DE2629009C2 - Vorrichtung zur kontinuierlichen Sulfonierung oder Sulfatierung organischer Flüssigkeiten - Google Patents
Vorrichtung zur kontinuierlichen Sulfonierung oder Sulfatierung organischer FlüssigkeitenInfo
- Publication number
- DE2629009C2 DE2629009C2 DE2629009A DE2629009A DE2629009C2 DE 2629009 C2 DE2629009 C2 DE 2629009C2 DE 2629009 A DE2629009 A DE 2629009A DE 2629009 A DE2629009 A DE 2629009A DE 2629009 C2 DE2629009 C2 DE 2629009C2
- Authority
- DE
- Germany
- Prior art keywords
- reaction
- annular
- sulfonated
- liquid
- feed arrangement
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007788 liquid Substances 0.000 title claims description 51
- 238000006277 sulfonation reaction Methods 0.000 title claims description 28
- 230000019635 sulfation Effects 0.000 title claims description 8
- 238000005670 sulfation reaction Methods 0.000 title claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 47
- 239000010409 thin film Substances 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 2
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 20
- 239000013543 active substance Substances 0.000 description 10
- 125000004432 carbon atom Chemical group C* 0.000 description 10
- 239000010408 film Substances 0.000 description 10
- 239000007795 chemical reaction product Substances 0.000 description 8
- 238000002474 experimental method Methods 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000011148 porous material Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 150000004996 alkyl benzenes Chemical class 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000004040 coloring Methods 0.000 description 4
- 239000000498 cooling water Substances 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- -1 alkylbenzene sulfonate Chemical class 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 239000004711 α-olefin Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 150000008051 alkyl sulfates Chemical class 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- 229910000906 Bronze Inorganic materials 0.000 description 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 239000010974 bronze Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 125000002573 ethenylidene group Chemical group [*]=C=C([H])[H] 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 150000007530 organic bases Chemical class 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/247—Suited for forming thin films
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/02—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor of the thin-film type
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B45/00—Formation or introduction of functional groups containing sulfur
- C07B45/02—Formation or introduction of functional groups containing sulfur of sulfo or sulfonyldioxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP50080645A JPS525712A (en) | 1975-06-30 | 1975-06-30 | Apparatus for continuous sulfonation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2629009A1 DE2629009A1 (de) | 1977-05-05 |
| DE2629009C2 true DE2629009C2 (de) | 1983-08-18 |
Family
ID=13724094
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2629009A Expired DE2629009C2 (de) | 1975-06-30 | 1976-06-28 | Vorrichtung zur kontinuierlichen Sulfonierung oder Sulfatierung organischer Flüssigkeiten |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4036596A (en, 2012) |
| JP (1) | JPS525712A (en, 2012) |
| AU (1) | AU502019B2 (en, 2012) |
| DE (1) | DE2629009C2 (en, 2012) |
| GB (1) | GB1505956A (en, 2012) |
| SU (1) | SU1072792A3 (en, 2012) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7258680B2 (en) | 2002-09-02 | 2007-08-21 | Unomedical A/S | Device for subcutaneous administration of a medicament to a patient |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4272462A (en) * | 1980-09-11 | 1981-06-09 | The Trane Company | Liquid wetted gas cooled heat exchanger |
| JPS57147502A (en) * | 1981-03-09 | 1982-09-11 | Shinko Fuaudoraa Kk | Reaction apparatus |
| IT1255737B (it) * | 1992-05-19 | 1995-11-15 | Reattore multitubolare a film cadente | |
| US5587500A (en) * | 1993-09-17 | 1996-12-24 | The Chemithon Corporation | Sulfonation of fatty acid esters |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3328460A (en) * | 1964-02-04 | 1967-06-27 | Allied Chem | Process for sulfonation of organic compounds |
| JPS5118934B2 (en, 2012) * | 1971-09-18 | 1976-06-14 | ||
| JPS5218682B2 (en, 2012) * | 1972-04-15 | 1977-05-24 |
-
1975
- 1975-06-30 JP JP50080645A patent/JPS525712A/ja active Granted
-
1976
- 1976-06-25 US US05/699,712 patent/US4036596A/en not_active Expired - Lifetime
- 1976-06-28 DE DE2629009A patent/DE2629009C2/de not_active Expired
- 1976-06-29 GB GB27111/76A patent/GB1505956A/en not_active Expired
- 1976-07-28 AU AU16316/76A patent/AU502019B2/en not_active Expired
- 1976-12-28 SU SU762435651A patent/SU1072792A3/ru active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7258680B2 (en) | 2002-09-02 | 2007-08-21 | Unomedical A/S | Device for subcutaneous administration of a medicament to a patient |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS525712A (en) | 1977-01-17 |
| US4036596A (en) | 1977-07-19 |
| AU1631676A (en) | 1978-02-02 |
| DE2629009A1 (de) | 1977-05-05 |
| GB1505956A (en) | 1978-04-05 |
| AU502019B2 (en) | 1979-07-12 |
| JPS577631B2 (en, 2012) | 1982-02-12 |
| SU1072792A3 (ru) | 1984-02-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8125 | Change of the main classification |
Ipc: C07B 13/06 |
|
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition |