DE602004028891D1 - Axial-hermetisch abgeschlossene Probenbehälter für die NMR - Google Patents
Axial-hermetisch abgeschlossene Probenbehälter für die NMRInfo
- Publication number
- DE602004028891D1 DE602004028891D1 DE602004028891T DE602004028891T DE602004028891D1 DE 602004028891 D1 DE602004028891 D1 DE 602004028891D1 DE 602004028891 T DE602004028891 T DE 602004028891T DE 602004028891 T DE602004028891 T DE 602004028891T DE 602004028891 D1 DE602004028891 D1 DE 602004028891D1
- Authority
- DE
- Germany
- Prior art keywords
- nmr
- axially
- hermetically sealed
- sample containers
- sealed sample
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01R—MEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
- G01R33/00—Arrangements or instruments for measuring magnetic variables
- G01R33/20—Arrangements or instruments for measuring magnetic variables involving magnetic resonance
- G01R33/28—Details of apparatus provided for in groups G01R33/44 - G01R33/64
- G01R33/30—Sample handling arrangements, e.g. sample cells, spinning mechanisms
- G01R33/307—Sample handling arrangements, e.g. sample cells, spinning mechanisms specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer
Landscapes
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Sampling And Sample Adjustment (AREA)
- Spinning Or Twisting Of Yarns (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/387,762 US6812706B2 (en) | 2003-03-12 | 2003-03-12 | Axially-sealed NMR sample tube assemblies |
Publications (1)
Publication Number | Publication Date |
---|---|
DE602004028891D1 true DE602004028891D1 (de) | 2010-10-14 |
Family
ID=32771617
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE602004028891T Expired - Lifetime DE602004028891D1 (de) | 2003-03-12 | 2004-03-11 | Axial-hermetisch abgeschlossene Probenbehälter für die NMR |
Country Status (4)
Country | Link |
---|---|
US (1) | US6812706B2 (de) |
EP (1) | EP1457787B1 (de) |
JP (1) | JP2004279416A (de) |
DE (1) | DE602004028891D1 (de) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10343405B4 (de) * | 2003-09-19 | 2006-05-04 | Bruker Biospin Ag | NMR-Spektrometer mit Greifvorrichtung zur Handhabung einer Probenhülse mit Außennut |
US7119542B1 (en) * | 2005-04-08 | 2006-10-10 | Varian, Inc. | Azimuthally-orienting NMR samples |
JP4795047B2 (ja) * | 2006-02-15 | 2011-10-19 | 住友ゴム工業株式会社 | ゴム試料引張治具、伸長状態のゴム試料の分子構造・分子運動性分析装置ならびに分析方法 |
US7728593B2 (en) * | 2007-09-14 | 2010-06-01 | Norell, Inc. | NMR sample tube size adapter |
US8054080B2 (en) * | 2007-11-16 | 2011-11-08 | Norell, Inc. | Closure and system for NMR sample containers |
JP5370728B2 (ja) * | 2008-12-16 | 2013-12-18 | 独立行政法人物質・材料研究機構 | Mas試料管 |
US8098069B1 (en) | 2009-04-17 | 2012-01-17 | Bruker Biospin Corporation | Adaptive closure with removable vent for sealing containers and method of use |
JP5544616B2 (ja) * | 2009-10-22 | 2014-07-09 | 独立行政法人物質・材料研究機構 | 密封式mas試料管 |
US8192702B2 (en) * | 2010-02-01 | 2012-06-05 | Norell, Inc. | Sample tubes for use in automated systems and methods of manufacture |
JP5517086B2 (ja) * | 2012-09-21 | 2014-06-11 | 独立行政法人物質・材料研究機構 | 固体nmr用masプローブ装置 |
JP5953633B2 (ja) * | 2012-10-09 | 2016-07-20 | 日本電子株式会社 | Nmr測定用スピナ |
US10281416B2 (en) * | 2014-08-04 | 2019-05-07 | Waters Technologies Corporation | Devices for use in solid-state NMR analysis |
