DE2447133A1 - Photochemisches verfahren zur herstellung von kohlenwasserstoffaddukten - Google Patents
Photochemisches verfahren zur herstellung von kohlenwasserstoffadduktenInfo
- Publication number
- DE2447133A1 DE2447133A1 DE19742447133 DE2447133A DE2447133A1 DE 2447133 A1 DE2447133 A1 DE 2447133A1 DE 19742447133 DE19742447133 DE 19742447133 DE 2447133 A DE2447133 A DE 2447133A DE 2447133 A1 DE2447133 A1 DE 2447133A1
- Authority
- DE
- Germany
- Prior art keywords
- reactor
- liquid phase
- phase
- production
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 21
- 238000004519 manufacturing process Methods 0.000 title claims description 9
- 229930195733 hydrocarbon Natural products 0.000 title claims description 8
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 8
- 239000004215 Carbon black (E152) Substances 0.000 title claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 30
- 239000000460 chlorine Substances 0.000 claims description 19
- 239000007791 liquid phase Substances 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 11
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 10
- 239000003153 chemical reaction reagent Substances 0.000 claims description 8
- LLCOIQRNSJBFSN-UHFFFAOYSA-N methane;sulfurochloridic acid Chemical compound C.OS(Cl)(=O)=O LLCOIQRNSJBFSN-UHFFFAOYSA-N 0.000 claims description 8
- 239000000376 reactant Substances 0.000 claims description 8
- 239000012071 phase Substances 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 6
- 239000007795 chemical reaction product Substances 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Inorganic materials O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 claims 1
- 239000007789 gas Substances 0.000 description 10
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 7
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 5
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 150000001336 alkenes Chemical class 0.000 description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical class S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 238000010672 photosynthesis Methods 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- -1 sulfur anhydride Chemical class 0.000 description 2
- XTHPWXDJESJLNJ-UHFFFAOYSA-N sulfurochloridic acid Chemical class OS(Cl)(=O)=O XTHPWXDJESJLNJ-UHFFFAOYSA-N 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- OGDBYKXYIXUNQT-UHFFFAOYSA-N butane;sulfurochloridic acid Chemical class CCCC.OS(Cl)(=O)=O OGDBYKXYIXUNQT-UHFFFAOYSA-N 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- OSVXSBDYLRYLIG-UHFFFAOYSA-N chlorine dioxide Inorganic materials O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 description 1
- 235000019398 chlorine dioxide Nutrition 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000008246 gaseous mixture Substances 0.000 description 1
- 150000002334 glycols Chemical class 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 230000031700 light absorption Effects 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 238000006303 photolysis reaction Methods 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 230000015843 photosynthesis, light reaction Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/12—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
- B01J19/122—Incoherent waves
- B01J19/123—Ultraviolet light
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B45/00—Formation or introduction of functional groups containing sulfur
- C07B45/06—Formation or introduction of functional groups containing sulfur of mercapto or sulfide groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
- C07C17/04—Preparation of halogenated hydrocarbons by addition of halogens to unsaturated halogenated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7335526A FR2246520B1 (https=) | 1973-10-04 | 1973-10-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2447133A1 true DE2447133A1 (de) | 1975-04-10 |
Family
ID=9125925
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19742447133 Pending DE2447133A1 (de) | 1973-10-04 | 1974-10-02 | Photochemisches verfahren zur herstellung von kohlenwasserstoffaddukten |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE820662A (https=) |
| DE (1) | DE2447133A1 (https=) |
| FR (1) | FR2246520B1 (https=) |
| GB (1) | GB1457065A (https=) |
| NL (1) | NL7413157A (https=) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113636990A (zh) * | 2021-06-22 | 2021-11-12 | 山东盛安贝新能源有限公司 | 一种二醋洛尔中间体5-乙酰胺基-2-(2，3-环氧丙氧基)苯乙酮的方法 |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61158956A (ja) * | 1984-12-29 | 1986-07-18 | Toyo Kasei Kogyo Kk | 塩化メタンスルホニルの製造方法 |
| FR2595095B2 (fr) * | 1986-03-03 | 1988-05-27 | Elf Aquitaine | Procede et appareil pour la sulfochloration photochimique d'alcanes gazeux |
| DE3666949D1 (en) * | 1985-03-14 | 1989-12-21 | Elf Aquitaine | Process and apparatus for the photochemical sulfochlorination of gaseous alkanes |
| FR2578841B1 (fr) * | 1985-03-14 | 1987-05-29 | Elf Aquitaine | Procede et appareil pour la sulfochloration photochimique d'alcanes gazeux |
| FR2777565B1 (fr) * | 1998-04-21 | 2000-05-19 | Atochem Elf Sa | Procede de sulfochloration photochimique d'alcanes gazeux |
| US7311884B2 (en) * | 2003-12-08 | 2007-12-25 | Jts Enterprises, Inc. | Continuous chlorine dioxide generation |
| US20120116121A1 (en) * | 2009-07-30 | 2012-05-10 | Dow Global Technologies Llc | Process for the sulfochlorination of hydrocarbons |
-
1973
- 1973-10-04 FR FR7335526A patent/FR2246520B1/fr not_active Expired
-
1974
- 1974-10-02 DE DE19742447133 patent/DE2447133A1/de active Pending
- 1974-10-03 BE BE149175A patent/BE820662A/xx unknown
- 1974-10-04 NL NL7413157A patent/NL7413157A/xx not_active Application Discontinuation
- 1974-10-04 GB GB4318774A patent/GB1457065A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113636990A (zh) * | 2021-06-22 | 2021-11-12 | 山东盛安贝新能源有限公司 | 一种二醋洛尔中间体5-乙酰胺基-2-(2，3-环氧丙氧基)苯乙酮的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| NL7413157A (nl) | 1975-04-08 |
| FR2246520B1 (https=) | 1976-06-18 |
| GB1457065A (en) | 1976-12-01 |
| FR2246520A1 (https=) | 1975-05-02 |
| BE820662A (fr) | 1975-02-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OHJ | Non-payment of the annual fee |