DE3114147A1 - Verfahren zur gewinnung von aldehyden - Google Patents
Verfahren zur gewinnung von aldehydenInfo
- Publication number
- DE3114147A1 DE3114147A1 DE19813114147 DE3114147A DE3114147A1 DE 3114147 A1 DE3114147 A1 DE 3114147A1 DE 19813114147 DE19813114147 DE 19813114147 DE 3114147 A DE3114147 A DE 3114147A DE 3114147 A1 DE3114147 A1 DE 3114147A1
- Authority
- DE
- Germany
- Prior art keywords
- column
- aldehydes
- gas
- hydroformylation
- phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 150000001299 aldehydes Chemical class 0.000 title claims abstract description 31
- 238000000034 method Methods 0.000 title claims abstract description 15
- 238000007037 hydroformylation reaction Methods 0.000 claims abstract description 13
- 239000012071 phase Substances 0.000 claims abstract description 12
- 239000007791 liquid phase Substances 0.000 claims abstract description 8
- 150000001875 compounds Chemical class 0.000 claims abstract description 7
- 239000003054 catalyst Substances 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims abstract description 6
- 229910052703 rhodium Inorganic materials 0.000 claims abstract description 6
- 239000010948 rhodium Substances 0.000 claims abstract description 6
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000004821 distillation Methods 0.000 claims abstract description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 238000003786 synthesis reaction Methods 0.000 claims description 3
- 230000002040 relaxant effect Effects 0.000 claims description 2
- 230000006835 compression Effects 0.000 claims 1
- 238000007906 compression Methods 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 239000007789 gas Substances 0.000 abstract description 28
- 239000002912 waste gas Substances 0.000 abstract description 2
- NBBJYMSMWIIQGU-UHFFFAOYSA-N Propionic aldehyde Chemical compound CCC=O NBBJYMSMWIIQGU-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- ZTQSAGDEMFDKMZ-UHFFFAOYSA-N butyric aldehyde Natural products CCCC=O ZTQSAGDEMFDKMZ-UHFFFAOYSA-N 0.000 description 7
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 5
- 239000005977 Ethylene Substances 0.000 description 5
- 150000001336 alkenes Chemical class 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 238000009835 boiling Methods 0.000 description 3
- 238000007872 degassing Methods 0.000 description 3
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000012188 paraffin wax Substances 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000003303 reheating Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- HGBOYTHUEUWSSQ-UHFFFAOYSA-N valeric aldehyde Natural products CCCCC=O HGBOYTHUEUWSSQ-UHFFFAOYSA-N 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/49—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide
- C07C45/50—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide by oxo-reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/06—Reactor-distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/09—Plural feed
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19813114147 DE3114147A1 (de) | 1981-04-08 | 1981-04-08 | Verfahren zur gewinnung von aldehyden |
| US06/363,565 US4479012A (en) | 1981-04-08 | 1982-03-30 | Recovery of aldehydes from hydroformylation reaction gas |
| EP82102664A EP0062282B1 (de) | 1981-04-08 | 1982-03-30 | Verfahren zur Gewinnung von Aldehyden |
| DE8282102664T DE3260698D1 (en) | 1981-04-08 | 1982-03-30 | Process for obtaining aldehydes |
| CA000399835A CA1173060A (en) | 1981-04-08 | 1982-03-30 | Obtaining aldehydes |
| AT82102664T ATE9322T1 (de) | 1981-04-08 | 1982-03-30 | Verfahren zur gewinnung von aldehyden. |
| JP57056156A JPS57179131A (en) | 1981-04-08 | 1982-04-06 | Manufacture of aldehyde |
| ES511259A ES511259A0 (es) | 1981-04-08 | 1982-04-07 | Procedimiento para obtener aldehidos. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19813114147 DE3114147A1 (de) | 1981-04-08 | 1981-04-08 | Verfahren zur gewinnung von aldehyden |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3114147A1 true DE3114147A1 (de) | 1982-10-28 |
Family
ID=6129658
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19813114147 Withdrawn DE3114147A1 (de) | 1981-04-08 | 1981-04-08 | Verfahren zur gewinnung von aldehyden |
