DE3307974A1 - Verfahren zur gewinnung von stickstoff - Google Patents

Verfahren zur gewinnung von stickstoff

Info

Publication number
DE3307974A1
DE3307974A1 DE19833307974 DE3307974A DE3307974A1 DE 3307974 A1 DE3307974 A1 DE 3307974A1 DE 19833307974 DE19833307974 DE 19833307974 DE 3307974 A DE3307974 A DE 3307974A DE 3307974 A1 DE3307974 A1 DE 3307974A1
Authority
DE
Germany
Prior art keywords
nitrogen
pressure
reactor
gas
product gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE19833307974
Other languages
German (de)
English (en)
Inventor
Burkhard Dr. 4200 Oberhausen Harder
Heinz 4300 Essen Heimbach
Karl Dr. Knoblauch
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bergwerksverband GmbH
Original Assignee
Bergwerksverband GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bergwerksverband GmbH filed Critical Bergwerksverband GmbH
Priority to DE19833307974 priority Critical patent/DE3307974A1/de
Priority to DE8484100647T priority patent/DE3465066D1/de
Priority to EP84100647A priority patent/EP0121042B1/de
Priority to JP59042242A priority patent/JPS59169909A/ja
Priority to ZA841705A priority patent/ZA841705B/xx
Priority to US06/587,241 priority patent/US4548799A/en
Publication of DE3307974A1 publication Critical patent/DE3307974A1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047—Pressure swing adsorption
    • B01D53/0473—Rapid pressure swing adsorption
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • C01B21/0405—Purification or separation processes
    • C01B21/0433—Physical processing only
    • C01B21/045—Physical processing only by adsorption in solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10—Inorganic adsorbents
    • B01D2253/116—Molecular sieves other than zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2253/00—Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/25—Coated, impregnated or composite adsorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2256/00—Main component in the product gas stream after treatment
    • B01D2256/10—Nitrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/10—Single element gases other than halogens
    • B01D2257/104—Oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40035—Equalization
    • B01D2259/40037—Equalization with two sub-steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/40011—Methods relating to the process cycle in pressure or temperature swing adsorption
    • B01D2259/40058—Number of sequence steps, including sub-steps, per cycle
    • B01D2259/40062—Four
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2259/00—Type of treatment
    • B01D2259/40—Further details for adsorption processes and devices
    • B01D2259/402—Further details for adsorption processes and devices using two beds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
DE19833307974 1983-03-07 1983-03-07 Verfahren zur gewinnung von stickstoff Withdrawn DE3307974A1 (de)

Priority Applications (6)

Application Number Priority Date Filing Date Title
DE19833307974 DE3307974A1 (de) 1983-03-07 1983-03-07 Verfahren zur gewinnung von stickstoff
DE8484100647T DE3465066D1 (en) 1983-03-07 1984-01-21 Process for the production of nitrogen
EP84100647A EP0121042B1 (de) 1983-03-07 1984-01-21 Verfahren zur Gewinnung von Stickstoff
JP59042242A JPS59169909A (ja) 1983-03-07 1984-03-07 窒素の製造法
ZA841705A ZA841705B (en) 1983-03-07 1984-03-07 Process for recovering nitrogen from oxygen-containing gas mixtures
US06/587,241 US4548799A (en) 1983-03-07 1984-03-07 Process for recovering nitrogen from oxygen-containing gas mixtures

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19833307974 DE3307974A1 (de) 1983-03-07 1983-03-07 Verfahren zur gewinnung von stickstoff

Publications (1)

Publication Number Publication Date
DE3307974A1 true DE3307974A1 (de) 1984-09-13

Family

ID=6192712

Family Applications (2)

Application Number Title Priority Date Filing Date
DE19833307974 Withdrawn DE3307974A1 (de) 1983-03-07 1983-03-07 Verfahren zur gewinnung von stickstoff
DE8484100647T Expired DE3465066D1 (en) 1983-03-07 1984-01-21 Process for the production of nitrogen

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE8484100647T Expired DE3465066D1 (en) 1983-03-07 1984-01-21 Process for the production of nitrogen

Country Status (5)

Country Link
US (1) US4548799A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
EP (1) EP0121042B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JP (1) JPS59169909A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DE (2) DE3307974A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
ZA (1) ZA841705B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3835164A1 (de) * 1987-10-17 1989-04-27 Tokico Ltd Gastrennungsvorrichtung zur erzeugung eines gasprodukts
DE3941487C1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1989-12-15 1991-04-25 Bergwerksverband Gmbh, 4300 Essen, De