US10126380B2 (en) * | 2015-06-15 | 2018-11-13 | Norell, Inc. | Closure and system for NMR sample containers with a secondary locking seal |
US10550889B2 (en) * | 2016-08-01 | 2020-02-04 | Battelle Memorial Institute | Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy |
CN108226207B (zh) * | 2016-12-14 | 2024-03-29 | 中国科学院兰州化学物理研究所 | 液体核磁自动原位反应分析测试系统 |
CN108827725A (zh) * | 2018-04-13 | 2018-11-16 | 中国科学院昆明植物研究所 | 一种适用于黏性高分子的液体核磁样品制备方法 |
US11137458B2 (en) | 2019-05-29 | 2021-10-05 | Battelle Memorial Institute | High-temperature NMR MAS probe with optimized temperature gradient across sample rotor |
CN112649458B (zh) * | 2019-10-10 | 2022-08-05 | 中国科学院大连化学物理研究所 | 一种用于宽压力范围下原位处理和密封固体核磁测试样品的装置及系统 |
DE102020204379B3 (de) | 2020-04-03 | 2021-05-20 | Bruker Switzerland Ag | Magnetisch kompensierter NMR-Rotor und Verfahren zur Auslegung und Herstellung |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2960649A (en) | 1954-06-18 | 1960-11-15 | Bloch Felix | Line narrowing gyromagnetic apparatus |
US3681683A (en) | 1970-09-14 | 1972-08-01 | Varian Associates | Gyromagnetic resonance spectrometer utilizing an improved sample spinning and ejecting structure |
US4088944A (en) | 1976-10-04 | 1978-05-09 | Varian Associates, Inc. | NMR Spectrometer employing self centering turbine |
US4275350A (en) | 1979-05-29 | 1981-06-23 | Varian Associates, Inc. | Sample spinning mechanism for NMR probes |
US4510450A (en) * | 1982-09-28 | 1985-04-09 | The Medical College Of Wisconsin, Inc. | Apparatus and assay method for the quantitative determination of mineral content in bone |
JPS59178347A (ja) * | 1983-03-30 | 1984-10-09 | Hitachi Ltd | 固体高分解能核磁気共鳴装置用温度可変プロ−ブ |
US4739270A (en) | 1986-06-03 | 1988-04-19 | Varian Associates, Inc. | High speed spinner for NMR spectrometer |
US4827761A (en) * | 1987-06-25 | 1989-05-09 | Shell Oil Company | Sample holder |
DE19509062C2 (de) * | 1994-05-11 | 1997-02-13 | Bruker Analytische Messtechnik | NMR-Probenhalter und Verfahren zum Befüllen des Probenhalters |
DE4442742C1 (de) * | 1994-12-01 | 1996-05-23 | Bruker Analytische Messtechnik | Probenkopf für die Kernresonanz-Spektroskopie |
US6054857A (en) * | 1997-03-18 | 2000-04-25 | Doty Scientific, Inc. | NMR MAS sealing sample cells and methods |
US6362624B1 (en) * | 1997-11-12 | 2002-03-26 | The Research Foundation Of State University Of New York | Apparatus and method for high pressure NMR spectroscopy |
DE10111672C2 (de) * | 2001-03-09 | 2003-02-06 | Bruker Biospin Ag Faellanden | Vorrichtung zur genauen Zentrierung eines NMR-Probengläschens |
DE10111674C2 (de) * | 2001-03-09 | 2003-02-06 | Bruker Biospin Ag Faellanden | Vorrichtung zum Transport sowie zur exakten Positionierung eines Probengläschens in einem hochauflösenden NRM-Spektrometer |
-
2003
- 2003-03-12 US US10/387,762 patent/US6812706B2/en not_active Expired - Fee Related
-
2004
- 2004-03-08 JP JP2004064208A patent/JP2004279416A/ja active Pending
- 2004-03-11 DE DE602004028891T patent/DE602004028891D1/de not_active Expired - Lifetime
- 2004-03-11 EP EP04251402A patent/EP1457787B1/de not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP1457787A3 (de) | 2005-04-20 |
US6812706B2 (en) | 2004-11-02 |
EP1457787B1 (de) | 2010-09-01 |
EP1457787A2 (de) | 2004-09-15 |
JP2004279416A (ja) | 2004-10-07 |
US20040178793A1 (en) | 2004-09-16 |
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