DE3244898C2 - Verfahren zur Abtrennung von mineralischem ultrafeinen Korn aus Waschwässern der Kohleaufbereitung bzw. aus Kohleschlämmen - Google Patents
Verfahren zur Abtrennung von mineralischem ultrafeinen Korn aus Waschwässern der Kohleaufbereitung bzw. aus KohleschlämmenInfo
- Publication number
- DE3244898C2 DE3244898C2 DE3244898A DE3244898A DE3244898C2 DE 3244898 C2 DE3244898 C2 DE 3244898C2 DE 3244898 A DE3244898 A DE 3244898A DE 3244898 A DE3244898 A DE 3244898A DE 3244898 C2 DE3244898 C2 DE 3244898C2
- Authority
- DE
- Germany
- Prior art keywords
- coal
- washing water
- mineral
- molecular weight
- separation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003245 coal Substances 0.000 title claims abstract description 41
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 20
- 238000000034 method Methods 0.000 title claims abstract description 18
- 238000005406 washing Methods 0.000 title claims abstract description 11
- 239000010802 sludge Substances 0.000 title claims abstract description 7
- 238000000926 separation method Methods 0.000 title claims description 8
- 229910052500 inorganic mineral Inorganic materials 0.000 title abstract description 24
- 239000011707 mineral Substances 0.000 title abstract description 24
- 239000002270 dispersing agent Substances 0.000 claims abstract description 25
- 229920000642 polymer Polymers 0.000 claims description 4
- 229920001059 synthetic polymer Polymers 0.000 claims description 4
- 239000006185 dispersion Substances 0.000 claims description 3
- 238000010790 dilution Methods 0.000 claims description 2
- 239000012895 dilution Substances 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 239000011435 rock Substances 0.000 claims 2
- 150000001450 anions Chemical class 0.000 claims 1
- 238000005189 flocculation Methods 0.000 abstract description 8
- 230000016615 flocculation Effects 0.000 abstract description 8
- 125000000129 anionic group Chemical group 0.000 abstract description 7
- 239000007787 solid Substances 0.000 description 18
- 239000002956 ash Substances 0.000 description 14
- 239000008394 flocculating agent Substances 0.000 description 9
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 8
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 8
- 229920001577 copolymer Polymers 0.000 description 7
- 238000005188 flotation Methods 0.000 description 7
- 239000002245 particle Substances 0.000 description 7
- 238000004062 sedimentation Methods 0.000 description 7
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 6
- 239000006228 supernatant Substances 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 5
- 229920006318 anionic polymer Polymers 0.000 description 4
- 239000012141 concentrate Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 239000011734 sodium Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 description 3
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 3
- 229940048053 acrylate Drugs 0.000 description 3
- 238000005065 mining Methods 0.000 description 3
- 229920002401 polyacrylamide Polymers 0.000 description 3
- 229940047670 sodium acrylate Drugs 0.000 description 3
- IRLPACMLTUPBCL-KQYNXXCUSA-N 5'-adenylyl sulfate Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](COP(O)(=O)OS(O)(=O)=O)[C@@H](O)[C@H]1O IRLPACMLTUPBCL-KQYNXXCUSA-N 0.000 description 2
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 2
- 229920006322 acrylamide copolymer Polymers 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 229920000536 2-Acrylamido-2-methylpropane sulfonic acid Polymers 0.000 description 1
- XHZPRMZZQOIPDS-UHFFFAOYSA-N 2-Methyl-2-[(1-oxo-2-propenyl)amino]-1-propanesulfonic acid Chemical compound OS(=O)(=O)CC(C)(C)NC(=O)C=C XHZPRMZZQOIPDS-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 235000002918 Fraxinus excelsior Nutrition 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229920002845 Poly(methacrylic acid) Polymers 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 240000003834 Triticum spelta Species 0.000 description 1
- 150000001252 acrylic acid derivatives Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 241001233037 catfish Species 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropanol acetate Natural products CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 description 1
- 229940011051 isopropyl acetate Drugs 0.000 description 1
- FQPSGWSUVKBHSU-UHFFFAOYSA-N methacrylamide Chemical compound CC(=C)C(N)=O FQPSGWSUVKBHSU-UHFFFAOYSA-N 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 229920000058 polyacrylate Polymers 0.000 description 1
- 239000004584 polyacrylic acid Substances 0.000 description 1
- 229920000867 polyelectrolyte Polymers 0.000 description 1
