DE19748359A1 - Verfahren zur Herstellung teilkristalliner Polyetherpolyole - Google Patents

Verfahren zur Herstellung teilkristalliner Polyetherpolyole

Info

Publication number
DE19748359A1
DE19748359A1 DE19748359A DE19748359A DE19748359A1 DE 19748359 A1 DE19748359 A1 DE 19748359A1 DE 19748359 A DE19748359 A DE 19748359A DE 19748359 A DE19748359 A DE 19748359A DE 19748359 A1 DE19748359 A1 DE 19748359A1
Authority
DE
Germany
Prior art keywords
polyether polyols
bimetallic
functionality
oxoalkoxides
formula
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE19748359A
Other languages
German (de)
English (en)
Inventor
Walter Dr Schaefer
Joerg Dr Hofmann
Pramod Dr Gupta
Hanns-Peter Dr Mueller
Harald Dr Pielartzik
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Priority to DE19748359A priority Critical patent/DE19748359A1/de
Priority to EP98958860A priority patent/EP1028990B1/de
Priority to US09/530,304 priority patent/US6458918B1/en
Priority to HK01104361.2A priority patent/HK1033834B/xx
Priority to DE59810564T priority patent/DE59810564D1/de
Priority to KR1020007004761A priority patent/KR100556175B1/ko
Priority to CN98810796A priority patent/CN1116335C/zh
Priority to JP2000519004A priority patent/JP4399108B2/ja
Priority to BR9814110-4A priority patent/BR9814110A/pt
Priority to ES98958860T priority patent/ES2212381T3/es
Priority to AU14858/99A priority patent/AU1485899A/en
Priority to CA002308168A priority patent/CA2308168C/en
Priority to PCT/EP1998/006689 priority patent/WO1999023135A1/de
Priority to TW087118009A priority patent/TW486494B/zh
Publication of DE19748359A1 publication Critical patent/DE19748359A1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/269—Mixed catalyst systems, i.e. containing more than one reactive component or catalysts formed in-situ
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C08G65/10—Saturated oxiranes characterised by the catalysts used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/06—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing polymers
    • B01J31/068—Polyalkylene glycols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/165—Polymer immobilised coordination complexes, e.g. organometallic complexes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/22—Organic complexes
    • B01J31/2204—Organic complexes the ligands containing oxygen or sulfur as complexing atoms
    • B01J31/2208—Oxygen, e.g. acetylacetonates
    • B01J31/2226—Anionic ligands, i.e. the overall ligand carries at least one formal negative charge
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
    • C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
    • C08G65/08—Saturated oxiranes
    • C08G65/10—Saturated oxiranes characterised by the catalysts used
    • C08G65/12—Saturated oxiranes characterised by the catalysts used containing organo-metallic compounds or metal hydrides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/40—Substitution reactions at carbon centres, e.g. C-C or C-X, i.e. carbon-hetero atom, cross-coupling, C-H activation or ring-opening reactions
    • B01J2231/48—Ring-opening reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/02—Compositional aspects of complexes used, e.g. polynuclearity
    • B01J2531/0213—Complexes without C-metal linkages
    • B01J2531/0216—Bi- or polynuclear complexes, i.e. comprising two or more metal coordination centres, without metal-metal bonds, e.g. Cp(Lx)Zr-imidazole-Zr(Lx)Cp
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/02—Compositional aspects of complexes used, e.g. polynuclearity
    • B01J2531/0213—Complexes without C-metal linkages
    • B01J2531/0219—Bimetallic complexes, i.e. comprising one or more units of two metals, with metal-metal bonds but no all-metal (M)n rings, e.g. Cr2(OAc)4
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/20—Complexes comprising metals of Group II (IIA or IIB) as the central metal
    • B01J2531/26—Zinc
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/30—Complexes comprising metals of Group III (IIIA or IIIB) as the central metal
    • B01J2531/31—Aluminium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/40—Complexes comprising metals of Group IV (IVA or IVB) as the central metal
    • B01J2531/46—Titanium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/60—Complexes comprising metals of Group VI (VIA or VIB) as the central metal
    • B01J2531/62—Chromium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/60—Complexes comprising metals of Group VI (VIA or VIB) as the central metal
    • B01J2531/64—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/70—Complexes comprising metals of Group VII (VIIB) as the central metal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84—Metals of the iron group
    • B01J2531/842—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/84—Metals of the iron group
    • B01J2531/845—Cobalt
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2250/00—Compositions for preparing crystalline polymers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyethers (AREA)
DE19748359A 1997-11-03 1997-11-03 Verfahren zur Herstellung teilkristalliner Polyetherpolyole Withdrawn DE19748359A1 (de)

Priority Applications (14)

Application Number Priority Date Filing Date Title
DE19748359A DE19748359A1 (de) 1997-11-03 1997-11-03 Verfahren zur Herstellung teilkristalliner Polyetherpolyole
EP98958860A EP1028990B1 (de) 1997-11-03 1998-10-21 Verfahren zur herstellung teilkristalliner polyetherpolyole
US09/530,304 US6458918B1 (en) 1997-11-03 1998-10-21 Method for producing partially crystalline polyether polyols
HK01104361.2A HK1033834B (en) 1997-11-03 1998-10-21 Method for producing partially crystalline polyether polyols
DE59810564T DE59810564D1 (de) 1997-11-03 1998-10-21 Verfahren zur herstellung teilkristalliner polyetherpolyole
KR1020007004761A KR100556175B1 (ko) 1997-11-03 1998-10-21 부분 결정질 폴리에테르 폴리올의 제조 방법
CN98810796A CN1116335C (zh) 1997-11-03 1998-10-21 部分结晶的聚醚多元醇的制备方法
JP2000519004A JP4399108B2 (ja) 1997-11-03 1998-10-21 部分結晶性ポリエーテルポリオールの製造方法
BR9814110-4A BR9814110A (pt) 1997-11-03 1998-10-21 Processo para a preparação de poliéter-polióis semicristalinos
ES98958860T ES2212381T3 (es) 1997-11-03 1998-10-21 Procedimiento para la fabricacion de polioleteres semicristalinos.
AU14858/99A AU1485899A (en) 1997-11-03 1998-10-21 Method for producing partially crystalline polyether polyols
CA002308168A CA2308168C (en) 1997-11-03 1998-10-21 Method for producing partially crystalline polyether polyols
PCT/EP1998/006689 WO1999023135A1 (de) 1997-11-03 1998-10-21 Verfahren zur herstellung teilkristalliner polyetherpolyole
TW087118009A TW486494B (en) 1997-11-03 1998-10-30 A process for the preparation of partially crystalline polyether polyols

