DE3111331A1 - "verfahren zur verhinderung von korrosion und wasserstoff-versproedung von aus tantal hergestellten einrichtungen, in denen heisse konzentrierte schwefelsaeure gehandhabt wird" - Google Patents
"verfahren zur verhinderung von korrosion und wasserstoff-versproedung von aus tantal hergestellten einrichtungen, in denen heisse konzentrierte schwefelsaeure gehandhabt wird"Info
- Publication number
- DE3111331A1 DE3111331A1 DE19813111331 DE3111331A DE3111331A1 DE 3111331 A1 DE3111331 A1 DE 3111331A1 DE 19813111331 DE19813111331 DE 19813111331 DE 3111331 A DE3111331 A DE 3111331A DE 3111331 A1 DE3111331 A1 DE 3111331A1
- Authority
- DE
- Germany
- Prior art keywords
- sulfuric acid
- concentrated sulfuric
- tantalum
- corrosion
- test
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title claims description 49
- 238000005260 corrosion Methods 0.000 title claims description 31
- 230000007797 corrosion Effects 0.000 title claims description 31
- 239000001257 hydrogen Substances 0.000 title claims description 25
- 229910052739 hydrogen Inorganic materials 0.000 title claims description 25
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical class [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims description 22
- 238000000034 method Methods 0.000 title claims description 21
- 229910052715 tantalum Inorganic materials 0.000 claims description 30
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims description 30
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 24
- 229910017604 nitric acid Inorganic materials 0.000 claims description 24
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 13
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 claims description 11
- 239000007800 oxidant agent Substances 0.000 claims description 11
- JPVYNHNXODAKFH-UHFFFAOYSA-N Cu2+ Chemical compound [Cu+2] JPVYNHNXODAKFH-UHFFFAOYSA-N 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 4
- SYRHIZPPCHMRIT-UHFFFAOYSA-N tin(4+) Chemical compound [Sn+4] SYRHIZPPCHMRIT-UHFFFAOYSA-N 0.000 claims description 4
- 150000002500 ions Chemical class 0.000 claims description 3
- 229910021645 metal ion Inorganic materials 0.000 claims description 3
- -1 tin (IV) ion Chemical class 0.000 claims description 3
- XTEGARKTQYYJKE-UHFFFAOYSA-M Chlorate Chemical class [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 claims 1
- 244000078856 Prunus padus Species 0.000 claims 1
- 150000002823 nitrates Chemical class 0.000 claims 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims 1
- 238000007792 addition Methods 0.000 description 17
- 230000002285 radioactive effect Effects 0.000 description 9
- 238000005452 bending Methods 0.000 description 7
- 239000000243 solution Substances 0.000 description 6
- 238000009835 boiling Methods 0.000 description 5
- 239000010949 copper Substances 0.000 description 5
- 239000002910 solid waste Substances 0.000 description 5
- 239000012085 test solution Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical class [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 3
- 230000015556 catabolic process Effects 0.000 description 3
- 238000000354 decomposition reaction Methods 0.000 description 3
- 238000006731 degradation reaction Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 150000002431 hydrogen Chemical class 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- PXXFCBNDPUWVDY-UHFFFAOYSA-N [Ta].S(O)(O)(=O)=O Chemical compound [Ta].S(O)(O)(=O)=O PXXFCBNDPUWVDY-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000000184 acid digestion Methods 0.000 description 1
- 235000013405 beer Nutrition 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 239000010970 precious metal Substances 0.000 description 1
- 239000012857 radioactive material Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/04—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in markedly acid liquids
