DE50004079D1 - Rohrbündelreaktor, insbesondere für katalytische gasphasenreaktionen - Google Patents

Rohrbündelreaktor, insbesondere für katalytische gasphasenreaktionen

Info

Publication number
DE50004079D1
DE50004079D1 DE50004079T DE50004079T DE50004079D1 DE 50004079 D1 DE50004079 D1 DE 50004079D1 DE 50004079 T DE50004079 T DE 50004079T DE 50004079 T DE50004079 T DE 50004079T DE 50004079 D1 DE50004079 D1 DE 50004079D1
Authority
DE
Germany
Prior art keywords
sub
diameter
reactor
catalytic gas
phase reactions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE50004079T
Other languages
English (en)
Inventor
Gerhard Olbert
Franz Corr
Peter Reuter
Ludwig Wambach
Ulrich Hammon
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to DE50004079T priority Critical patent/DE50004079D1/de
Application granted granted Critical
Publication of DE50004079D1 publication Critical patent/DE50004079D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/2425—Tubular reactors in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/37—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups
    • C07C45/38—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups being a primary hydroxyl group
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Catalysts (AREA)
DE50004079T 1999-03-16 2000-03-15 Rohrbündelreaktor, insbesondere für katalytische gasphasenreaktionen Expired - Lifetime DE50004079D1 (de)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE50004079T DE50004079D1 (de) 1999-03-16 2000-03-15 Rohrbündelreaktor, insbesondere für katalytische gasphasenreaktionen

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE19912735 1999-03-16
DE19956329 1999-11-23
DE50004079T DE50004079D1 (de) 1999-03-16 2000-03-15 Rohrbündelreaktor, insbesondere für katalytische gasphasenreaktionen
PCT/EP2000/002304 WO2000054877A2 (de) 1999-03-16 2000-03-15 Rohrbündelreaktor, insbesondere für katalytische gasphasenreaktionen

Publications (1)

Publication Number Publication Date
DE50004079D1 true DE50004079D1 (de) 2003-11-20

Family

ID=26052502

Family Applications (1)

Application Number Title Priority Date Filing Date
DE50004079T Expired - Lifetime DE50004079D1 (de) 1999-03-16 2000-03-15 Rohrbündelreaktor, insbesondere für katalytische gasphasenreaktionen

Country Status (14)

Country Link
US (1) US7226567B1 (de)
EP (1) EP1169119B1 (de)
JP (1) JP5204356B2 (de)
KR (1) KR100648579B1 (de)
CN (1) CN1231291C (de)
AT (1) ATE251944T1 (de)
AU (1) AU4538700A (de)
BR (1) BR0009000B1 (de)
DE (1) DE50004079D1 (de)
ES (1) ES2209870T3 (de)
MX (1) MX220474B (de)
MY (1) MY125244A (de)
TW (1) TW527218B (de)
WO (1) WO2000054877A2 (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010076252A2 (de) 2008-12-29 2010-07-08 Basf Se Verfahren zur reinigung wässriger glyoxal-lösungen