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19748359A DE19748359A1 (de) 1997-11-03 1997-11-03 Verfahren zur Herstellung teilkristalliner Polyetherpolyole

Publications (1)

Publication Number Publication Date
DE19748359A1 true DE19748359A1 (de) 1999-05-06

Family

ID=7847346

Family Applications (2)

Application Number Title Priority Date Filing Date
DE19748359A Withdrawn DE19748359A1 (de) 1997-11-03 1997-11-03 Verfahren zur Herstellung teilkristalliner Polyetherpolyole
DE59810564T Expired - Lifetime DE59810564D1 (de) 1997-11-03 1998-10-21 Verfahren zur herstellung teilkristalliner polyetherpolyole

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE59810564T Expired - Lifetime DE59810564D1 (de) 1997-11-03 1998-10-21 Verfahren zur herstellung teilkristalliner polyetherpolyole

Country Status (12)

Country Link
US (1) US6458918B1 (https=)
EP (1) EP1028990B1 (https=)
JP (1) JP4399108B2 (https=)
KR (1) KR100556175B1 (https=)
CN (1) CN1116335C (https=)
AU (1) AU1485899A (https=)
BR (1) BR9814110A (https=)
CA (1) CA2308168C (https=)
DE (2) DE19748359A1 (https=)
ES (1) ES2212381T3 (https=)
TW (1) TW486494B (https=)
WO (1) WO1999023135A1 (https=)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19919267A1 (de) * 1999-04-28 2000-11-02 Bayer Ag Kristallisierende Polyetherpolyole, ein Verfahren zu deren Herstellung sowie deren Verwendung
US7750891B2 (en) 2003-04-09 2010-07-06 Tegic Communications, Inc. Selective input system based on tracking of motion parameters of an input device
US7821503B2 (en) 2003-04-09 2010-10-26 Tegic Communications, Inc. Touch screen and graphical user interface
GB0305817D0 (en) * 2003-03-13 2003-04-16 Ic Innovations Ltd Polymerisation initiators
CN1289904C (zh) * 2003-08-01 2006-12-13 博奥生物有限公司 一种微阵列反应装置及其应用
KR100581616B1 (ko) * 2004-02-03 2006-05-22 에스케이씨 주식회사 광학 입체 규칙성을 갖는 폴리에테르폴리올 및 그의제조방법
JP2008163220A (ja) * 2006-12-28 2008-07-17 Sanyo Chem Ind Ltd ポリ乳酸樹脂用改質剤
JP5490372B2 (ja) * 2007-04-26 2014-05-14 三洋化成工業株式会社 結晶性ポリオキシアルキレンポリオールの製造方法およびこれを原料とした樹脂
US9052623B2 (en) 2010-10-06 2015-06-09 Sanyo Chemical Industries, Ltd. Toner binder and toner composition
JP2013080200A (ja) 2011-05-02 2013-05-02 Ricoh Co Ltd 電子写真用トナー、現像剤、及び画像形成装置
CA2859566A1 (en) 2011-12-20 2013-06-27 Bayer Intellectual Property Gmbh Hydroxy-aminopolymers and method for producing same
JP6323015B2 (ja) 2013-03-15 2018-05-16 株式会社リコー 静電荷像現像用トナー
JP6510515B2 (ja) * 2013-11-22 2019-05-08 ダウ グローバル テクノロジーズ エルエルシー エポキシドモノマーの重合のための亜鉛触媒／添加剤システム

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1478334A (fr) * 1965-05-06 1967-04-28 Inst Francais Du Petrole Catalyseur à base de métaux bivalents, sa préparation et ses applications, en particulier pour la polymérisation d'éthers cycliques
ES2150616T3 (es) * 1995-05-31 2000-12-01 Hoechst Ag Lamina de polipropileno biaxialmente orientada con una estabilidad dimensional mejorada.

Also Published As

Publication number Publication date
JP4399108B2 (ja) 2010-01-13
DE59810564D1 (de) 2004-02-12
BR9814110A (pt) 2000-10-03
KR100556175B1 (ko) 2006-03-03
CA2308168A1 (en) 1999-05-14
TW486494B (en) 2002-05-11
EP1028990B1 (de) 2004-01-07
WO1999023135A1 (de) 1999-05-14
AU1485899A (en) 1999-05-24
EP1028990A1 (de) 2000-08-23
KR20010031698A (ko) 2001-04-16
CA2308168C (en) 2008-05-06
US6458918B1 (en) 2002-10-01
CN1278278A (zh) 2000-12-27
CN1116335C (zh) 2003-07-30
ES2212381T3 (es) 2004-07-16
HK1033834A1 (en) 2001-09-28
JP2001521957A (ja) 2001-11-13

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