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61266302A (ja) * 1985-05-17 1986-11-26 Seitetsu Kagaku Co Ltd 濃縮酸素回収方法
US5051115A (en) * 1986-05-21 1991-09-24 Linde Aktiengesellschaft Pressure swing adsorption process
GB8622509D0 (en) * 1986-09-18 1986-10-22 Boc Group Plc Separation of gas mixtures
US4767606A (en) * 1986-11-14 1988-08-30 United Technologies Corporation Process and apparatus for producing nitrogen
JPH0194915A (ja) * 1987-10-02 1989-04-13 Kuraray Chem Corp 圧力変動吸着方式による窒素ガス分離方法
DE3830506A1 (de) * 1988-09-08 1990-03-15 Bergwerksverband Gmbh Verfahren zur gewinnung von stickstoff aus sauerstoff und stickstoff enthaltenden gasgemischen mittels druckwechseladsorption an kohlenstoff-molekularsieben
EP0380723B1 (en) * 1989-02-01 1994-04-06 Kuraray Chemical Co., Ltd. Process for separating nitrogen gas by pressure swing adsorption system
JP2575874B2 (ja) * 1989-04-21 1997-01-29 三菱重工業株式会社 自己再生型脱硝方法
US5082474A (en) * 1990-08-14 1992-01-21 The Boc Group, Inc Pressurization psa systems for the production of high purity product gas
US5204003A (en) * 1991-05-08 1993-04-20 The United States Of America As Represented By The United States Department Of Energy Separation processes using expulsion from dilute supercritical solutions
US5183483A (en) * 1991-08-21 1993-02-02 Healthdyne, Inc. Pneumatic circuit control for pressure swing adsorption systems
CA2121312A1 (en) * 1993-04-21 1994-10-22 Shivaji Sircar Adsorption process to produce 99+% oxygen from air
US5433770A (en) * 1993-12-27 1995-07-18 Uop PSA process employing a rapid depressurization step to create a disequilibrium effect
US5441558A (en) * 1994-08-09 1995-08-15 Air Products And Chemicals, Inc. High purity nitrogen PSA utilizing controlled internal flows
US5938979A (en) * 1997-10-31 1999-08-17 Nanogram Corporation Electromagnetic shielding
EP0958887B1 (en) * 1998-05-13 2003-03-19 Enshu Limited Nitrogen gas supply system for dry-cut working machine
US6527831B2 (en) * 2000-12-29 2003-03-04 Praxair Technology, Inc. Argon purification process
DE102011083519A1 (de) * 2011-09-27 2013-03-28 Siemens Ag Transformator mit Stickstofferzeugungseinrichtung
WO2017029764A1 (ja) * 2015-08-20 2017-02-23 システム・インスツルメンツ株式会社 Ｍｓ用窒素ガス安全供給モニターおよび窒素ガス生成装置
US10730006B2 (en) 2018-08-14 2020-08-04 Air Products And Chemicals, Inc. Port separation for rotary bed PSA
US10835856B2 (en) 2018-08-14 2020-11-17 Air Products And Chemicals, Inc. Carbon molecular sieve adsorbent
US10744450B2 (en) 2018-08-14 2020-08-18 Air Products And Chemicals, Inc. Multi-bed rapid cycle kinetic PSA

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3146189A1 (de) * 1981-11-21 1983-05-26 Leybold-Heraeus GmbH, 5000 Köln Verfahren zum betrieb einer druckwechselanlage und nach diesem verfahren arbeitende druckwechselanlage
DE3207089A1 (de) * 1982-02-26 1983-09-15 Union Carbide Corp., 06817 Danbury, Conn. Druckwechseladsorptionsverfahren

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4203958A (en) * 1978-03-06 1980-05-20 General Motors Corporation Process for producing oxygen-free nitrogen atmosphere
GB2025254B (en) * 1978-07-12 1982-09-02 Linde Ag Separating gas mixtures
US4256469A (en) * 1978-11-06 1981-03-17 Linde Aktiengesellschaft Repressurization technique for pressure swing adsorption
DE2932333C2 (de) * 1979-08-09 1986-08-07 Bergwerksverband Gmbh, 4300 Essen Verfahren zur adsorptiven Trennung von neben Stickstoff wenigstens Sauerstoff enthaltenden Gasgemischen
ZA811931B (en) * 1980-03-31 1982-05-26 African Oxygen Ltd Process and apparatus for the separation of gaseous mixture
US4386945A (en) * 1982-02-01 1983-06-07 Litton Systems, Inc. Process and compound bed means for evolving a first component enriched gas
US4440548A (en) * 1982-04-19 1984-04-03 Calgon Carbon Corporation Pressure swing absorption system
JPS598605A (ja) * 1982-07-07 1984-01-17 Osaka Oxgen Ind Ltd 窒素濃縮方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3146189A1 (de) * 1981-11-21 1983-05-26 Leybold-Heraeus GmbH, 5000 Köln Verfahren zum betrieb einer druckwechselanlage und nach diesem verfahren arbeitende druckwechselanlage
DE3207089A1 (de) * 1982-02-26 1983-09-15 Union Carbide Corp., 06817 Danbury, Conn. Druckwechseladsorptionsverfahren

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
US-Z: Chem. Ind. Februar 1983, S.87-90 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3835164A1 (de) * 1987-10-17 1989-04-27 Tokico Ltd Gastrennungsvorrichtung zur erzeugung eines gasprodukts
DE3941487C1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1989-12-15 1991-04-25 Bergwerksverband Gmbh, 4300 Essen, De

Also Published As

Publication number Publication date
EP0121042B1 (de) 1987-07-29
JPH0365206B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1991-10-11
JPS59169909A (ja) 1984-09-26
DE3465066D1 (en) 1987-09-03
US4548799A (en) 1985-10-22
EP0121042A2 (de) 1984-10-10
EP0121042A3 (en) 1986-01-29
ZA841705B (en) 1984-10-31

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