DE169683C - - Google Patents

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Publication number

DE169683C

DE169683C DENDAT169683D DE169683DA DE169683C DE 169683 C DE169683 C DE 169683C DE NDAT169683 D DENDAT169683 D DE NDAT169683D DE 169683D A DE169683D A DE 169683DA DE 169683 C DE169683 C DE 169683C

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DE

Germany

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sulfonic acid

Prior art date

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• LSNNMFCWUKXFEE-UHFFFAOYSA-N sulfonic acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims description 8
• GHMLBKRAJCXXBS-UHFFFAOYSA-N Resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 6
• JWAZRIHNYRIHIV-UHFFFAOYSA-N 2-Naphthol Chemical compound C1=CC=CC2=CC(O)=CC=C21 JWAZRIHNYRIHIV-UHFFFAOYSA-N 0.000 claims description 5
• KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-Naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 claims description 4
• 229940018564 M-PHENYLENEDIAMINE Drugs 0.000 claims description 3
• WZCQRUWWHSTZEM-UHFFFAOYSA-N M-Phenylenediamine Chemical compound NC1=CC=CC(N)=C1 WZCQRUWWHSTZEM-UHFFFAOYSA-N 0.000 claims description 3
• 238000000034 method Methods 0.000 claims description 3
• VOZKAJLKRJDJLL-UHFFFAOYSA-N 2,4-Diaminotoluene Chemical compound CC1=CC=C(N)C=C1N VOZKAJLKRJDJLL-UHFFFAOYSA-N 0.000 claims description 2
• RJKGJBPXVHTNJL-UHFFFAOYSA-N 1-nitronaphthalene Chemical compound C1=CC=C2C([N+](=O)[O-])=CC=CC2=C1 RJKGJBPXVHTNJL-UHFFFAOYSA-N 0.000 claims 1
• ALKYHXVLJMQRLQ-UHFFFAOYSA-N 3-Hydroxy-2-naphthoate Chemical compound C1=CC=C2C=C(O)C(C(=O)O)=CC2=C1 ALKYHXVLJMQRLQ-UHFFFAOYSA-N 0.000 claims 1
• 108060005223 NARF Proteins 0.000 claims 1
• 239000002253 acid Substances 0.000 claims 1
• 239000000987 azo dye Substances 0.000 claims 1
• 239000000843 powder Substances 0.000 description 18
• 239000000975 dye Substances 0.000 description 13
• 239000002244 precipitate Substances 0.000 description 10
• 235000005811 Viola adunca Nutrition 0.000 description 7
• 235000013487 Viola odorata Nutrition 0.000 description 7
• 235000002254 Viola papilionacea Nutrition 0.000 description 7
• HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
• UPKAWFACSJWKND-ZXFFUEEESA-J tetrasodium;(6E)-4-amino-6-[[4-[4-[(2Z)-2-(8-amino-1-oxo-5,7-disulfonatonaphthalen-2-ylidene)hydrazinyl]-3-methoxyphenyl]-2-methoxyphenyl]hydrazinylidene]-5-oxonaphthalene-1,3-disulfonate Chemical compound [Na+].[Na+].[Na+].[Na+].C\1=CC2=C(S([O-])(=O)=O)C=C(S([O-])(=O)=O)C(N)=C2C(=O)C/1=N/NC(C(OC)=C1)=CC=C1C1=CC=C(N\N=C\2C(C3=C(N)C(=CC(=C3C=C/2)S([O-])(=O)=O)S([O-])(=O)=O)=O)C(OC)=C1 UPKAWFACSJWKND-ZXFFUEEESA-J 0.000 description 6
• 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 description 5
• 239000002932 luster Substances 0.000 description 5
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
• 240000003497 Rubus idaeus Species 0.000 description 4
• 240000000358 Viola adunca Species 0.000 description 4
• -1 nitrodiazooxynaphthalene sulfonic acid Chemical class 0.000 description 4
