DE2244780B2 - - Google Patents
Info
- Publication number
- DE2244780B2 DE2244780B2 DE2244780A DE2244780A DE2244780B2 DE 2244780 B2 DE2244780 B2 DE 2244780B2 DE 2244780 A DE2244780 A DE 2244780A DE 2244780 A DE2244780 A DE 2244780A DE 2244780 B2 DE2244780 B2 DE 2244780B2
- Authority
- DE
- Germany
- Prior art keywords
- phase
- outlet
- stream
- separation
- organic phase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000012071 phase Substances 0.000 claims description 38
- 239000008346 aqueous phase Substances 0.000 claims description 28
- 239000012074 organic phase Substances 0.000 claims description 27
- 238000005191 phase separation Methods 0.000 claims description 25
- 238000000926 separation method Methods 0.000 claims description 16
- 239000012530 fluid Substances 0.000 claims description 6
- BQJCRHHNABKAKU-KBQPJGBKSA-N morphine Chemical compound O([C@H]1[C@H](C=C[C@H]23)O)C4=C5[C@@]12CCN(C)[C@@H]3CC5=CC=C4O BQJCRHHNABKAKU-KBQPJGBKSA-N 0.000 description 20
- 210000002700 urine Anatomy 0.000 description 11
- 229960005181 morphine Drugs 0.000 description 10
- 239000007788 liquid Substances 0.000 description 8
- 239000007791 liquid phase Substances 0.000 description 8
- 239000002904 solvent Substances 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000004458 analytical method Methods 0.000 description 5
- 238000000605 extraction Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 238000011109 contamination Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 230000005484 gravity Effects 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000007853 buffer solution Substances 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 239000005871 repellent Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 229940079593 drug Drugs 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- -1 polytetrafluoroethylene Polymers 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 239000011877 solvent mixture Substances 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- FOJYFDFNGPRXDR-SQILNHJXSA-N (4r,4ar,7s,7ar,12bs)-10-[(4r,4ar,7s,7ar,12bs)-7,9-dihydroxy-3-methyl-2,4,4a,7,7a,13-hexahydro-1h-4,12-methanobenzofuro[3,2-e]isoquinoline-10-yl]-3-methyl-2,4,4a,7,7a,13-hexahydro-1h-4,12-methanobenzofuro[3,2-e]isoquinoline-7,9-diol Chemical compound C([C@H]12)=C[C@H](O)[C@@H]3OC4=C(O)C(C=5C=C6C7=C(C=5O)O[C@@H]5[C@]77CCN([C@H](C6)[C@@H]7C=C[C@@H]5O)C)=CC5=C4[C@]13CCN(C)[C@@H]2C5 FOJYFDFNGPRXDR-SQILNHJXSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- FOJYFDFNGPRXDR-UHFFFAOYSA-N Pseudomorphine Natural products C12C=CC(O)C3OC4=C(O)C(C=5C=C6C7=C(C=5O)OC5C77CCN(C(C6)C7C=CC5O)C)=CC5=C4C23CCN(C)C1C5 FOJYFDFNGPRXDR-UHFFFAOYSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 238000005206 flow analysis Methods 0.000 description 1
- 239000007792 gaseous phase Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 239000012454 non-polar solvent Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000009331 sowing Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/08—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor using a stream of discrete samples flowing along a tube system, e.g. flow injection analysis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/04—Breaking emulsions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/04—Breaking emulsions
- B01D17/045—Breaking emulsions with coalescers
Landscapes
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Thermal Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Automatic Analysis And Handling Materials Therefor (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Degasification And Air Bubble Elimination (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US18883071A | 1971-10-13 | 1971-10-13 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2244780A1 DE2244780A1 (de) | 1973-04-26 |
| DE2244780B2 true DE2244780B2 (enrdf_load_stackoverflow) | 1975-05-07 |
| DE2244780C3 DE2244780C3 (enrdf_load_stackoverflow) | 1975-12-18 |
Family
ID=22694708
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2244780A Granted DE2244780A1 (de) | 1971-10-13 | 1972-09-13 | Vorrichtung zur trennung der phasen eines kontinuierlich stroemenden, mehrphasigen fluidstroms |
Country Status (11)
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4002269A (en) * | 1974-08-16 | 1977-01-11 | Technicon Instruments Corporation | Liquid proportioning system in a liquid sample analyzer |
| BE850201A (fr) | 1976-03-23 | 1977-07-07 | Novais Paiva Manuel P De | Procede de separation de substances de masses differentes |
| US4028056A (en) * | 1976-04-20 | 1977-06-07 | Technicon Instruments Corporation | Substance separation technique |
| US4418039A (en) * | 1976-12-27 | 1983-11-29 | Technicon Instruments Corporation | Solute transfer technique |
| SE414872B (sv) * | 1977-10-03 | 1980-08-25 | Bifok Ab | Forfarande och anordning vid flodesinjektionsextraktion |
| JPS6029B2 (ja) * | 1978-09-06 | 1985-01-05 | 藤沢薬品工業株式会社 | 固定化酵素カラム |
| DE2967343D1 (en) * | 1978-09-06 | 1985-02-14 | Fujisawa Pharmaceutical Co | Immobilized enzyme column |
| US5149658A (en) * | 1987-07-14 | 1992-09-22 | Technicon Instruments Corporation | Method for the separation and/or formation of immiscible liquid streams |
| US5045473A (en) * | 1987-07-14 | 1991-09-03 | Technicon Instruments Corporation | Apparatus and method for the separation and/or formation of immicible liquid streams |
| US4816226A (en) * | 1987-12-30 | 1989-03-28 | Shell Oil Company | Apparatus for continuous flow injection solvent extraction analysis |
| EP1032471B1 (de) * | 1997-11-19 | 2002-04-24 | Biognosis GmbH | Vorrichtung zur sequentiellen ausgabe von fliessfähigen reagenzien |
| US6613579B2 (en) * | 2001-02-02 | 2003-09-02 | Global Fia, Inc. | Sequential injection liquid-liquid extraction |
| WO2004067182A2 (ja) * | 2003-01-31 | 2004-08-12 | Sumitomo Chemical Company, Limited | エマルションの分級装置および分級方法、エマルションの解乳化方法 |
| US9477233B2 (en) * | 2004-07-02 | 2016-10-25 | The University Of Chicago | Microfluidic system with a plurality of sequential T-junctions for performing reactions in microdroplets |
| EP2660482B1 (en) | 2005-08-22 | 2019-08-07 | Life Technologies Corporation | Vorrichtung, System und Verfahren unter Verwendung von nichtmischbaren Flüssigkeiten mit unterschiedlichen Volumen |
| US9152150B1 (en) * | 2007-02-22 | 2015-10-06 | Applied Biosystems, Llc | Compositions, systems, and methods for immiscible fluid discrete volume manipulation |
| CN101566533B (zh) * | 2009-06-05 | 2011-05-11 | 中国原子能科学研究院 | 油-水两相中油相取样方法 |
| US10639631B2 (en) * | 2015-02-13 | 2020-05-05 | International Business Machines Corporation | Microfluidic probe head for processing a sequence of liquid volumes separated by spacers |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2214248A (en) * | 1935-05-24 | 1940-09-10 | Hawley Virginia Taylor | Emulsion breaker |
| US2968308A (en) * | 1957-03-28 | 1961-01-17 | Phillips Petroleum Co | Continuous analysis of process streams |
| US2903342A (en) * | 1958-04-01 | 1959-09-08 | Buchler Joseph | Device for fractionated extraction using more than two solvents |
| US3557869A (en) * | 1967-11-15 | 1971-01-26 | Hartmann & Braun Ag | Condensate draining device |
| US3471018A (en) * | 1968-07-24 | 1969-10-07 | Univ Eng Inc | Method and apparatus for separating a liquid mixture |
| SE341575B (enrdf_load_stackoverflow) * | 1969-11-05 | 1972-01-10 | Alfa Laval Ab | |
| US3627495A (en) * | 1970-05-25 | 1971-12-14 | Technicon Instr | Decantation fitting |
-
0
- BE BE788754D patent/BE788754A/xx unknown
-
1971
- 1971-10-13 US US00188830A patent/US3743103A/en not_active Expired - Lifetime
-
1972
- 1972-08-17 NL NL7211217A patent/NL7211217A/xx not_active Application Discontinuation
- 1972-08-18 CA CA149,730A patent/CA982491A/en not_active Expired
- 1972-08-22 IT IT28378/72A patent/IT964153B/it active
- 1972-08-25 AU AU45970/72A patent/AU465465B2/en not_active Expired
- 1972-09-12 GB GB4223772A patent/GB1378717A/en not_active Expired
- 1972-09-13 DE DE2244780A patent/DE2244780A1/de active Granted
- 1972-09-14 CH CH1350472A patent/CH546089A/xx not_active IP Right Cessation
- 1972-09-27 FR FR7234115A patent/FR2156619B1/fr not_active Expired
- 1972-10-12 JP JP10166572A patent/JPS5525882B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| AU465465B2 (en) | 1975-09-25 |
| CA982491A (en) | 1976-01-27 |
| JPS4847888A (enrdf_load_stackoverflow) | 1973-07-06 |
| AU4597072A (en) | 1974-02-28 |
| JPS5525882B2 (enrdf_load_stackoverflow) | 1980-07-09 |
| BE788754A (enrdf_load_stackoverflow) | 1973-03-13 |
| US3743103A (en) | 1973-07-03 |
| IT964153B (it) | 1974-01-21 |
| CH546089A (de) | 1974-02-28 |
| DE2244780C3 (enrdf_load_stackoverflow) | 1975-12-18 |
| GB1378717A (en) | 1974-12-27 |
| FR2156619B1 (enrdf_load_stackoverflow) | 1977-08-26 |
| FR2156619A1 (enrdf_load_stackoverflow) | 1973-06-01 |
| DE2244780A1 (de) | 1973-04-26 |
| NL7211217A (enrdf_load_stackoverflow) | 1973-04-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| 8339 | Ceased/non-payment of the annual fee |