DE2135435C3 - Verfahren zur Herstellung von gegen Schwefeldioxid beständigen Molybdatorange- und Molybdatrotpigmenten - Google Patents
Verfahren zur Herstellung von gegen Schwefeldioxid beständigen Molybdatorange- und MolybdatrotpigmentenInfo
- Publication number
- DE2135435C3 DE2135435C3 DE2135435A DE2135435A DE2135435C3 DE 2135435 C3 DE2135435 C3 DE 2135435C3 DE 2135435 A DE2135435 A DE 2135435A DE 2135435 A DE2135435 A DE 2135435A DE 2135435 C3 DE2135435 C3 DE 2135435C3
- Authority
- DE
- Germany
- Prior art keywords
- molybdate
- suspension
- sulfur dioxide
- antimony
- pigments
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 title claims description 12
- AUNAPVYQLLNFOI-UHFFFAOYSA-L [Pb++].[Pb++].[Pb++].[O-]S([O-])(=O)=O.[O-][Cr]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O Chemical compound [Pb++].[Pb++].[Pb++].[O-]S([O-])(=O)=O.[O-][Cr]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O AUNAPVYQLLNFOI-UHFFFAOYSA-L 0.000 title claims description 9
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 239000001054 red pigment Substances 0.000 title claims description 4
- 238000000034 method Methods 0.000 title claims description 3
- 239000000049 pigment Substances 0.000 claims description 14
- 239000000725 suspension Substances 0.000 claims description 13
- 238000001556 precipitation Methods 0.000 claims description 9
- -1 fluorine ions Chemical class 0.000 claims description 7
- SZOADBKOANDULT-UHFFFAOYSA-K antimonous acid Chemical compound O[Sb](O)O SZOADBKOANDULT-UHFFFAOYSA-K 0.000 claims description 5
- 229910001634 calcium fluoride Inorganic materials 0.000 claims description 4
- 229910052731 fluorine Inorganic materials 0.000 claims description 4
- 239000011737 fluorine Substances 0.000 claims description 4
- TWWDDFFHABKNMQ-UHFFFAOYSA-N oxosilicon;hydrate Chemical compound O.[Si]=O TWWDDFFHABKNMQ-UHFFFAOYSA-N 0.000 claims description 4
- 239000007864 aqueous solution Substances 0.000 claims description 3
- 239000007900 aqueous suspension Substances 0.000 claims description 2
- 229940043430 calcium compound Drugs 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 229910052787 antimony Inorganic materials 0.000 description 5
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 3
- 239000004115 Sodium Silicate Substances 0.000 description 3
- GUNJVIDCYZYFGV-UHFFFAOYSA-K antimony trifluoride Chemical compound F[Sb](F)F GUNJVIDCYZYFGV-UHFFFAOYSA-K 0.000 description 3
- 239000011575 calcium Substances 0.000 description 3
- 229910052791 calcium Inorganic materials 0.000 description 3
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 3
- 229910052911 sodium silicate Inorganic materials 0.000 description 3
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 2
- 239000001110 calcium chloride Substances 0.000 description 2
- 229910001628 calcium chloride Inorganic materials 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 239000001053 orange pigment Substances 0.000 description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical class O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 2
- 239000002966 varnish Substances 0.000 description 2
- ODNBVEIAQAZNNM-UHFFFAOYSA-N 1-(6-chloroimidazo[1,2-b]pyridazin-3-yl)ethanone Chemical compound C1=CC(Cl)=NN2C(C(=O)C)=CN=C21 ODNBVEIAQAZNNM-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 229920000877 Melamine resin Polymers 0.000 description 1
- 239000004640 Melamine resin Substances 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- MEYPRMGRFQCXHY-UHFFFAOYSA-N [Na].F[Si](F)(F)F Chemical compound [Na].F[Si](F)(F)F MEYPRMGRFQCXHY-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000000809 air pollutant Substances 0.000 description 1
- 231100001243 air pollutant Toxicity 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- FAPDDOBMIUGHIN-UHFFFAOYSA-K antimony trichloride Chemical compound Cl[Sb](Cl)Cl FAPDDOBMIUGHIN-UHFFFAOYSA-K 0.000 description 1
- 150000001674 calcium compounds Chemical class 0.000 description 1
- 239000004359 castor oil Substances 0.000 description 1
- 235000019438 castor oil Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- TXKMVPPZCYKFAC-UHFFFAOYSA-N disulfur monoxide Inorganic materials O=S=S TXKMVPPZCYKFAC-UHFFFAOYSA-N 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 1
- XLYOFNOQVPJJNP-ZSJDYOACSA-N heavy water Substances [2H]O[2H] XLYOFNOQVPJJNP-ZSJDYOACSA-N 0.000 description 1
- 150000004677 hydrates Chemical class 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 239000001023 inorganic pigment Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 150000003377 silicon compounds Chemical class 0.000 description 1