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JP4648515B2 (ja) * 2000-05-02 2011-03-09 株式会社日本触媒 反応器のスタートアップ方法
WO2004052524A1 (de) * 2002-12-12 2004-06-24 Man Dwe Gmbh Mantelrohrreaktor für katalytische gasphasenreaktionen
DE10258153A1 (de) * 2002-12-12 2004-06-24 Basf Ag Verfahren zur Herstellung von Chlor durch Gasphasenoxidation von Chlorwasserstoff
JP4838585B2 (ja) * 2003-07-14 2011-12-14 三菱レイヨン株式会社 固定床多管式反応器
KR101237662B1 (ko) * 2004-05-07 2013-02-26 바스프 에스이 촉매 튜브 다발의 촉매 튜브를 구조화된 방식으로 충진하는방법
DE102005010645A1 (de) * 2005-03-08 2005-08-04 Basf Ag Verfahren zum Befüllen eines Reaktors
EP1909954B2 (de) * 2005-03-08 2016-09-14 Basf Se Verfahren zum befüllen eines reaktors
CN100393404C (zh) * 2005-04-28 2008-06-11 浙江工业大学 一种适用于强放热反应的固定床反应器
WO2007132011A1 (de) * 2006-05-17 2007-11-22 Basf Aktiengesellschaft Verfahren zur herstellung vicinaler dioxoverbindungen durch oxidation vicinaler dihydroxyverbindungen an einer strukturierten katalysatorschüttung
DE102006034811A1 (de) * 2006-07-27 2008-01-31 Man Dwe Gmbh Verfahren zur Temperaturänderung eines Rohrbündelreaktors
WO2010045104A2 (en) * 2008-10-13 2010-04-22 Dow Global Technologies, Inc. Process for the production of chlorinated and/or fluorinated propenes
DE102009001021A1 (de) * 2009-02-19 2010-08-26 Wacker Chemie Ag Verfahren und Vorrichtung zur Herstellung von Vinylacetat
US8581012B2 (en) * 2009-10-09 2013-11-12 Dow Global Technologies, Llc Processes for the production of chlorinated and/or fluorinated propenes and higher alkenes
US20110087056A1 (en) * 2009-10-09 2011-04-14 Dow Global Technologies Adiabatic plug flow reactors and processes incorporating the same
WO2011044514A2 (en) 2009-10-09 2011-04-14 Dow Global Technologies, Inc Isothermal multitube reactors and processes incorporating the same
US8581011B2 (en) * 2009-10-09 2013-11-12 Dow Global Technologies, Llc Process for the production of chlorinated and/or fluorinated propenes
CN103153929B (zh) 2010-10-01 2015-06-03 巴斯夫欧洲公司 提纯乙二醛水溶液的方法
US8461396B2 (en) 2010-10-01 2013-06-11 Basf Se Process for purifying aqueous glyoxal solutions
CA2837292C (en) 2011-05-31 2020-01-28 Max Markus Tirtowidjojo Process for the production of chlorinated propenes
WO2012166393A1 (en) 2011-05-31 2012-12-06 Dow Global Technologies, Llc Process for the production of chlorinated propenes
CA2837956C (en) 2011-06-08 2016-06-28 Dow Agrosciences, Llc Process for the production of chlorinated and/or fluorinated propenes
EP3366661A1 (de) 2011-08-07 2018-08-29 Blue Cube IP LLC Verfahren zur herstellung chlorierter propene
CN103717559A (zh) 2011-08-07 2014-04-09 陶氏环球技术有限责任公司 生产氯化的丙烯的方法
CA2856271A1 (en) 2011-11-21 2013-05-30 Dow Global Technologies Llc Process for the production of chlorinated alkanes
IN2014CN04029A (de) 2011-12-02 2015-10-23 Dow Global Technologies Llc
EP2785670B1 (de) 2011-12-02 2017-10-25 Blue Cube IP LLC Verfahren zur herstellung von chlorierten alkanen
US9334205B2 (en) 2011-12-13 2016-05-10 Blue Cube Ip Llc Process for the production of chlorinated propanes and propenes
CN104011000A (zh) 2011-12-22 2014-08-27 陶氏环球技术有限责任公司 生产四氯甲烷的方法
US9512049B2 (en) 2011-12-23 2016-12-06 Dow Global Technologies Llc Process for the production of alkenes and/or aromatic compounds
CN102744018B (zh) * 2012-06-25 2014-08-27 华东理工大学 一种可调节进口物料温度的固定床催化反应装置
US9321707B2 (en) 2012-09-20 2016-04-26 Blue Cube Ip Llc Process for the production of chlorinated propenes
JP2015529247A (ja) 2012-09-20 2015-10-05 ダウ グローバル テクノロジーズ エルエルシー 塩素化プロペンの生成のためのプロセス
US9440903B2 (en) 2012-09-24 2016-09-13 Arkema Inc. Shell and tube oxidation reactor with improved resistance to fouling
JP6272878B2 (ja) 2012-09-30 2018-01-31 ブルー キューブ アイピー エルエルシー せきクエンチおよびそれを組み込んだ方法
JP6363610B2 (ja) 2012-10-26 2018-07-25 ブルー キューブ アイピー エルエルシー 混合器およびそれを組み込んだプロセス
EP2935165A1 (de) 2012-12-18 2015-10-28 Blue Cube IP LLC Verfahren zur herstellung von chlorierten propenen
CN104918904B (zh) 2012-12-19 2017-10-31 蓝立方知识产权有限责任公司 用于生产氯化丙烯的方法
US9382176B2 (en) 2013-02-27 2016-07-05 Blue Cube Ip Llc Process for the production of chlorinated propenes
WO2014164368A1 (en) 2013-03-09 2014-10-09 Dow Global Technologies Llc Process for the production of chlorinated alkanes
DE102014226928A1 (de) * 2014-12-23 2016-06-23 Siemens Aktiengesellschaft Dampfkraftwerksystem mit Katalysatoranordnung
JP6630721B2 (ja) * 2015-03-23 2020-01-15 千代田化工建設株式会社 合成ガスの製造方法および製造装置
CN105381778A (zh) * 2015-12-18 2016-03-09 张家港市江南锅炉压力容器有限公司 反应釜
DK201700031A1 (en) * 2016-09-27 2017-11-13 Haldor Topsoe As Short Gasket Reactor

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010076252A2 (de) 2008-12-29 2010-07-08 Basf Se Verfahren zur reinigung wässriger glyoxal-lösungen

Also Published As

Publication number Publication date
TW527218B (en) 2003-04-11
CN1231291C (zh) 2005-12-14
MXPA01009012A (es) 2002-01-01
US7226567B1 (en) 2007-06-05
CN1343137A (zh) 2002-04-03
WO2000054877A2 (de) 2000-09-21
KR20020004965A (ko) 2002-01-16
KR100648579B1 (ko) 2006-11-24
BR0009000A (pt) 2002-01-02
MY125244A (en) 2006-07-31
JP2002538951A (ja) 2002-11-19
MX220474B (en) 2004-05-20
BR0009000B1 (pt) 2011-01-25
EP1169119A2 (de) 2002-01-09
ATE251944T1 (de) 2003-11-15
WO2000054877A3 (de) 2001-04-05
ES2209870T3 (es) 2004-07-01
AU4538700A (en) 2000-10-04
EP1169119B1 (de) 2003-10-15
JP5204356B2 (ja) 2013-06-05

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Owner name: BASF SE, 67063 LUDWIGSHAFEN, DE