DE2247497A1 - Verfahren zur gewinnung von kupfer, nickel, kobalt und molybdaen aus tiefseemanganknollen - Google Patents
Verfahren zur gewinnung von kupfer, nickel, kobalt und molybdaen aus tiefseemanganknollenInfo
- Publication number
- DE2247497A1 DE2247497A1 DE19722247497 DE2247497A DE2247497A1 DE 2247497 A1 DE2247497 A1 DE 2247497A1 DE 19722247497 DE19722247497 DE 19722247497 DE 2247497 A DE2247497 A DE 2247497A DE 2247497 A1 DE2247497 A1 DE 2247497A1
- Authority
- DE
- Germany
- Prior art keywords
- pellets
- tubers
- nickel
- copper
- cobalt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 44
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims description 40
- 229910052759 nickel Inorganic materials 0.000 title claims description 19
- 238000000605 extraction Methods 0.000 title claims description 18
- 239000010941 cobalt Substances 0.000 title claims description 17
- 229910017052 cobalt Inorganic materials 0.000 title claims description 17
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 title claims description 17
- 239000008188 pellet Substances 0.000 claims description 105
- 239000002245 particle Substances 0.000 claims description 31
- 239000010949 copper Substances 0.000 claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 18
- 229910052802 copper Inorganic materials 0.000 claims description 18
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 16
- 229910052748 manganese Inorganic materials 0.000 claims description 16
- 239000011572 manganese Substances 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 14
- 239000003638 chemical reducing agent Substances 0.000 claims description 14
- 238000000227 grinding Methods 0.000 claims description 11
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 9
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 9
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 9
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 8
- 229910052750 molybdenum Inorganic materials 0.000 claims description 8
- 239000011733 molybdenum Substances 0.000 claims description 8
- 239000007789 gas Substances 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 6
- 238000005054 agglomeration Methods 0.000 claims description 5
- 230000002776 aggregation Effects 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 5
- 239000003245 coal Substances 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 150000003863 ammonium salts Chemical class 0.000 claims description 4
- 239000003575 carbonaceous material Substances 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 239000002802 bituminous coal Substances 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000000571 coke Substances 0.000 claims description 3
- WHDPTDWLEKQKKX-UHFFFAOYSA-N cobalt molybdenum Chemical compound [Co].[Co].[Mo] WHDPTDWLEKQKKX-UHFFFAOYSA-N 0.000 claims description 2
- 239000003077 lignite Substances 0.000 claims description 2
- 235000013379 molasses Nutrition 0.000 claims description 2
- 239000010779 crude oil Substances 0.000 claims 2
- RHZUVFJBSILHOK-UHFFFAOYSA-N anthracen-1-ylmethanolate Chemical compound C1=CC=C2C=C3C(C[O-])=CC=CC3=CC2=C1 RHZUVFJBSILHOK-UHFFFAOYSA-N 0.000 claims 1
- 239000003830 anthracite Substances 0.000 claims 1
- XXLDWSKFRBJLMX-UHFFFAOYSA-N carbon dioxide;carbon monoxide Chemical compound O=[C].O=C=O XXLDWSKFRBJLMX-UHFFFAOYSA-N 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 238000003801 milling Methods 0.000 claims 1
- 238000003786 synthesis reaction Methods 0.000 claims 1
- 238000002386 leaching Methods 0.000 description 13
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 8
- 239000001099 ammonium carbonate Substances 0.000 description 8
- 235000012501 ammonium carbonate Nutrition 0.000 description 8
- 239000000295 fuel oil Substances 0.000 description 8
- 239000012299 nitrogen atmosphere Substances 0.000 description 8
- 239000011324 bead Substances 0.000 description 7
- 238000005453 pelletization Methods 0.000 description 6
- 239000012298 atmosphere Substances 0.000 description 5
- 238000001035 drying Methods 0.000 description 5
- 238000010626 work up procedure Methods 0.000 description 5
- 239000011521 glass Substances 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 3
- 239000000440 bentonite Substances 0.000 description 3
- 229910000278 bentonite Inorganic materials 0.000 description 3
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 3
- 210000004907 gland Anatomy 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000000920 calcium hydroxide Substances 0.000 description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 239000003208 petroleum Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 1
- 150000001341 alkaline earth metal compounds Chemical class 0.000 description 1
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 description 1
- 229910000287 alkaline earth metal oxide Inorganic materials 0.000 description 1
