DE155633C - - Google Patents

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Publication number

DE155633C

DE155633C DENDAT155633D DE155633DA DE155633C DE 155633 C DE155633 C DE 155633C DE NDAT155633 D DENDAT155633 D DE NDAT155633D DE 155633D A DE155633D A DE 155633DA DE 155633 C DE155633 C DE 155633C

Authority

DE

Germany

Prior art keywords

anthrachrysone

dialkyl

yellow

dimethyl ether

water

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

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• NNAUDJVNWLIGDT-UHFFFAOYSA-N 1,3,5,7-tetrahydroxyanthracene-9,10-dione Chemical class OC1=CC(O)=C2C(=O)C3=CC(O)=CC(O)=C3C(=O)C2=C1 NNAUDJVNWLIGDT-UHFFFAOYSA-N 0.000 claims description 3
• 150000001447 alkali salts Chemical class 0.000 claims description 3
• -1 anthrachrysone dialkyl ethers Chemical class 0.000 claims description 3
• 238000000034 method Methods 0.000 claims description 3
• 150000008050 dialkyl sulfates Chemical class 0.000 claims description 2
• RKYAZRHUKGRDNT-UHFFFAOYSA-N heptacyclo[16.12.0.02,11.03,8.012,17.021,30.023,28]triaconta-1(18),2(11),3,5,7,12,14,16,19,21,23,25,27,29-tetradecaen-9-one Chemical class C12=C3C=C4C=CC=CC4=CC3=CC=C2C2=CC=CC=C2C2=C1C1=CC=CC=C1C(=O)C2 RKYAZRHUKGRDNT-UHFFFAOYSA-N 0.000 claims 1
• LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 10
• QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
• AYNUDFKSZLCYEV-UHFFFAOYSA-N 10,13-dinitroheptacyclo[16.12.0.02,11.03,8.012,17.021,30.023,28]triaconta-1,3,5,7,11,13,15,17,19,21,23,25,27,29-tetradecaen-9-one Chemical compound [N+](=O)([O-])C1=CC=CC2=C3C(=C4C=5C=CC=CC5C(C(C4=C12)[N+](=O)[O-])=O)C1=CC2=CC=CC=C2C=C1C=C3 AYNUDFKSZLCYEV-UHFFFAOYSA-N 0.000 description 3
• 239000000843 powder Substances 0.000 description 3
• 159000000000 sodium salts Chemical class 0.000 description 3
• 239000007858 starting material Substances 0.000 description 3
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
• QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical group N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
• KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 2
• 239000004327 boric acid Substances 0.000 description 2
• VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical compound COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 description 2
• 150000003839 salts Chemical class 0.000 description 2
• 239000000243 solution Substances 0.000 description 2
• POIMGHRQQQGFQZ-UHFFFAOYSA-N 10,13-dibromoheptacyclo[16.12.0.02,11.03,8.012,17.021,30.023,28]triaconta-1,3,5,7,11,13,15,17,19,21,23,25,27,29-tetradecaen-9-one Chemical compound BrC1C(=O)c2ccccc2-c2c1c1c(Br)cccc1c1ccc3cc4ccccc4cc3c21 POIMGHRQQQGFQZ-UHFFFAOYSA-N 0.000 description 1
• UWOGELSGKTUEAK-UHFFFAOYSA-N 9-oxoheptacyclo[16.12.0.02,11.03,8.012,17.021,30.023,28]triaconta-1,3,5,7,11,13,15,17,19,21,23,25,27,29-tetradecaene-10,13-disulfonic acid Chemical compound C1(C(C=2C3=C(C=CC=C3C3=C(C2C=2C=CC=CC12)C1=CC2=CC=CC=C2C=C1C=C3)S(=O)(=O)O)S(=O)(=O)O)=O UWOGELSGKTUEAK-UHFFFAOYSA-N 0.000 description 1
• WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
• CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
• 229960000583 acetic acid Drugs 0.000 description 1
• 239000002253 acid Substances 0.000 description 1
• 229910021529 ammonia Inorganic materials 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 239000001045 blue dye Substances 0.000 description 1
• GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
• 229910052794 bromium Inorganic materials 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 150000001983 dialkylethers Chemical class 0.000 description 1
• 239000000975 dye Substances 0.000 description 1
• 239000012362 glacial acetic acid Substances 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 230000008018 melting Effects 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 150000003142 primary aromatic amines Chemical class 0.000 description 1
• GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
• 239000002904 solvent Substances 0.000 description 1