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21F—PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
- G21F9/00—Treating radioactively contaminated material; Decontamination arrangements therefor
- G21F9/04—Treating liquids
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP3621880A JPS56133474A (en) | 1980-03-24 | 1980-03-24 | Apparatus made of tantalum and usable for hot sulfuric acid and preventing method for corrosion and hydrogen embrittlement of said apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE3111331A1 true DE3111331A1 (de) | 1982-02-18 |
Family
ID=12463618
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19813111331 Withdrawn DE3111331A1 (de) | 1980-03-24 | 1981-03-23 | "verfahren zur verhinderung von korrosion und wasserstoff-versproedung von aus tantal hergestellten einrichtungen, in denen heisse konzentrierte schwefelsaeure gehandhabt wird" |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4356148A (enExample) |
| JP (1) | JPS56133474A (enExample) |
| DE (1) | DE3111331A1 (enExample) |
| FR (1) | FR2478678A1 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5931039B2 (ja) * | 1980-05-16 | 1984-07-30 | 動力炉・核燃料開発事業団 | タンタル製酸消化釜による酸消化処理方法 |
| JPS5928879B2 (ja) * | 1980-05-16 | 1984-07-16 | 動力炉・核燃料開発事業団 | タンタル製酸消化釜による酸消化処理の運転制御方法 |
| AU2012204789B2 (en) | 2011-01-05 | 2016-11-10 | Ecolab Usa Inc. | Aqueous acid cleaning, corrosion and stain inhibiting compositions in the vapor phase comprising a blend of nitric and sulfuric acid |
| CA2819127C (en) | 2011-01-05 | 2021-05-25 | Ecolab Usa Inc. | Acid cleaning and corrosion inhibiting compositions comprising a blend of nitric and sulfuric acid |
| CN119506899A (zh) | 2018-11-22 | 2025-02-25 | 艺康美国股份有限公司 | 用来增强污垢去除的酸性cip/cop清洗组合物 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1012474A (fr) * | 1949-10-04 | 1952-07-10 | Electro Chimie Soc D | Procédé pour empêcher les aciers inoxydables d'être corrodés par l'acide sulfurique |
| DE2807361A1 (de) * | 1977-02-23 | 1978-08-24 | Naphtachimie Sa | Verfahren zur herstellung von katalysatoren fuer die polymerisation von alpha-olefinen |
| US4154791A (en) * | 1977-12-27 | 1979-05-15 | Allied Chemical Corporation | Inhibition of corrosive attack by sulfuric acid on carbon steel |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3957676A (en) * | 1972-09-22 | 1976-05-18 | The United States Of America As Represented By The United States Energy Research And Development Administration | Chemical digestion of low level nuclear solid waste material |
| IT1087257B (it) * | 1977-10-14 | 1985-06-04 | Montedison Spa | Procedimento per concentrare acido solforino inibendo i fenomeni di corrosione |
-
1980
- 1980-03-24 JP JP3621880A patent/JPS56133474A/ja active Granted
-
1981
- 1981-03-13 US US06/243,399 patent/US4356148A/en not_active Expired - Fee Related
- 1981-03-20 FR FR8105624A patent/FR2478678A1/fr active Granted
- 1981-03-23 DE DE19813111331 patent/DE3111331A1/de not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1012474A (fr) * | 1949-10-04 | 1952-07-10 | Electro Chimie Soc D | Procédé pour empêcher les aciers inoxydables d'être corrodés par l'acide sulfurique |
| DE2807361A1 (de) * | 1977-02-23 | 1978-08-24 | Naphtachimie Sa | Verfahren zur herstellung von katalysatoren fuer die polymerisation von alpha-olefinen |
| US4154791A (en) * | 1977-12-27 | 1979-05-15 | Allied Chemical Corporation | Inhibition of corrosive attack by sulfuric acid on carbon steel |
Also Published As
| Publication number | Publication date |
|---|---|
| US4356148A (en) | 1982-10-26 |
| FR2478678A1 (fr) | 1981-09-25 |
| JPS5727939B2 (enExample) | 1982-06-14 |
| FR2478678B1 (enExample) | 1984-12-07 |
| JPS56133474A (en) | 1981-10-19 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8110 | Request for examination paragraph 44 | ||
| 8139 | Disposal/non-payment of the annual fee |