- 239000011775 sodium fluoride Substances 0.000 description 1
- 235000013024 sodium fluoride Nutrition 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical compound S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/0003—Compounds of molybdenum
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE786363D BE786363A (fr) | 1971-07-15 | Procede de preparation de pigments d'orange molybdate et de rouge molybdate | |
| DE2135435A DE2135435C3 (de) | 1971-07-15 | 1971-07-15 | Verfahren zur Herstellung von gegen Schwefeldioxid beständigen Molybdatorange- und Molybdatrotpigmenten |
| ZA723645A ZA723645B (en) | 1971-07-15 | 1972-05-29 | Process for the preparation of molybdate orange and molybdate red pigments stable to sulphur dioxide |
| NL7208060A NL7208060A (enExample) | 1971-07-15 | 1972-06-13 | |
| CH1048372A CH567063A5 (enExample) | 1971-07-15 | 1972-07-12 | |
| IT26962/72A IT962794B (it) | 1971-07-15 | 1972-07-13 | Processo per la preparazione di pigmenti di arancio molibdato e rosso molibdato stabili all ani dride solforosa |
| AU44522/72A AU469061B2 (en) | 1971-07-15 | 1972-07-13 | Process for the preparation of molybdate orange and molybdate red pigments stable to sulphur dioxide |
| FR7225486A FR2145686B1 (enExample) | 1971-07-15 | 1972-07-13 | |
| DK354272AA DK129135B (da) | 1971-07-15 | 1972-07-14 | Fremgangsmåde til fremstilling af SO2-bestandige molybdatorange- og molybdatrødt-pigmenter. |
| GB3300972A GB1396794A (en) | 1971-07-15 | 1972-07-14 | Molybdate orange and molybdate red |
| BR4670/72A BR7204670D0 (pt) | 1971-07-15 | 1972-07-14 | Processo para a preparacao de pigmentos laranja de molibdato e pigmentos vermelhos de molibdato resistentes ao dioxido de enxofre |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2135435A DE2135435C3 (de) | 1971-07-15 | 1971-07-15 | Verfahren zur Herstellung von gegen Schwefeldioxid beständigen Molybdatorange- und Molybdatrotpigmenten |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE2135435A1 DE2135435A1 (de) | 1973-01-25 |
| DE2135435B2 DE2135435B2 (de) | 1976-05-20 |
| DE2135435C3 true DE2135435C3 (de) | 1978-06-22 |
Family
ID=5813812
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE2135435A Expired DE2135435C3 (de) | 1971-07-15 | 1971-07-15 | Verfahren zur Herstellung von gegen Schwefeldioxid beständigen Molybdatorange- und Molybdatrotpigmenten |
Country Status (11)
| Country | Link |
|---|---|
| AU (1) | AU469061B2 (enExample) |
| BE (1) | BE786363A (enExample) |
| BR (1) | BR7204670D0 (enExample) |
| CH (1) | CH567063A5 (enExample) |
| DE (1) | DE2135435C3 (enExample) |
| DK (1) | DK129135B (enExample) |
| FR (1) | FR2145686B1 (enExample) |
| GB (1) | GB1396794A (enExample) |
| IT (1) | IT962794B (enExample) |
| NL (1) | NL7208060A (enExample) |
| ZA (1) | ZA723645B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2120451C1 (ru) * | 1996-07-04 | 1998-10-20 | Тамбовский государственный технический университет | Способ выделения пигмента из водной суспензии |
-
0
- BE BE786363D patent/BE786363A/xx unknown
-
1971
- 1971-07-15 DE DE2135435A patent/DE2135435C3/de not_active Expired
-
1972
- 1972-05-29 ZA ZA723645A patent/ZA723645B/xx unknown
- 1972-06-13 NL NL7208060A patent/NL7208060A/xx unknown
- 1972-07-12 CH CH1048372A patent/CH567063A5/xx not_active IP Right Cessation
- 1972-07-13 FR FR7225486A patent/FR2145686B1/fr not_active Expired
- 1972-07-13 IT IT26962/72A patent/IT962794B/it active
- 1972-07-13 AU AU44522/72A patent/AU469061B2/en not_active Expired
- 1972-07-14 GB GB3300972A patent/GB1396794A/en not_active Expired
- 1972-07-14 BR BR4670/72A patent/BR7204670D0/pt unknown
- 1972-07-14 DK DK354272AA patent/DK129135B/da unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2120451C1 (ru) * | 1996-07-04 | 1998-10-20 | Тамбовский государственный технический университет | Способ выделения пигмента из водной суспензии |
Also Published As
| Publication number | Publication date |
|---|---|
| NL7208060A (enExample) | 1973-01-17 |
| BE786363A (fr) | 1973-01-17 |
| ZA723645B (en) | 1973-03-28 |
| FR2145686B1 (enExample) | 1977-04-01 |
| DE2135435B2 (de) | 1976-05-20 |
| CH567063A5 (enExample) | 1975-09-30 |
| BR7204670D0 (pt) | 1973-05-24 |
| AU4452272A (en) | 1974-01-17 |
| GB1396794A (en) | 1975-06-04 |
| DK129135B (da) | 1974-08-26 |
| AU469061B2 (en) | 1976-02-05 |
| FR2145686A1 (enExample) | 1973-02-23 |
| DE2135435A1 (de) | 1973-01-25 |
| IT962794B (it) | 1973-12-31 |
| DK129135C (enExample) | 1975-01-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| EHJ | Ceased/non-payment of the annual fee |