en) 2005-10-27
US7705170B2 (en) 2010-04-27
AU2005233615B2 (en) 2010-04-22
AU2005233615A1 (en) 2005-10-27

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