- 229920001444 polymaleic acid Polymers 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000009666 routine test Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000009331 sowing Methods 0.000 description 1
- 229920001897 terpolymer Polymers 0.000 description 1
- 239000011882 ultra-fine particle Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D21/00—Separation of suspended solid particles from liquids by sedimentation
- B01D21/01—Separation of suspended solid particles from liquids by sedimentation using flocculating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B1/00—Conditioning for facilitating separation by altering physical properties of the matter to be treated
- B03B1/04—Conditioning for facilitating separation by altering physical properties of the matter to be treated by additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B9/00—General arrangement of separating plant, e.g. flow sheets
- B03B9/005—General arrangement of separating plant, e.g. flow sheets specially adapted for coal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D3/00—Differential sedimentation
- B03D3/06—Flocculation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3244898A DE3244898C2 (de) | 1982-12-04 | 1982-12-04 | Verfahren zur Abtrennung von mineralischem ultrafeinen Korn aus Waschwässern der Kohleaufbereitung bzw. aus Kohleschlämmen |
| CA000442398A CA1227294A (en) | 1982-12-04 | 1983-12-01 | Process for separating mineral ultra-fine grain from washings obtained in coal processing or from coal slurries |
| BE0/211968A BE898360A (fr) | 1982-12-04 | 1983-12-02 | Procédé pour séparer les particules minérales ultra-fines des eaux de lavages du charbon ou de schlamms de charbon. |
| AU21942/83A AU572479B2 (en) | 1982-12-04 | 1983-12-02 | Process for separating mineral ultra-fine grain from washings (eg. flocculation) |
| FR8319345A FR2537016B1 (fr) | 1982-12-04 | 1983-12-02 | Procede pour separer les particules minerales ultra-fines des eaux de lavage d'operations de traitement du charbon ou de schlamms de charbons |
| PL1983244887A PL140420B1 (en) | 1982-12-04 | 1983-12-02 | Method of separating mineral ultrafine grains from coal processing washing or coal slurry |
| ZA838980A ZA838980B (en) | 1982-12-04 | 1983-12-02 | Process for separating ultra-fine mineral particles from coal washings |
| IN812/DEL/83A IN160097B (enExample) | 1982-12-04 | 1983-12-02 | |
| GB08332401A GB2134416B (en) | 1982-12-04 | 1983-12-05 | Process for separating mineral finest grain from washings obtained in coal processing or from coal slurries |
| US06/741,765 US4618414A (en) | 1982-12-04 | 1985-06-06 | Process for separating mineral ultra-fine grain from washings obtained in coal processing or from coal slurries |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3244898A DE3244898C2 (de) | 1982-12-04 | 1982-12-04 | Verfahren zur Abtrennung von mineralischem ultrafeinen Korn aus Waschwässern der Kohleaufbereitung bzw. aus Kohleschlämmen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3244898A1 DE3244898A1 (de) | 1984-06-07 |
| DE3244898C2 true DE3244898C2 (de) | 1985-04-11 |
Family
ID=6179795
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3244898A Expired DE3244898C2 (de) | 1982-12-04 | 1982-12-04 | Verfahren zur Abtrennung von mineralischem ultrafeinen Korn aus Waschwässern der Kohleaufbereitung bzw. aus Kohleschlämmen |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4618414A (enExample) |
| AU (1) | AU572479B2 (enExample) |
| BE (1) | BE898360A (enExample) |
| CA (1) | CA1227294A (enExample) |
| DE (1) | DE3244898C2 (enExample) |
| FR (1) | FR2537016B1 (enExample) |
| GB (1) | GB2134416B (enExample) |
| IN (1) | IN160097B (enExample) |
| PL (1) | PL140420B1 (enExample) |
| ZA (1) | ZA838980B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3836064A1 (de) * | 1987-10-22 | 1989-05-03 | Greenwald Sen | Verfahren zum abtrennen von ton aus ultrafeiner kohle und zur anschliessenden entwaesserung der kohle sowie vorrichtung zur durchfuehrung des verfahrens |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8513868D0 (en) * | 1985-06-01 | 1985-07-03 | British Petroleum Co Plc | Removing mineral matter from solid carbonaceous fuels |
| GB2175916B (en) * | 1985-06-01 | 1988-11-09 | British Petroleum Co Plc | Removing mineral matter from solid carbonaceous fuels |
| US4770766A (en) * | 1986-03-12 | 1988-09-13 | Otisca Industries, Ltd. | Time-controlled processes for agglomerating coal |
| US4857221A (en) * | 1986-05-14 | 1989-08-15 | Fospur Limited | Recovering coal fines |
| US4778598A (en) * | 1987-02-02 | 1988-10-18 | Zimpro Inc. | Separation of ash from regenerated adsorbent |
