DE2412118A1 - Verfahren zur isolierung einer proteinfraktion - Google Patents
Verfahren zur isolierung einer proteinfraktionInfo
- Publication number
- DE2412118A1 DE2412118A1 DE2412118A DE2412118A DE2412118A1 DE 2412118 A1 DE2412118 A1 DE 2412118A1 DE 2412118 A DE2412118 A DE 2412118A DE 2412118 A DE2412118 A DE 2412118A DE 2412118 A1 DE2412118 A1 DE 2412118A1
- Authority
- DE
- Germany
- Prior art keywords
- milk
- retentate
- ultrafiltration
- diluted
- protein
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000108 ultra-filtration Methods 0.000 title claims abstract description 39
- 238000010790 dilution Methods 0.000 title abstract description 11
- 239000012895 dilution Substances 0.000 title abstract description 11
- 238000002955 isolation Methods 0.000 title description 3
- 102000004169 proteins and genes Human genes 0.000 claims abstract description 69
- 108090000623 proteins and genes Proteins 0.000 claims abstract description 69
- 235000013336 milk Nutrition 0.000 claims abstract description 42
- 239000008267 milk Substances 0.000 claims abstract description 42
- 210000004080 milk Anatomy 0.000 claims abstract description 42
- 238000000034 method Methods 0.000 claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- 239000000126 substance Substances 0.000 claims abstract description 18
- 239000000725 suspension Substances 0.000 claims abstract description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 3
- 239000012465 retentate Substances 0.000 claims description 29
- 239000007864 aqueous solution Substances 0.000 claims description 18
- 235000020183 skimmed milk Nutrition 0.000 claims description 17
- 239000000203 mixture Substances 0.000 claims description 14
- 239000007900 aqueous suspension Substances 0.000 claims description 12
- 239000007787 solid Substances 0.000 claims description 12
- 235000015155 buttermilk Nutrition 0.000 claims description 7
- 238000011282 treatment Methods 0.000 claims description 7
- 239000012466 permeate Substances 0.000 claims description 5
- 235000020167 acidified milk Nutrition 0.000 claims description 3
- 239000003925 fat Substances 0.000 claims description 3
- 239000008346 aqueous phase Substances 0.000 claims description 2
- 235000018102 proteins Nutrition 0.000 abstract description 66
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 abstract description 15
- 239000008101 lactose Substances 0.000 abstract description 15
- 239000005018 casein Substances 0.000 abstract description 12
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 abstract description 12
- 235000021240 caseins Nutrition 0.000 abstract description 12
- 229910052791 calcium Inorganic materials 0.000 abstract description 9
- 230000008569 process Effects 0.000 abstract description 9
- 235000013351 cheese Nutrition 0.000 abstract description 8
- 102000004407 Lactalbumin Human genes 0.000 abstract description 7
- 108090000942 Lactalbumin Proteins 0.000 abstract description 7
- 229910052708 sodium Inorganic materials 0.000 abstract description 7
- 239000005862 Whey Substances 0.000 abstract description 2
- 102000007544 Whey Proteins Human genes 0.000 abstract description 2
- 108010046377 Whey Proteins Proteins 0.000 abstract description 2
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- 235000013861 fat-free Nutrition 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 15
- 239000012528 membrane Substances 0.000 description 14
- 238000000926 separation method Methods 0.000 description 11
- 102000011632 Caseins Human genes 0.000 description 10
- 108010076119 Caseins Proteins 0.000 description 10
- 239000000243 solution Substances 0.000 description 9
- 239000011575 calcium Substances 0.000 description 8
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 7
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 6
- 239000011734 sodium Substances 0.000 description 6
- 230000008859 change Effects 0.000 description 5
- 235000013305 food Nutrition 0.000 description 4
- 230000020477 pH reduction Effects 0.000 description 4
- 238000011084 recovery Methods 0.000 description 4
- 229940108461 rennet Drugs 0.000 description 4
- 108010058314 rennet Proteins 0.000 description 4
- 239000012141 concentrate Substances 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 238000000265 homogenisation Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 102000014171 Milk Proteins Human genes 0.000 description 2
- 108010011756 Milk Proteins Proteins 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 235000005911 diet Nutrition 0.000 description 2
- 238000007865 diluting Methods 0.000 description 2
- 238000004108 freeze drying Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 235000021239 milk protein Nutrition 0.000 description 2
- 239000002808 molecular sieve Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 235000020200 pasteurised milk Nutrition 0.000 description 2