• IVNZBWNBYXERPK-DZGBHZPSSA-K trisodium;(8Z)-7-oxo-8-[(4-sulfonatonaphthalen-1-yl)hydrazinylidene]naphthalene-1,3-disulfonate Chemical compound [Na+].[Na+].[Na+].C1=CC=C2C(N\N=C3/C(=O)C=CC=4C=C(C=C(C=43)S([O-])(=O)=O)S(=O)(=O)[O-])=CC=C(S([O-])(=O)=O)C2=C1 IVNZBWNBYXERPK-DZGBHZPSSA-K 0.000 description 4
• 235000011034 Rubus glaucus Nutrition 0.000 description 3
• 235000009122 Rubus idaeus Nutrition 0.000 description 3
• 240000009038 Viola odorata Species 0.000 description 3
• 230000015572 biosynthetic process Effects 0.000 description 3
• 238000005755 formation reaction Methods 0.000 description 3
• 239000000203 mixture Substances 0.000 description 3
• VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
• 238000004040 coloring Methods 0.000 description 2
• 150000001875 compounds Chemical class 0.000 description 2
• 230000000875 corresponding Effects 0.000 description 2
• 230000001808 coupling Effects 0.000 description 2
• 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 2
• 238000001556 precipitation Methods 0.000 description 2
• FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
• 238000003756 stirring Methods 0.000 description 2
• SOAAGHDAWFEEPP-JZJYNLBNSA-N (4Z)-4-[(2,4-dimethylphenyl)hydrazinylidene]-3-oxonaphthalene-2,7-disulfonic acid Chemical compound CC1=CC(C)=CC=C1N\N=C/1C2=CC=C(S(O)(=O)=O)C=C2C=C(S(O)(=O)=O)C\1=O SOAAGHDAWFEEPP-JZJYNLBNSA-N 0.000 description 1
• WZPLEIAOQJXZJX-UHFFFAOYSA-N 2,3-dihydroxynaphthalene-1-carboxylic acid Chemical compound C1=CC=C2C(C(=O)O)=C(O)C(O)=CC2=C1 WZPLEIAOQJXZJX-UHFFFAOYSA-N 0.000 description 1
• 241000974482 Aricia saepiolus Species 0.000 description 1
• BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
• NIKFYOSELWJIOF-UHFFFAOYSA-O Fuchsine Chemical compound Cl.C1=C(N)C(C)=CC(C(=C2C=CC(=[NH2+])C=C2)C=2C=CC(N)=CC=2)=C1 NIKFYOSELWJIOF-UHFFFAOYSA-O 0.000 description 1
• ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Natural products OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
• 210000002268 Wool Anatomy 0.000 description 1
• 230000002378 acidificating Effects 0.000 description 1
• 239000000654 additive Substances 0.000 description 1
• 230000000996 additive Effects 0.000 description 1
• QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
• 125000000751 azo group Chemical group [*]N=N[*] 0.000 description 1
• OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
• 235000012730 carminic acid Nutrition 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 238000010168 coupling process Methods 0.000 description 1
• 238000005859 coupling reaction Methods 0.000 description 1
• 150000008049 diazo compounds Chemical class 0.000 description 1
• 239000010438 granite Substances 0.000 description 1
• 235000015810 grayleaf red raspberry Nutrition 0.000 description 1
• 150000004780 naphthols Chemical class 0.000 description 1
• 238000006396 nitration reaction Methods 0.000 description 1
• 150000002989 phenols Chemical class 0.000 description 1
• VMHLLURERBWHNL-UHFFFAOYSA-M sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
• 239000001632 sodium acetate Substances 0.000 description 1
• 235000017281 sodium acetate Nutrition 0.000 description 1
• 239000011780 sodium chloride Substances 0.000 description 1
• 239000004071 soot Substances 0.000 description 1
• 238000010626 work up procedure Methods 0.000 description 1