| US4859318A (en) * | 1987-10-16 | 1989-08-22 | Fospur Limited | Recovering coal fines |
| US5795484A (en) * | 1987-10-22 | 1998-08-18 | Greenwald, Sr.; Edward H. | Method and apparatus for dewatering |
| US5236596A (en) * | 1987-10-22 | 1993-08-17 | Greenwald Sr Edward H | Method and apparatus for dewatering |
| GB8726857D0 (en) * | 1987-11-17 | 1987-12-23 | Fospur Ltd | Froth floatation of mineral fines |
| US5089142A (en) * | 1990-10-30 | 1992-02-18 | Betz Laboratories, Inc. | Methods for dewatering coal and mineral concentrates |
| US6544425B2 (en) * | 2001-02-16 | 2003-04-08 | Slurry Cleanup Environmental, Inc. | Method for dewatering coal tailings and slurries and removing contaminants therefrom |
| DE10111300B4 (de) * | 2001-03-09 | 2007-12-13 | Schenk, Jürgen | Aufbereitungsvorrichtung insbesondere für Aushub |
| RU2220006C1 (ru) * | 2002-09-05 | 2003-12-27 | Всероссийский научно-исследовательский институт минерального сырья им. Н.М. Федоровского | Способ флотации тонкодисперсных ниобиевых руд |
| US7189327B2 (en) * | 2004-04-08 | 2007-03-13 | Nalco Company | Use of anionic copolymers for enhanced recovery of useful coal and potassium chloride from screen bowl centrifuge |
| FR2931367B1 (fr) * | 2008-05-21 | 2010-12-17 | Coatex Sas | Procede de combustion du charbon avec mise en oeuvre d'un agent absorbant en dispersion aqueuse, cendres obtenues et leurs utilisations |
| CN105728204B (zh) * | 2016-03-22 | 2018-04-03 | 中国矿业大学 | 一种微细粒炼焦煤的选择性絮凝分选工艺 |
| CN111762856A (zh) * | 2020-06-28 | 2020-10-13 | 宁夏神耀科技有限责任公司 | 一种处理煤气化黑水的自动化连续加药系统 |
| CN113413643B (zh) * | 2021-07-26 | 2022-07-01 | 中建西部建设建材科学研究院有限公司 | 一种混凝土搅拌站废浆高效沉降方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA825235A (en) * | 1969-10-14 | P. Priesing Charles | Process for dewatering organic waste solids | |
| US3418237A (en) * | 1963-12-22 | 1968-12-24 | American Cyanamid Co | Settling of non-argillaceous ore pulps and mineral suspensions by use of water-soluble acrylic polymers |
| US3408293A (en) * | 1966-04-11 | 1968-10-29 | Nalco Chemical Co | Coal slurry clarification |
| US3717574A (en) * | 1971-09-21 | 1973-02-20 | American Cyanamid Co | Flocculation of coal slimes |
| CA1050179A (en) * | 1975-01-13 | 1979-03-06 | Leonard Messer | Method of reclaiming water and coal from coal treatment underflow by two-stage separation of solids |
| US4133747A (en) * | 1976-10-14 | 1979-01-09 | Canadian Patents & Development Limited | Method for processing raw coal |
| AU516444B2 (en) * | 1977-08-25 | 1981-06-04 | Edward High Robert | Dewatering coal |
| US4186887A (en) * | 1978-08-15 | 1980-02-05 | Otisca Industries, Ltd. | Processes for recovering coal |
| CA1130231A (en) * | 1978-11-08 | 1982-08-24 | Douglas V. Keller, Jr. | Coal recovery process |
| GB2059811B (en) * | 1979-10-15 | 1983-01-06 | English Olays Lovering Pochin | Beneficiation of minerals |
| ZA818636B (en) * | 1980-12-30 | 1982-10-27 | Union Carbide Corp | A process for the flocculation of mineral containing slurries |
| CA1198704A (en) * | 1981-03-24 | 1985-12-31 | Douglas V. Keller, Jr. | Agglomeration type coal recovery processes |
-
1982
- 1982-12-04 DE DE3244898A patent/DE3244898C2/de not_active Expired
-
1983
- 1983-12-01 CA CA000442398A patent/CA1227294A/en not_active Expired
- 1983-12-02 IN IN812/DEL/83A patent/IN160097B/en unknown
- 1983-12-02 AU AU21942/83A patent/AU572479B2/en not_active Ceased
- 1983-12-02 PL PL1983244887A patent/PL140420B1/pl unknown
- 1983-12-02 FR FR8319345A patent/FR2537016B1/fr not_active Expired
- 1983-12-02 BE BE0/211968A patent/BE898360A/fr not_active IP Right Cessation
- 1983-12-02 ZA ZA838980A patent/ZA838980B/xx unknown
- 1983-12-05 GB GB08332401A patent/GB2134416B/en not_active Expired
-
1985
- 1985-06-06 US US06/741,765 patent/US4618414A/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3836064A1 (de) * | 1987-10-22 | 1989-05-03 | Greenwald Sen | Verfahren zum abtrennen von ton aus ultrafeiner kohle und zur anschliessenden entwaesserung der kohle sowie vorrichtung zur durchfuehrung des verfahrens |
Also Published As
| Publication number | Publication date |
|---|---|
| AU2194283A (en) | 1984-06-07 |
| DE3244898A1 (de) | 1984-06-07 |
| PL244887A1 (en) | 1984-07-30 |
| FR2537016B1 (fr) | 1988-04-15 |
| PL140420B1 (en) | 1987-04-30 |
| ZA838980B (en) | 1984-08-29 |
| BE898360A (fr) | 1984-03-30 |
| GB2134416A (en) | 1984-08-15 |
| US4618414A (en) | 1986-10-21 |
| GB2134416B (en) | 1986-02-26 |
| FR2537016A1 (fr) | 1984-06-08 |
| GB8332401D0 (en) | 1984-01-11 |
| IN160097B (enExample) | 1987-06-27 |
| CA1227294A (en) | 1987-09-22 |
| AU572479B2 (en) | 1988-05-12 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |