DE1228016B - Method of manufacturing lubricants for use in hot extrusion of steel blocks - Google Patents

Method of manufacturing lubricants for use in hot extrusion of steel blocks

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Publication number
DE1228016B
DE1228016B DEM60706A DEM0060706A DE1228016B DE 1228016 B DE1228016 B DE 1228016B DE M60706 A DEM60706 A DE M60706A DE M0060706 A DEM0060706 A DE M0060706A DE 1228016 B DE1228016 B DE 1228016B
Authority
DE
Germany
Prior art keywords
lubricants
hot extrusion
steel blocks
powdered
sintered
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DEM60706A
Other languages
German (de)
Inventor
Kurt Darschewski
Dr-Ing Gerhard Naeser
Dipl-Ing Otto Wessel
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Vodafone GmbH
Original Assignee
Mannesmann AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to DEM60373A priority Critical patent/DE1204767B/en
Application filed by Mannesmann AG filed Critical Mannesmann AG
Priority to DEM60706A priority patent/DE1228016B/en
Priority to DE19651594495 priority patent/DE1594495A1/en
Priority to AT205565A priority patent/AT257794B/en
Priority to NL6503091A priority patent/NL6503091A/xx
Priority to ES0310730A priority patent/ES310730A1/en
Priority to GB11798/65A priority patent/GB1107183A/en
Priority to SE03574/65A priority patent/SE325981B/xx
Priority to FR10086A priority patent/FR1448029A/en
Priority to BE661471D priority patent/BE661471A/xx
Publication of DE1228016B publication Critical patent/DE1228016B/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M7/00Solid or semi-solid compositions essentially based on lubricating components other than mineral lubricating oils or fatty oils and their use as lubricants; Use as lubricants of single solid or semi-solid substances
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/02Water
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06Metal compounds
    • C10M2201/062Oxides; Hydroxides; Carbonates or bicarbonates
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06Metal compounds
    • C10M2201/063Peroxides
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    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08Inorganic acids or salts thereof
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08Inorganic acids or salts thereof
    • C10M2201/081Inorganic acids or salts thereof containing halogen
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08Inorganic acids or salts thereof
    • C10M2201/082Inorganic acids or salts thereof containing nitrogen
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08Inorganic acids or salts thereof
    • C10M2201/084Inorganic acids or salts thereof containing sulfur, selenium or tellurium
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/085Phosphorus oxides, acids or salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/086Chromium oxides, acids or salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00Metal present as such or in compounds
    • C10N2010/02Groups 1 or 11
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2010/00Metal present as such or in compounds
    • C10N2010/04Groups 2 or 12
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    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/22Metal working with essential removal of material, e.g. cutting, grinding or drilling
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/24Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/241Manufacturing joint-less pipes
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/242Hot working
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/243Cold working
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/244Metal working of specific metals
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/244Metal working of specific metals
    • C10N2040/245Soft metals, e.g. aluminum
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/244Metal working of specific metals
    • C10N2040/246Iron or steel
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/244Metal working of specific metals
    • C10N2040/247Stainless steel
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    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00Form in which the lubricant is applied to the material being lubricated
    • C10N2050/015Dispersions of solid lubricants
    • C10N2050/02Dispersions of solid lubricants dissolved or suspended in a carrier which subsequently evaporates to leave a lubricant coating
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00Form in which the lubricant is applied to the material being lubricated
    • C10N2050/08Solids
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    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10Semi-solids; greasy
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    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10N2070/00Specific manufacturing methods for lubricant compositions

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Description

Verfahren zum Herstellen von Schmierkörpern zur Verwendung bei Warmstrangpressen von Stahlblöcken Es ist bekannt, zum Schmieren der Werkzeuge beim Warmstrangpressen von Stahlblöcken pulverförmige Schmierstoffe, wie Glaspulver, zu verwenden. Der an sich vorteilhaften - Verwendung glasartiger Schmiermittel in Pulverform steht im allgemeinen die Schwierigkeit entgegen; `dag Pulver in gleichmäßigen Schichten zwischen Preßblock und Matrize oder Preßstempel einzubringen. Besonders tritt diese Schwierigkeit beim waagerechten Strangpressen auf. Aus diesem Grund werden aus diesen pulverförmigen Schmierstoffen Formkörper hergestellt, z. B. Scheiben oder Ringe, und zwar durch Agglomerieren der Pulver oder unter Verwendung eines Bindemittels. Diese Formkörper gewährleisten die Ausbildung eines gleichmäßigen Schmierfilmes.Process for the production of lubricants for use in hot extrusion of steel blocks It is known to lubricate the tools during hot extrusion to use powdered lubricants such as glass powder from steel blocks. Of the Advantageous in itself - use of vitreous lubricants in powder form generally opposed to the difficulty; `dag powder in even layers to be introduced between the press block and die or ram. Especially this occurs Difficulty in horizontal extrusion. Because of this, these become powdered lubricants molded bodies produced, for. B. discs or rings, by agglomerating the powders or using a binder. These molded bodies ensure the formation of a uniform lubricating film.

In einem neuen, noch nicht bekanntgewordenen Vorschlag wird die Verwendung von Salzen oder Salzgemischen zum Schmieren beim Strangpressen von Stahl empfohlen, die einen Unwandlungspunkt aufweisen und die vor ihrem Gebrauch als Schmiermittel auf eine bei oder über dem Umwandlungspunkt liegende Temperatur erhitzt worden sind.In a new, not yet known proposal, the use of of salts or salt mixtures recommended for lubrication when extruding steel, which have a transformation point and which are prior to their use as lubricants have been heated to a temperature at or above the transition point.

