DE2557456C2 - Verfahren zur Herstellung von Aminoxiden - Google Patents
Verfahren zur Herstellung von AminoxidenInfo
- Publication number
- DE2557456C2 DE2557456C2 DE19752557456 DE2557456A DE2557456C2 DE 2557456 C2 DE2557456 C2 DE 2557456C2 DE 19752557456 DE19752557456 DE 19752557456 DE 2557456 A DE2557456 A DE 2557456A DE 2557456 C2 DE2557456 C2 DE 2557456C2
- Authority
- DE
- Germany
- Prior art keywords
- water
- weight
- amine
- concentration
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000001412 amines Chemical class 0.000 title claims description 29
- 238000000034 method Methods 0.000 title claims description 9
- 238000002360 preparation method Methods 0.000 title claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- 239000000203 mixture Substances 0.000 claims description 15
- 125000000217 alkyl group Chemical group 0.000 claims description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- 125000004432 carbon atom Chemical group C* 0.000 claims description 5
- 230000003647 oxidation Effects 0.000 claims description 5
- 238000007254 oxidation reaction Methods 0.000 claims description 5
- 239000003054 catalyst Substances 0.000 claims description 2
- 125000005429 oxyalkyl group Chemical group 0.000 claims description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 24
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 15
- 239000000047 product Substances 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 239000007864 aqueous solution Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 5
- 150000003512 tertiary amines Chemical class 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 3
- 150000002978 peroxides Chemical class 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- YNJSNEKCXVFDKW-UHFFFAOYSA-N 3-(5-amino-1h-indol-3-yl)-2-azaniumylpropanoate Chemical compound C1=C(N)C=C2C(CC(N)C(O)=O)=CNC2=C1 YNJSNEKCXVFDKW-UHFFFAOYSA-N 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- IENXJNLJEDMNTE-UHFFFAOYSA-N acetic acid;ethane-1,2-diamine Chemical compound CC(O)=O.NCCN IENXJNLJEDMNTE-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000003421 catalytic decomposition reaction Methods 0.000 description 1
- 241001233037 catfish Species 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- VFFDVELHRCMPLY-UHFFFAOYSA-N dimethyldodecyl amine Natural products CC(C)CCCCCCCCCCCN VFFDVELHRCMPLY-UHFFFAOYSA-N 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- XONPDZSGENTBNJ-UHFFFAOYSA-N molecular hydrogen;sodium Chemical compound [Na].[H][H] XONPDZSGENTBNJ-UHFFFAOYSA-N 0.000 description 1
- YWFWDNVOPHGWMX-UHFFFAOYSA-N n,n-dimethyldodecan-1-amine Chemical compound CCCCCCCCCCCCN(C)C YWFWDNVOPHGWMX-UHFFFAOYSA-N 0.000 description 1
- 231100000989 no adverse effect Toxicity 0.000 description 1
- 125000005702 oxyalkylene group Chemical group 0.000 description 1
- 238000005502 peroxidation Methods 0.000 description 1
- 125000000864 peroxy group Chemical group O(O*)* 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000009666 routine test Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000012258 stirred mixture Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C291/00—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00
- C07C291/02—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00 containing nitrogen-oxide bonds
- C07C291/04—Compounds containing carbon and nitrogen and having functional groups not covered by groups C07C201/00 - C07C281/00 containing nitrogen-oxide bonds containing amino-oxide bonds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB5500774A GB1538199A (en) | 1974-12-19 | 1974-12-19 | Preparation of amine oxides |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2557456A1 DE2557456A1 (de) | 1976-06-24 |
| DE2557456C2 true DE2557456C2 (de) | 1985-08-01 |
Family
ID=10472694
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19752557456 Expired DE2557456C2 (de) | 1974-12-19 | 1975-12-19 | Verfahren zur Herstellung von Aminoxiden |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE2557456C2 (show.php) |
| FR (1) | FR2295021A1 (show.php) |
| GB (1) | GB1538199A (show.php) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3613944C1 (de) * | 1986-04-24 | 1987-08-13 | Goldschmidt Ag Th | Verfahren zur Herstellung einer hochkonzentrierten,fliess- und pumpfaehigen Betainloesung |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5528968A (en) * | 1978-08-24 | 1980-02-29 | Nissan Chem Ind Ltd | Production of amine oxide |
| DE3218026C2 (de) * | 1982-05-13 | 1984-03-29 | A. Nattermann & Cie GmbH, 5000 Köln | Verfahren zur Herstellung von 3-(10,11-Dihydro-5H-dibenzo[a,d]-cyclohepten-5-yliden)-N,N-dimethyl-1-propanamin-N-oxid- Dihydrat |
| US4970340A (en) * | 1985-07-01 | 1990-11-13 | Ethyl Corporation | Amine oxide process and composition |
| DE3545152A1 (de) * | 1985-12-19 | 1987-06-25 | Hoechst Ag | Verfahren zur herestellung von fluessigen, hochkonzentrierten aminoxiden und diese enthaltende faserpraeparationsmittel |
| EP3339288A1 (de) | 2016-12-23 | 2018-06-27 | Aurotec GmbH | Herstellung eines aminoxids durch oxidation eines tertiären amins |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE937058C (de) * | 1952-11-04 | 1955-12-29 | Basf Ag | Verfahren zur Herstellung von niedrigmolekularen Trialkylaminoxyden und deren Hydraten |
| US3215741A (en) * | 1963-01-08 | 1965-11-02 | Du Pont | Process for preparing maine oxides |
| US3283007A (en) * | 1963-06-28 | 1966-11-01 | Du Pont | Production of amine oxides |
| FR1418653A (fr) * | 1963-12-24 | 1965-11-19 | Armour Hess Chem Ltd | Oxydes d'amines et leur procédé de préparation |
| US3336387A (en) * | 1964-02-28 | 1967-08-15 | Shell Oil Co | Tertiary amine oxides |
| DE1518104B1 (de) * | 1965-05-21 | 1970-05-14 | Pennsalt Chemicals Corp | Verfahren zur Herstellung von tertiaeren Aminoxyden |
| US3494924A (en) * | 1966-09-30 | 1970-02-10 | Atlantic Richfield Co | Preparation of tertiary amine oxides |
-
1974
- 1974-12-19 GB GB5500774A patent/GB1538199A/en not_active Expired
-
1975
- 1975-12-19 FR FR7539192A patent/FR2295021A1/fr active Granted
- 1975-12-19 DE DE19752557456 patent/DE2557456C2/de not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3613944C1 (de) * | 1986-04-24 | 1987-08-13 | Goldschmidt Ag Th | Verfahren zur Herstellung einer hochkonzentrierten,fliess- und pumpfaehigen Betainloesung |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2557456A1 (de) | 1976-06-24 |
| FR2295021A1 (fr) | 1976-07-16 |
| GB1538199A (en) | 1979-01-10 |
| FR2295021B1 (show.php) | 1978-12-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8128 | New person/name/address of the agent |
Representative=s name: BERENDT, T., DIPL.-CHEM. DR., PAT.-ANW., 8000 MUEN |
|
| 8110 | Request for examination paragraph 44 | ||
| D2 | Grant after examination | ||
| 8363 | Opposition against the patent | ||
| 8330 | Complete disclaimer |