DE1598265A1 - Verfahren und Vorrichtung zur Analyse durch Molekular-Destillation - Google Patents
Verfahren und Vorrichtung zur Analyse durch Molekular-DestillationInfo
- Publication number
- DE1598265A1 DE1598265A1 DE19661598265 DE1598265A DE1598265A1 DE 1598265 A1 DE1598265 A1 DE 1598265A1 DE 19661598265 DE19661598265 DE 19661598265 DE 1598265 A DE1598265 A DE 1598265A DE 1598265 A1 DE1598265 A1 DE 1598265A1
- Authority
- DE
- Germany
- Prior art keywords
- mixture
- temperature
- analyzed
- analysis
- monitored
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004458 analytical method Methods 0.000 title claims description 16
- 238000000034 method Methods 0.000 title claims description 11
- 238000000199 molecular distillation Methods 0.000 title claims description 4
- 239000000203 mixture Substances 0.000 claims description 32
- 239000003990 capacitor Substances 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 239000002826 coolant Substances 0.000 claims description 4
- 238000001704 evaporation Methods 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 230000001105 regulatory effect Effects 0.000 claims description 4
- 229910001220 stainless steel Inorganic materials 0.000 claims description 4
- 239000010935 stainless steel Substances 0.000 claims description 4
- 238000009833 condensation Methods 0.000 claims description 3
- 230000005494 condensation Effects 0.000 claims description 3
- 239000012212 insulator Substances 0.000 claims description 3
- 238000004949 mass spectrometry Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000012544 monitoring process Methods 0.000 claims description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 2
- 230000008020 evaporation Effects 0.000 claims 2
- 238000004566 IR spectroscopy Methods 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 230000002123 temporal effect Effects 0.000 claims 1
- 239000000523 sample Substances 0.000 description 8
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 229920000265 Polyparaphenylene Polymers 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000000110 cooling liquid Substances 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000002605 large molecules Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- -1 polyphenylene Polymers 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/12—Molecular distillation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/14—Investigating or analyzing materials by the use of thermal means by using distillation, extraction, sublimation, condensation, freezing, or crystallisation
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR17156A FR1458175A (fr) | 1965-05-14 | 1965-05-14 | Procédé et dispositif pour l'analyse par distillation moléculaire |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1598265A1 true DE1598265A1 (de) | 1972-03-02 |
Family
ID=8578813
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19661598265 Pending DE1598265A1 (de) | 1965-05-14 | 1966-05-11 | Verfahren und Vorrichtung zur Analyse durch Molekular-Destillation |
Country Status (10)
| Country | Link |
|---|---|
| BE (1) | BE680662A (cg-RX-API-DMAC10.html) |
| CH (1) | CH462506A (cg-RX-API-DMAC10.html) |
| DE (1) | DE1598265A1 (cg-RX-API-DMAC10.html) |
| ES (1) | ES326762A1 (cg-RX-API-DMAC10.html) |
| FR (1) | FR1458175A (cg-RX-API-DMAC10.html) |
| GB (1) | GB1119883A (cg-RX-API-DMAC10.html) |
| IL (1) | IL25733A (cg-RX-API-DMAC10.html) |
| LU (1) | LU51062A1 (cg-RX-API-DMAC10.html) |
| NL (1) | NL6606354A (cg-RX-API-DMAC10.html) |
| SE (1) | SE307026B (cg-RX-API-DMAC10.html) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3039487A1 (de) * | 1980-10-18 | 1982-05-19 | Compagnie Française de Raffinage S.A., Paris | Verfahren und vorrichtung zur untersuchung von hochsiedenden produkten durch destillation |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2123782A5 (en) * | 1971-02-01 | 1972-09-15 | Delalande Sa | Vacuum drying chamber - permits constant observation of chemical samples during drying process |
-
1965
- 1965-05-14 FR FR17156A patent/FR1458175A/fr not_active Expired
-
1966
- 1966-05-06 BE BE680662D patent/BE680662A/xx unknown
- 1966-05-09 GB GB2051866A patent/GB1119883A/en not_active Expired
- 1966-05-10 NL NL6606354A patent/NL6606354A/xx unknown
- 1966-05-10 IL IL2573366A patent/IL25733A/xx unknown
- 1966-05-10 LU LU51062A patent/LU51062A1/xx unknown
- 1966-05-11 DE DE19661598265 patent/DE1598265A1/de active Pending
- 1966-05-13 CH CH700166A patent/CH462506A/fr unknown
- 1966-05-13 SE SE661066A patent/SE307026B/xx unknown
- 1966-05-14 ES ES0326762A patent/ES326762A1/es not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3039487A1 (de) * | 1980-10-18 | 1982-05-19 | Compagnie Française de Raffinage S.A., Paris | Verfahren und vorrichtung zur untersuchung von hochsiedenden produkten durch destillation |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1458175A (fr) | 1966-03-04 |
| CH462506A (fr) | 1968-09-15 |
| NL6606354A (cg-RX-API-DMAC10.html) | 1966-11-15 |
| SE307026B (cg-RX-API-DMAC10.html) | 1968-12-16 |
| BE680662A (cg-RX-API-DMAC10.html) | 1966-10-17 |
| GB1119883A (en) | 1968-07-17 |
| ES326762A1 (es) | 1967-07-01 |
| IL25733A (en) | 1969-11-30 |
| LU51062A1 (cg-RX-API-DMAC10.html) | 1966-07-11 |
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