- 238000009928 pasteurization Methods 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 230000010287 polarization Effects 0.000 description 2
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 2
- 238000007738 vacuum evaporation Methods 0.000 description 2
- 101800000263 Acidic protein Proteins 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000124008 Mammalia Species 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001669 calcium Chemical class 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000010909 chemical acidification Methods 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 210000003022 colostrum Anatomy 0.000 description 1
- 235000021277 colostrum Nutrition 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 235000021185 dessert Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 230000000378 dietary effect Effects 0.000 description 1
- 230000001516 effect on protein Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 235000020243 first infant milk formula Nutrition 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000002864 food coloring agent Nutrition 0.000 description 1
- 235000020256 human milk Nutrition 0.000 description 1
- 210000004251 human milk Anatomy 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000037361 pathway Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- 229940080237 sodium caseinate Drugs 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 239000008371 vanilla flavor Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 235000008939 whole milk Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/20—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from milk, e.g. casein; from whey
- A23J1/205—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from milk, e.g. casein; from whey from whey, e.g. lactalbumine
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
- A23C19/00—Cheese; Cheese preparations; Making thereof
- A23C19/02—Making cheese curd
- A23C19/028—Making cheese curd without substantial whey separation from coagulated milk
- A23C19/0285—Making cheese curd without substantial whey separation from coagulated milk by dialysis or ultrafiltration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/14—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment
- A23C9/142—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment by dialysis, reverse osmosis or ultrafiltration
- A23C9/1422—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment by dialysis, reverse osmosis or ultrafiltration by ultrafiltration, microfiltration or diafiltration of milk, e.g. for separating protein and lactose; Treatment of the UF permeate
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Biochemistry (AREA)
- Water Supply & Treatment (AREA)
- Dairy Products (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1111773A CH571317A5 (enExample) | 1973-07-31 | 1973-07-31 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2412118A1 true DE2412118A1 (de) | 1975-03-27 |
Family
ID=4370249
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2412118A Pending DE2412118A1 (de) | 1973-07-31 | 1974-03-13 | Verfahren zur isolierung einer proteinfraktion |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE817248A (enExample) |
| CH (1) | CH571317A5 (enExample) |
| DE (1) | DE2412118A1 (enExample) |
| SU (1) | SU697037A3 (enExample) |
| ZA (1) | ZA744679B (enExample) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0113447A3 (en) * | 1982-12-09 | 1985-04-10 | Schott Glaswerke | Process for the fractional separation of protein mixtures with membranes |
| CN112088941A (zh) * | 2019-06-17 | 2020-12-18 | 内蒙古蒙牛乳业（集团）股份有限公司 | 一种脱乳糖的乳制品及其制备方法 |
| CN112088942A (zh) * | 2019-06-17 | 2020-12-18 | 内蒙古蒙牛乳业（集团）股份有限公司 | 一种添加藜麦颗粒的脱乳糖乳制品及其制备方法 |
-
1973
- 1973-07-31 CH CH1111773A patent/CH571317A5/xx not_active IP Right Cessation
-
1974
- 1974-03-13 DE DE2412118A patent/DE2412118A1/de active Pending
- 1974-07-04 BE BE146214A patent/BE817248A/xx not_active IP Right Cessation
- 1974-07-22 ZA ZA00744679A patent/ZA744679B/xx unknown
- 1974-07-30 SU SU742052413A patent/SU697037A3/ru active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0113447A3 (en) * | 1982-12-09 | 1985-04-10 | Schott Glaswerke | Process for the fractional separation of protein mixtures with membranes |
| CN112088941A (zh) * | 2019-06-17 | 2020-12-18 | 内蒙古蒙牛乳业（集团）股份有限公司 | 一种脱乳糖的乳制品及其制备方法 |
| CN112088942A (zh) * | 2019-06-17 | 2020-12-18 | 内蒙古蒙牛乳业（集团）股份有限公司 | 一种添加藜麦颗粒的脱乳糖乳制品及其制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| CH571317A5 (enExample) | 1976-01-15 |
| ZA744679B (en) | 1975-08-27 |
| BE817248A (fr) | 1975-01-06 |
| SU697037A3 (ru) | 1979-11-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OI | Miscellaneous see part 1 | ||
| OHN | Withdrawal |