| DE8282102664T Expired DE3260698D1 (en) | 1981-04-08 | 1982-03-30 | Process for obtaining aldehydes |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE8282102664T Expired DE3260698D1 (en) | 1981-04-08 | 1982-03-30 | Process for obtaining aldehydes |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4479012A (https=) |
| EP (1) | EP0062282B1 (https=) |
| JP (1) | JPS57179131A (https=) |
| AT (1) | ATE9322T1 (https=) |
| CA (1) | CA1173060A (https=) |
| DE (2) | DE3114147A1 (https=) |
| ES (1) | ES511259A0 (https=) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0144745A1 (de) * | 1983-11-12 | 1985-06-19 | Ruhrchemie Aktiengesellschaft | Verfahren zur Herstellung von Aldehyden |
| US4778929A (en) * | 1986-07-25 | 1988-10-18 | Basf Aktiengesellschaft | Continuous hydroformylation of olefinically unsaturated compounds |
Families Citing this family (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3245883A1 (de) * | 1982-12-11 | 1984-06-14 | Ruhrchemie Ag, 4200 Oberhausen | Verfahren zur hydroformylierung von olefinen |
| US4613701A (en) * | 1985-09-19 | 1986-09-23 | Celanese Corporation | Recovery of rhodium from hydroformylation reaction product |
| EP0313559B1 (en) * | 1986-07-01 | 1991-08-28 | DAVY McKEE (LONDON) LIMITED | Process for the production of aldehydes by hydroformylation |
| GB2192182B (en) * | 1986-07-01 | 1990-05-23 | Davy Mckee | Process for the production of aldehydes |
| US4871879A (en) * | 1987-10-27 | 1989-10-03 | Hoechst Celanese Corporation | Rhodium recovery from hydroformylation reaction product |
| US5180854A (en) * | 1988-07-14 | 1993-01-19 | Union Carbide Chemicals & Plastics Technology Corporation | Process for catalyst aldehyde product separation |
| US5001274A (en) * | 1989-06-23 | 1991-03-19 | Union Carbide Chemicals And Plastics Company Inc. | Hydroformylation process |
| US5102505A (en) * | 1990-11-09 | 1992-04-07 | Union Carbide Chemicals & Plastics Technology Corporation | Mixed aldehyde product separation by distillation |
| DE4214738A1 (de) * | 1992-05-04 | 1993-11-11 | Bayer Ag | Destillationskolonne mit dampfförmiger Seitenstromentnahme |
| ZA96178B (en) * | 1995-01-18 | 1997-06-30 | Exxon Chemical Patents Inc | Organic compounds and processes for their manufacture |
| DE19914259A1 (de) * | 1999-03-29 | 2000-10-05 | Basf Ag | Verfahren zur destillativen Auftrennung eines flüssigen Rohaldehydgemisches |
| CN101688024B (zh) | 2007-06-28 | 2013-01-09 | 巴斯夫欧洲公司 | 含有有机黑色颜料的热塑性模塑材料 |
| US9340480B2 (en) | 2013-04-30 | 2016-05-17 | Oxea Corporation | Aldehyde production process with multi-stage condensation |
| GB201604608D0 (en) | 2016-03-18 | 2016-05-04 | Johnson Matthey Davy Technologies Ltd | Process |
| EP3429984A1 (en) | 2016-03-18 | 2019-01-23 | Dow Technology Investments LLC | Hydroformylation process |
| US11365357B2 (en) | 2019-05-24 | 2022-06-21 | Eastman Chemical Company | Cracking C8+ fraction of pyoil |
| CN113891928B (zh) | 2019-05-24 | 2024-10-29 | 伊士曼化工公司 | 裂化热解油的c4-c7馏分 |
| US11946000B2 (en) | 2019-05-24 | 2024-04-02 | Eastman Chemical Company | Blend small amounts of pyoil into a liquid stream processed into a gas cracker |
| US12497467B2 (en) | 2019-05-24 | 2025-12-16 | Exxon Mobil Product Solutions Company | Recycle content cellulose ester |
| US12031091B2 (en) | 2019-05-24 | 2024-07-09 | Eastman Chemical Company | Recycle content cracked effluent |
| US20220325036A1 (en) | 2019-07-29 | 2022-10-13 | Eastman Chemical Company | Process for the preparation of polyesters with recycled monomers from pyrolysis and methanolysis |
| CN119912669A (zh) | 2019-07-29 | 2025-05-02 | 伊士曼化工公司 | 回收成分环丁二醇聚酯 |
| US20220281796A1 (en) | 2019-07-29 | 2022-09-08 | Eastman Chemical Company | Recycle content (c4)alkanoic acid |
| US12338211B2 (en) | 2019-07-29 | 2025-06-24 | Eastman Chemical Company | Recycle content (C4)alkanal |
| US11319262B2 (en) | 2019-10-31 | 2022-05-03 | Eastman Chemical Company | Processes and systems for making recycle content hydrocarbons |
| EP4051762A4 (en) | 2019-10-31 | 2023-12-27 | Eastman Chemical Company | PYROLYSIS PROCESS AND SYSTEM FOR RECYCLED WASTE |
| US11945998B2 (en) | 2019-10-31 | 2024-04-02 | Eastman Chemical Company | Processes and systems for making recycle content hydrocarbons |
