DE200980C - - Google Patents
Info
- Publication number
- DE200980C DE200980C DE1907200980D DE200980DD DE200980C DE 200980 C DE200980 C DE 200980C DE 1907200980 D DE1907200980 D DE 1907200980D DE 200980D D DE200980D D DE 200980DD DE 200980 C DE200980 C DE 200980C
- Authority
- DE
- Germany
- Prior art keywords
- vapors
- spirit
- floors
- upwards
- rising
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/26—Fractionating columns in which vapour and liquid flow past each other, or in which the fluid is sprayed into the vapour, or in which a two-phase mixture is passed in one direction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Description
KAISERLICHESIMPERIAL
PATENTAMT.PATENT OFFICE.
Gegenstand der Erfindung ist ein Spiritusrektifizierapparat mit horizontal angeordneten Böden, durch welche der aufsteigende Spiritusdampf gezwungen wird, den Apparat im Zickzackwege zu durchziehen. Das kennzeichnende Merkmal der Erfindung besteht darin, daß von den Böden je zwei derart angeordnet sind und miteinander in Verbindung stehen, daß beide nach oben gewölbt sind,The invention relates to a spirit rectifier with horizontally arranged Soils through which the rising spirit vapor is forced to keep the apparatus in the To pull through zigzag paths. The characteristic feature of the invention is that two of the floors are arranged in this way and are connected to each other so that both are arched upwards,
to der obere dicht an den Mantel der Säule heranreicht und die Dämpfe in der Mitte
nach oben durchläßt, der untere dagegen voll ausgebildet ist, aber einen ringförmigen Durchgang
für die Dämpfe freiläßt. Infolge dieser Anordnung sammelt sich der Lutter auf beiden
Böden nur an ihrem Rande an und bietet daher dem aufsteigenden Spiritusdampf nur
wenig Oberfläche, so daß die Gefahr, daß der Lutter durch den über ihn hinwegziehenden
Spiritusdampf nochmals zur Verdampfung gebracht wird, wesentlich herabgemindert ist.
Die Zeichnung zeigt die Erfindung in
Fig. ι in einem Längsschnitt, während
Fig. 2 in größerem Maßstabe die Anordnung der Böden erkennen läßt.to the upper one comes close to the jacket of the column and lets the vapors through in the middle upwards, while the lower one is fully formed, but leaves an annular passage for the vapors. As a result of this arrangement, the Lutter only collects at the edge of both floors and therefore offers little surface to the rising spirit vapor, so that the risk of the Lutter being caused to evaporate again by the spirit vapor flowing over it is considerably reduced. The drawing shows the invention in
Fig. Ι in a longitudinal section, while
Fig. 2 shows the arrangement of the floors on a larger scale.
Der Apparat α ist vorteilhaft über einer mit Wasser gefüllten Blase b angeordnet, welcher der Rohspiritus in Dampfform durch das Rohr c zugeführt wird. Die Böden d, e zwingen den Spiritus, den Apparat α im Zickzackwege zu durchwandern.The apparatus α is advantageously arranged above a water-filled bladder b to which the raw alcohol is fed in vapor form through the pipe c . The floors d, e force the spirit to wander through the apparatus α in a zigzag path.
Wie aus der Zeichnung zu erkennen ist, sind sowohl die Böden d als auch die Boden e nach oben gewölbt, und zwar reichen die Böden d bis an den Mantel der Säule a. heran und besitzen in ihrer Mitte eine Durchtrittsöffnung/ für den aufsteigenden Spiritusdampf, während die Böden e voll ausgebildet und derart angeordnet sind, daß sie einen ringförmigen Durchgang g für die aufsteigenden Spiritusdämpfe freilassen. Jeder Boden ist mit dem darunterliegenden durch ein Überlaufrohr h verbunden, so daß der sich am Rande der Böden sammelnde Lutter immer wieder auf den darunterliegenden Boden geleitet wird, bis er schließlich vom untersten Boden d durch das Rohr i abgezogen werden kann.As can be seen from the drawing, both the bottoms d and the bottoms e are arched upwards, namely the bottoms d extend to the jacket of the column a. approach and have in their middle a passage opening / for the rising spirit vapor, while the floors e are fully formed and are arranged in such a way that they leave an annular passage g free for the rising spirit vapors. Each tray is connected to the one below by an overflow pipe h , so that the Lutter that collects at the edge of the floors is repeatedly directed onto the tray below until it can finally be drawn off from the lowest tray d through the pipe i .
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE200980T | 1907-11-05 |
Publications (1)
Publication Number | Publication Date |
---|---|
DE200980C true DE200980C (en) | 1908-08-05 |
Family
ID=34484445
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE1907200980D Expired DE200980C (en) | 1907-11-05 | 1907-11-05 |
Country Status (1)
Country | Link |
---|---|
DE (1) | DE200980C (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2671053A (en) * | 1947-06-20 | 1954-03-02 | Shell Dev | Method and apparatus for high vacuum distillation |
-
1907
- 1907-11-05 DE DE1907200980D patent/DE200980C/de not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2671053A (en) * | 1947-06-20 | 1954-03-02 | Shell Dev | Method and apparatus for high vacuum distillation |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
DE3522234C2 (en) | Process for the energy-efficient operation of a distillation column | |
DE200980C (en) | ||
DE2717770A1 (en) | DEVICE FOR SEPARATING WATER AND MATERIALS CONTAINED IN IT | |
DE1084699B (en) | Device for evacuating the liquid from column floors | |
DE2037237A1 (en) | Distillative liquid separation | |
DE2412700A1 (en) | DEVICE FOR SEPARATING VAPORS FROM A FLOW OF AIR | |
DE2102424A1 (en) | Liquid distributor for a mass transfer column | |
DE1240045B (en) | Device for bringing a gas into contact with a liquid | |
DE2102678C3 (en) | Device for applying fine particles from an aerosol | |
DE205773C (en) | ||
DE624276C (en) | Method and device for washing or extracting immiscible or only partially miscible liquids in countercurrent | |
DE717851C (en) | Device for the intimate mixing of vapors and liquids in exchange columns | |
DE101323C (en) | ||
DE417040C (en) | Device for homogenizing liquids | |
DE449731C (en) | Suction air cleaning device for threshing machines | |
DE476161C (en) | Bracket for curtain rods | |
DE78678C (en) | Distiller for fatty acids, hydrocarbons and the like | |
DE1110139B (en) | Device for separating liquid particles from gases | |
DE2835462A1 (en) | Mass transfer tray with double feed from either side - two-sections identical with central support and end weir with downcomers and seal pans feeding tray below liq. flow being same on each tray | |
DE967462C (en) | Process for the parallel operation of two or more Fuellkoerpersaeulen | |
DE289644C (en) | ||
DE553196C (en) | Method and device for the fractional condensation of mineral oil fumes | |
DE663349C (en) | Separating column and exchange floors | |
DE185936C (en) | ||
DE49623C (en) | filter |