- 229910052586 apatite Inorganic materials 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 229910052626 biotite Inorganic materials 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 235000015115 caffè latte Nutrition 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000002734 clay mineral Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 239000010433 feldspar Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 230000009969 flowable effect Effects 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000002667 nucleating agent Substances 0.000 description 1
- 239000010747 number 6 fuel oil Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- VSIIXMUUUJUKCM-UHFFFAOYSA-D pentacalcium;fluoride;triphosphate Chemical compound [F-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O VSIIXMUUUJUKCM-UHFFFAOYSA-D 0.000 description 1
- 230000002688 persistence Effects 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000010405 reoxidation reaction Methods 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 239000003039 volatile agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B47/00—Obtaining manganese
- C22B47/0018—Treating ocean floor nodules
- C22B47/0027—Preliminary treatment
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B5/00—General methods of reducing to metals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/04—Manganese marine modules
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Ocean & Marine Engineering (AREA)
- Oceanography (AREA)
- Environmental & Geological Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US18439771A | 1971-09-28 | 1971-09-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2247497A1 true DE2247497A1 (de) | 1973-04-05 |
Family
ID=22676710
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19722247497 Withdrawn DE2247497A1 (de) | 1971-09-28 | 1972-09-28 | Verfahren zur gewinnung von kupfer, nickel, kobalt und molybdaen aus tiefseemanganknollen |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3788841A (en:Method) |
| JP (1) | JPS5516219B2 (en:Method) |
| CA (1) | CA980130A (en:Method) |
| DE (1) | DE2247497A1 (en:Method) |
| FR (1) | FR2154672B1 (en:Method) |
| GB (1) | GB1403230A (en:Method) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109295305A (zh) * | 2018-12-01 | 2019-02-01 | 湖南科技大学 | 褐煤还原浸取软锰矿后的褐煤回收利用方法 |
| CN112813260A (zh) * | 2020-12-28 | 2021-05-18 | 广东佳纳能源科技有限公司 | 一种还原浸出方法 |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3869360A (en) * | 1972-05-08 | 1975-03-04 | William S Kane | Reduction method for separating metal values from ocean floor nodule ore |
| US3984232A (en) * | 1973-08-22 | 1976-10-05 | The International Nickel Company, Inc. | Thermal upgrading of sea nodules |
| US3957485A (en) * | 1974-10-15 | 1976-05-18 | Kennecott Copper Corporation | Reduction smelting of manganese nodules with a liquid reductant |
| US3942974A (en) * | 1975-02-10 | 1976-03-09 | Kennecott Copper Corporation | Manganese nodule pelletizing |
| US4138249A (en) * | 1978-05-26 | 1979-02-06 | Cabot Corporation | Process for recovering valuable metals from superalloy scrap |
| US4501721A (en) * | 1983-06-10 | 1985-02-26 | Kamyr, Inc. | Leaching and washing a flocculated slurry having a fiber content |
| US4557905A (en) * | 1983-06-10 | 1985-12-10 | Kamyr, Inc. | Leaching and washing a flocculated slurry having a fiber content |
| JPS6032273U (ja) * | 1983-08-08 | 1985-03-05 | 大阪化学合金株式会社 | 水溶性包装体 |
| FR2612173B1 (fr) * | 1987-03-10 | 1991-04-19 | Japan Metals & Chem Co Ltd | Procede de preparation de composes de manganese de haute purete |
| TW461920B (en) * | 1998-09-25 | 2001-11-01 | Mitsubishi Heavy Ind Ltd | Method of producing reduced iron and production facilities therefor |
| JP4875442B2 (ja) * | 2006-09-12 | 2012-02-15 | 株式会社ニッキ | エンジンのガス燃料供給装置 |
| CN102643998B (zh) * | 2012-04-28 | 2013-07-17 | 中南大学 | 一种处理辉钼矿的方法 |
| CN102776357A (zh) * | 2012-06-28 | 2012-11-14 | 东北大学 | 一种微波-氨浸处理红土镍矿的方法 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3471285A (en) * | 1967-03-27 | 1969-10-07 | Dow Chemical Co | Process for the selective recovery of manganese and iron from ores |
-
1971
- 1971-09-28 US US00184397A patent/US3788841A/en not_active Expired - Lifetime
-
1972
- 1972-09-19 CA CA152,075A patent/CA980130A/en not_active Expired
- 1972-09-26 GB GB4445072A patent/GB1403230A/en not_active Expired
- 1972-09-27 JP JP9627872A patent/JPS5516219B2/ja not_active Expired
- 1972-09-28 FR FR7234315A patent/FR2154672B1/fr not_active Expired
- 1972-09-28 DE DE19722247497 patent/DE2247497A1/de not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109295305A (zh) * | 2018-12-01 | 2019-02-01 | 湖南科技大学 | 褐煤还原浸取软锰矿后的褐煤回收利用方法 |
| CN112813260A (zh) * | 2020-12-28 | 2021-05-18 | 广东佳纳能源科技有限公司 | 一种还原浸出方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS4841912A (en:Method) | 1973-06-19 |
| JPS5516219B2 (en:Method) | 1980-04-30 |
| US3788841A (en) | 1974-01-29 |
| FR2154672B1 (en:Method) | 1977-08-26 |
| AU4687872A (en) | 1974-03-28 |
| GB1403230A (en) | 1975-08-28 |
| CA980130A (en) | 1975-12-23 |
| FR2154672A1 (en:Method) | 1973-05-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| 8130 | Withdrawal |