DE212019C - - Google Patents
Info
- Publication number
- DE212019C DE212019C DENDAT212019D DE212019DA DE212019C DE 212019 C DE212019 C DE 212019C DE NDAT212019 D DENDAT212019 D DE NDAT212019D DE 212019D A DE212019D A DE 212019DA DE 212019 C DE212019 C DE 212019C
- Authority
- DE
- Germany
- Prior art keywords
- derivatives
- water
- heated
- ammonia
- addition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 238000000034 method Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000000984 vat dye Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B3/00—Dyes with an anthracene nucleus condensed with one or more carbocyclic rings
- C09B3/40—Pyranthrones
- C09B3/42—Preparation by synthesis of the nucleus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
PATENTSCHRIFTPATENT LETTERING
-JVl 212019-KLASSE 22b. GRUPPE -JVl 212019- CLASS 22b. GROUP
Zusatz zum Patente 175067 vom 6. April 1905.Addendum to patent 175067 of April 6, 1905.
Patentiert im Deutschen Reiche vom 31. Juli 1908 ab. Längste Dauer: 5. April 1920.Patented in the German Empire on July 31, 1908. Longest duration: April 5, 1920.
In dem Patent 175067 sowie in dem Zusatzpatent 211927 ist ein Verfahren beschrieben, nach dem 2 · 2' - Dimethyldianthrachinonyl oder dessen Derivate durch Erhitzen für sich oder bei der Behandlung mit wasserentziehenden Mitteln in neue 'Verbindungen übergeführt werden, welche die Eigenschaften von Küpenfarbstoffen besitzen (vgl. Patent 174494).In the patent 175067 and in the additional patent 211927 a method is described, after the 2 · 2 '- dimethyldianthraquinonyl or its derivatives by heating for itself or with after treatment with dehydrating agents are converted into new 'compounds, which have the properties of vat dyes (see patent 174494).
Es wurde nun gefunden, daß man dieses Verfahren in vorteilhafter Weise derart ausführen kann, daß man die genannten Verbindungen mit Wasser mit oder ohne Zusatz von Ammoniak oder Salzen erhitzt.It has now been found that this process can be carried out in an advantageous manner can that the compounds mentioned are heated with water with or without the addition of ammonia or salts.
Das Verfahren verläuft außerordentlich glatt und hat dabei den Vorteil größter Einfachheit.The process is extremely smooth and has the advantage of great simplicity.
Eine 5- bis ioprozentige wässerige Paste von 2 · 2' - Dimethyl -1 · 1' - dianthrachinonyl wird in einem geschlossenen Gefäß während 10 bis 12 Stunden auf 230 ° bis 250 ° erhitzt. Das Reaktionsprodukt ist identisch mit dem in den Beispielen 1 bis 3 des Hauptpatents beschriebenen Körper.A 5 to 10 percent aqueous paste of 2 · 2 '- dimethyl -1 · 1' - dianthraquinonyl is kept in a closed vessel during Heated to 230 ° to 250 ° for 10 to 12 hours. The reaction product is identical to that in Examples 1 to 3 of the main patent described body.
An Stelle von Wasser kann man auch wässeriges Ammoniak, Salzlösungen usw. verwenden, ferner kann das 2 · a'-Dimethyl-i · 1'-dianthraehinonyl durch seine Derivate ersetzt werden..Instead of water, you can also use aqueous ammonia, salt solutions, etc. furthermore, the 2 · a'-dimethyl-i · 1'-dianthraehinonyl be replaced by its derivatives ..
3030th
Claims (1)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE212019C true DE212019C (en) |
Family
ID=473780
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT212019D Active DE212019C (en) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE212019C (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2115131A1 (en) * | 1971-03-29 | 1972-10-05 | Badische Anilin- & Soda-Fabrik Ag, 6700 Ludwigshafen | Pyranthrones prodn - from 2,2-dialkyl 1,1-dianthraquinonyls by heating in polar solvents with alkali salts |
| US6502853B2 (en) | 2001-04-17 | 2003-01-07 | Milliken & Company | Low permeability airbag and method |
-
0
- DE DENDAT212019D patent/DE212019C/de active Active
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2115131A1 (en) * | 1971-03-29 | 1972-10-05 | Badische Anilin- & Soda-Fabrik Ag, 6700 Ludwigshafen | Pyranthrones prodn - from 2,2-dialkyl 1,1-dianthraquinonyls by heating in polar solvents with alkali salts |
| US6502853B2 (en) | 2001-04-17 | 2003-01-07 | Milliken & Company | Low permeability airbag and method |
| US6585293B2 (en) | 2001-04-17 | 2003-07-01 | Milliken & Company | Low permeability airbag and method |
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