BRPI0509742A - método de preparar ésteres de alquila de ácido graxo a partir de matéria-prima de ácido graxo reciclada ou residual - Google Patents

método de preparar ésteres de alquila de ácido graxo a partir de matéria-prima de ácido graxo reciclada ou residual

Info

Publication number
BRPI0509742A
BRPI0509742A BRPI0509742-8A BRPI0509742A BRPI0509742A BR PI0509742 A BRPI0509742 A BR PI0509742A BR PI0509742 A BRPI0509742 A BR PI0509742A BR PI0509742 A BRPI0509742 A BR PI0509742A
Authority
BR
Brazil
Prior art keywords
fatty acid
alkyl esters
recycled
acid alkyl
raw material
Prior art date
Application number
BRPI0509742-8A
Other languages
English (en)
Inventor
Paul D Bloom
Douglas F Geier
Ahmad K Hilaly
Peter Reimers
John G Soper
Original Assignee
Archer Daniels Midland Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Archer Daniels Midland Co filed Critical Archer Daniels Midland Co
Publication of BRPI0509742A publication Critical patent/BRPI0509742A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
    • C11B13/02—Recovery of fats, fatty oils or fatty acids from waste materials from soap stock
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/08—Refining
    • C11C1/10—Refining by distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)

Abstract

MéTODO DE PREPARAR éSTERES DE ALQUILA DE áCIDO GRAXO A PARTIR DE MATéRIA-PRIMA DE áCIDO GRAXO RECICLADA OU RESIDUAL. A presente invenção é direcionada a um método ou preparação de ésteres de alquila de ácido graxo de ácidos graxas contidos em correntes de co-produto ou matéria-prima de ácido graxa reciclada ou residual. O método presente utiliza uma resina acídica para converter a matéria-prima de ácido graxo em ésteres. O método presente cerca o usa de cromatografia de leito móvel simulado reativo, em que acima de cerca de 95 por cento da matéria-prima de ácido graxa são convertidos em ásteres de alquila de ácido graxo. O método presente foi otimizado para separar o produto de éster da corrente de rafinato formada durante o processo cromatográfico, desse modo melhorando o rendimento da esterificação e prevenindo hidrólise ácida do éster.
BRPI0509742-8A 2004-04-09 2005-04-11 método de preparar ésteres de alquila de ácido graxo a partir de matéria-prima de ácido graxo reciclada ou residual BRPI0509742A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US56061904P 2004-04-09 2004-04-09
PCT/US2005/012208 WO2005100519A1 (en) 2004-04-09 2005-04-11 Method of preparing fatty acid alkyl esters from waste or recycled fatty acid stock

Publications (1)

Publication Number Publication Date
BRPI0509742A true BRPI0509742A (pt) 2007-09-25

Family

ID=34965539

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0509742-8A BRPI0509742A (pt) 2004-04-09 2005-04-11 método de preparar ésteres de alquila de ácido graxo a partir de matéria-prima de ácido graxo reciclada ou residual

Country Status (10)

Country Link
US (1) US7705170B2 (pt)
EP (1) EP1749079B1 (pt)
AT (1) ATE495234T1 (pt)
AU (1) AU2005233615B2 (pt)
BR (1) BRPI0509742A (pt)
CA (1) CA2563301C (pt)
DE (1) DE602005025861D1 (pt)
MX (1) MXPA06011666A (pt)
MY (1) MY150129A (pt)
WO (1) WO2005100519A1 (pt)