| US12528995B2 (en) | 2019-10-31 | 2026-01-20 | ExxonMobil Product Solutions Company | Pyrolysis method and system for recycled waste |
| EP4055001A4 (en) | 2019-11-07 | 2024-02-14 | Eastman Chemical Company | MIXED ESTERS AND SOLVENTS WITH RECYCLED CONTENTS |
| CN114728868B (zh) | 2019-11-07 | 2024-09-03 | 伊士曼化工公司 | 回收成分羰基合成醇和羰基合成增塑剂 |
| CN118851872A (zh) | 2019-11-07 | 2024-10-29 | 伊士曼化工公司 | 回收成分丙醇 |
| US11939534B2 (en) | 2019-11-07 | 2024-03-26 | Eastman Chemical Company | Recycle content alpha olefins and fatty alcohols |
| BR112022015078A2 (pt) | 2020-02-10 | 2023-02-14 | Eastman Chem Co | Método para processar plástico residual, e, composição de coproduto de solvólise |
| CN115052730A (zh) | 2020-02-10 | 2022-09-13 | 伊士曼化工公司 | 处理的混合塑料废物流的化学回收 |
| BR112022015310A2 (pt) | 2020-02-10 | 2022-10-11 | Eastman Chem Co | Montagem de braço de arraste, suspensão de eixo de roda, braço de arraste, e, método para fabricar um braço de arraste |
| US12195674B2 (en) | 2021-09-21 | 2025-01-14 | Eastman Chemical Company | Using spent caustic solution from pygas treatment to neutralize halogens from liquified waste plastic |
| WO2025040614A1 (de) | 2023-08-22 | 2025-02-27 | Röhm Gmbh | Decarbonisierung der (meth)acrylat-herstellung |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2617756A (en) * | 1950-05-20 | 1952-11-11 | Stanolind Oil & Gas Co | Process for recovery and purification of propionaldehyde |
| US2821559A (en) * | 1951-07-25 | 1958-01-28 | British Petroleum Co | Production of aldehydes |
| US2757203A (en) * | 1955-04-15 | 1956-07-31 | Exxon Research Engineering Co | Synthesis of alcoiiol and aldehyde from olefins, carbon monoxide and hydrogen |
| US2995575A (en) * | 1956-11-30 | 1961-08-08 | Union Carbide Corp | High pressure oxo conversion process |
| US3092670A (en) * | 1957-08-16 | 1963-06-04 | Gulf Research Development Co | Oxo process for the production of alcohols |
| US3501531A (en) * | 1964-12-15 | 1970-03-17 | Ethyl Corp | Hydroformylation process |
| US3791935A (en) * | 1971-11-10 | 1974-02-12 | Monsanto Co | Purification of carboxylic acids |
| CA1090823A (en) * | 1976-04-08 | 1980-12-02 | Everard A.V. Brewester | Cyclic hydroformylation process |
| DE2737633C2 (de) * | 1977-08-20 | 1979-09-27 | Ruhrchemie Ag, 4200 Oberhausen | Verfahren zur Herstellung von Aldehyden |
| DE2749890B2 (de) * | 1977-11-08 | 1980-05-08 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Rückgewinnung von Propen bzw. Propen-Propan-Gemischen aus den Abgasen der HydroformyUerung von Propen |
| DE2965157D1 (en) * | 1979-03-21 | 1983-05-11 | Davy Mckee London | Process for the production of aldehydes by hydroformylation of alkenes |
| DE2928314A1 (de) * | 1979-07-13 | 1981-02-12 | Ruhrchemie Ag | Verfahren zur herstellung von aldehyden |
-
1981
- 1981-04-08 DE DE19813114147 patent/DE3114147A1/de not_active Withdrawn
-
1982
- 1982-03-30 DE DE8282102664T patent/DE3260698D1/de not_active Expired
- 1982-03-30 CA CA000399835A patent/CA1173060A/en not_active Expired
- 1982-03-30 US US06/363,565 patent/US4479012A/en not_active Expired - Lifetime
- 1982-03-30 AT AT82102664T patent/ATE9322T1/de not_active IP Right Cessation
- 1982-03-30 EP EP82102664A patent/EP0062282B1/de not_active Expired
- 1982-04-06 JP JP57056156A patent/JPS57179131A/ja active Granted
- 1982-04-07 ES ES511259A patent/ES511259A0/es active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0144745A1 (de) * | 1983-11-12 | 1985-06-19 | Ruhrchemie Aktiengesellschaft | Verfahren zur Herstellung von Aldehyden |
| US4778929A (en) * | 1986-07-25 | 1988-10-18 | Basf Aktiengesellschaft | Continuous hydroformylation of olefinically unsaturated compounds |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0062282B1 (de) | 1984-09-12 |
| EP0062282A2 (de) | 1982-10-13 |
| EP0062282A3 (en) | 1983-05-18 |
| JPH0155256B2 (https=) | 1989-11-22 |
| US4479012A (en) | 1984-10-23 |
| ES8304057A1 (es) | 1983-02-16 |
| CA1173060A (en) | 1984-08-21 |
| ATE9322T1 (de) | 1984-09-15 |
| JPS57179131A (en) | 1982-11-04 |
| ES511259A0 (es) | 1983-02-16 |
| DE3260698D1 (en) | 1984-10-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8130 | Withdrawal |