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DE60306515T2 (de) 2003-08-06 2007-06-21 De Smet Engineering N.V. Verfahren und Vorrichtung zum Vakuumstripping
EP1624047B1 (en) 2004-08-06 2006-10-18 De Smet Engineering N.V. Oil recuperation process
ATE369900T1 (de) 2004-09-15 2007-09-15 Smet Engineering N V De Gaswaschverfahren und -vorrichtung
US7582777B2 (en) * 2004-10-15 2009-09-01 Archer-Daniels-Midland Company Long chain (C22-C50) polyunsaturated hydrocarbons, derivatives, synthesis and uses thereof
US7828978B2 (en) * 2006-01-11 2010-11-09 Doug Geier Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel
EP1818088A1 (en) 2006-01-20 2007-08-15 De Smet Engineering N.V. Crystallisers useful in fractionation processes for oils and fats
WO2008016330A2 (en) * 2006-08-01 2008-02-07 Sie Hendery @ Hendery Bio formula to substitute diesel fuel
EP1894913A1 (en) * 2006-08-21 2008-03-05 Desmet Ballestra Oleo s.p.a. Production of esters of fatty acids and lower alcohols
EP1892232A1 (en) * 2006-08-21 2008-02-27 Desmet Ballestra Oleo s.p.a. Production of esters of fatty acids and lower alcohols
EP1905815A1 (en) 2006-09-28 2008-04-02 De Smet Engineering S.A. Phase transfer apparatus and process
US8123822B2 (en) * 2007-03-14 2012-02-28 Endicott Biofuels Ii, Llc Production of biodiesel fuels which are low in glycerin and sulfur
US20080228011A1 (en) * 2007-03-14 2008-09-18 Endicott Biofuels Ii, Llc Methods for Producing Triol Ethers by Reactive Distillation
WO2009017958A1 (en) 2007-07-31 2009-02-05 Endicott Biofuels Ii, Llc Production of renewable diesel by pyrolysis and esterification
US20090036705A1 (en) * 2007-07-31 2009-02-05 Endicott Biofuels Ii, Llc Production of Alkyl Esters from High Fatty Acid Feedstocks
WO2009018390A1 (en) * 2007-07-31 2009-02-05 Endicott Biofuels Ii, Llc Vacuum distillation process
EP2028258A1 (en) 2007-08-01 2009-02-25 N.V. Desmet Ballestra Engineering S.A. Process for equipment for desolventising under reduced pressure
US8105398B2 (en) * 2007-08-27 2012-01-31 Endicott Biofuels Ii, Llc Production of ester-based fuels such as biodiesel from renewable starting materials
ES2653573T3 (es) * 2007-12-27 2018-02-07 Cibus Europe B.V. Mezclas de éster butílico de ácido graso
US8097049B2 (en) * 2008-02-07 2012-01-17 The Dallas Group Of America, Inc. Biodiesel purification by a continuous regenerable adsorbent process
US20090247785A1 (en) * 2008-03-31 2009-10-01 The University Of Connecticut Methods and systems for pretreatment of an oil stream
PT2519332E (pt) 2009-12-30 2014-05-26 Basf Pharma Callanish Ltd Processo de separação cromatográfica em leito móvel simulado para a purificação de ácidos gordos poli-insaturados
GB201111601D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New process
GB201111595D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Improved process
GB201111594D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New improved process
GB201111591D0 (en) 2011-07-06 2011-08-24 Equateq Ltd Further new process
GB201111589D0 (en) 2011-07-06 2011-08-24 Equateq Ltd New modified process
GB201300354D0 (en) 2013-01-09 2013-02-20 Basf Pharma Callanish Ltd Multi-step separation process
EP2801604B1 (en) * 2013-05-07 2017-04-12 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
CN109679768A (zh) * 2013-05-07 2019-04-26 诺瓦塞普集团 用于生产高度纯化的多不饱和脂肪酸的色谱方法
US8802880B1 (en) 2013-05-07 2014-08-12 Group Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
US9428711B2 (en) 2013-05-07 2016-08-30 Groupe Novasep Chromatographic process for the production of highly purified polyunsaturated fatty acids
US9328054B1 (en) 2013-09-27 2016-05-03 Travis Danner Method of alcoholisis of fatty acids and fatty acid gyicerides
EP2883860B1 (fr) 2013-12-11 2016-08-24 Novasep Process Procédé chromatographique de production d'acides gras polyinsaturés
JP6303017B2 (ja) 2014-01-07 2018-03-28 ノヴァセプ プロセスＮｏｖａｓｅｐ Ｐｒｏｃｅｓｓ 芳香族アミノ酸を精製する方法
US10131862B2 (en) 2015-03-19 2018-11-20 Inventure Renewables Inc. Complete saponification and acidulation of natural oil processing byproducts and treatment of reaction products
US9745541B1 (en) 2016-09-09 2017-08-29 Inventure Renewables, Inc. Methods for making free fatty acids from soaps using thermal hydrolysis followed by acidification
EP3877355A4 (en) 2018-11-06 2022-08-03 Inventure International (Pte) Limited PROCESS FOR PRODUCTION OF FREE FATTY ACIDS AND FATTY ACID DERIVATIVES FROM MIXED LIPID RAW MATERIALS OR SOAP STICKS

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Also Published As

Publication number Publication date
CA2563301A1 (en) 2005-10-27
WO2005100519A1 (en) 2005-10-27
AU2005233615A1 (en) 2005-10-27
DE602005025861D1 (de) 2011-02-24
US7705170B2 (en) 2010-04-27
US20050245405A1 (en) 2005-11-03
MXPA06011666A (es) 2007-01-23
AU2005233615B2 (en) 2010-04-22
EP1749079B1 (en) 2011-01-12
ATE495234T1 (de) 2011-01-15
EP1749079A1 (en) 2007-02-07
MY150129A (en) 2013-11-29
CA2563301C (en) 2013-04-02

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B11B Dismissal acc. art. 36, par 1 of ipl - no reply within 90 days to fullfil the necessary requirements