Gegenstand der Erfindung ist ein Verfahren zum Herstellen von Schmierkörpern, wie Scheiben oder Ringen, durch Zusammensintern pulverförmiger Schmierstoffe für das Warmstrangpressen von Stahlblöcken, das erfindungsgemäß darin besteht, daß ein Gemisch aus pulverförmigem Alkalikarbonat oder -halogenid und 0,5 bis 5 Gewichtsprozent, vorzugsweise 0,3 bis 3 Gewichtsprozent, eines Salzes mit niedrigerem Schmelzpunkt, z. B. Natriumnitrat, in an sich bekannter Weise unter leichtem Druck bei Raumtemperatur in eine Form gepreßt und hierin bei einer Temperatur zwischen 400 und 800° C, vorzugsweise zwischen 550 und 600° C, gesintert wird.The invention relates to a method for producing lubricating bodies, like discs or rings, by sintering together powdered lubricants for the hot extrusion of steel blocks, which according to the invention consists in that a Mixture of powdered alkali carbonate or halide and 0.5 to 5 percent by weight, preferably 0.3 to 3 percent by weight, of a salt with a lower melting point, z. B. sodium nitrate, in a known manner under slight pressure at room temperature pressed into a mold and stored therein at a temperature between 400 and 800 ° C, preferably between 550 and 600 ° C, is sintered.

Eine Ausführungsform dieses Verfahrens besteht darin, daß eine Mischung von pulverförmigem Alkalikarbonat oder Alkalihalogenid und einer pulverisierten Schmelze einer aus verschiedenen Alkalisalzen, vorzugsweise aus Natrium- und Kaliumkarbonat, bestehenden eutektischen Verbindung gesintert wird. Schließlich kann auch eine Mischung gesintert werden, die 3 bis 5 Gewichtsprozent Wasser enthält.One embodiment of this method is that a mixture of powdered alkali carbonate or alkali halide and a powdered one Melt one of various alkali salts, preferably sodium and potassium carbonate, existing eutectic connection is sintered. Finally, it can also be a mixture be sintered, which contains 3 to 5 weight percent water.

Gegenüber den aus Glaspulver gesinterten Schmierscheiben weisen die nach dem erfindungsgemäßen Verfahren hergestellten Schmierkörper folgende besondere Wirkungen auf: Der Reibungsbeiwert beim Strangpressen beträgt nur etwa 50 bis 70% des bei Glasschmierung auftretenden Wertes. Die Preßkraft ist somit geringer, so daß größere Streckungen oder Preßgeschwindigkeiten möglich sind. Der Schmierfilm ist dünner.Compared to the grease washers sintered from glass powder, the The following special lubricants produced by the process according to the invention Effects on: The coefficient of friction during extrusion is only around 50 to 70% the value that occurs when the glass is smeared. The pressing force is therefore lower, see above that greater stretching or pressing speeds are possible. The lubricating film is thinner.

Die Oberfläche des Stranges ist glatter. (Bei Glas tritt meist die sogenannte »Apfelsinenhaut« auf.) Der Schmierfilm ist wasserlöslich und quantitativ z. B. durch Abspritzen mit Wasser entfernbar, was bei einer Schmierung mit Glas bekanntlich große Schwierigkeiten bereitet.The surface of the strand is smoother. (In the case of glass, the so-called »orange skin«.) The lubricating film is water-soluble and quantitative z. B. removable by spraying with water, which is when lubricated with glass known to cause great difficulties.

Beim Rückzug des Stempelkopfes aus dem Rezipienten tritt kein Verklemmen auf, da der Salzfilm sehr weich ist.When the stamp head is withdrawn from the recipient, there is no jamming because the salt film is very soft.

Gegenüber dem bekannten Vorschlag, Karbonate unter hohem Druck in die Strangpresse einzupressen, um das Ankleben des Werkstoffes an der Matrize bzw. am Dorn zu vermeiden, ist der Erfindungsgedanke, eine gesinterte Salzscheibe einzusetzen, leichter durchführbar, denn das bekannte Verfahren arbeitet mit flüssigen Karbonaten, was einen großen Aufwand an Heiz- und Druckaggregaten erfordert.Compared to the well-known proposal to use carbonates under high pressure in press in the extrusion press to prevent the material from sticking to the die or to avoid on the mandrel, the idea of the invention is to use a sintered salt disc, easier to carry out, because the known method works with liquid carbonates, which requires a lot of heating and pressure units.

Zur Schmierung von Pilgerdornen wurde Karbonat als Pulver aufgegeben. Ein Pulver ist bei horizontalen Strangpressen nicht anwendbar.Carbonate was used as a powder to lubricate pilgrim thorns. A powder cannot be used in horizontal extrusion presses.

Die nach dem erfindungsgemäßen Verfahren hergestellten Ringe oder Scheiben weisen nach dem Pressen und Sintern eine gute Haltbarkeit auf, was darauf zurückzuführen ist, daß die Festigkeit der Formkörper durch den Zusatz einer geringen Menge des niedriger schmelzenden Salzes um das Drei- bis Vierfache erhöht wird.The rings produced by the process according to the invention or After pressing and sintering, discs have a good shelf life, which is important is due to the fact that the strength of the molded body by the addition of a low Amount of lower melting salt is increased by three to four times.

Für den Fall, daß die Masse beim Sintern zu wenig schrumpfen sollte, klebt sie in der Preßform fest. Es hat sich gezeigt, daß die gesinterten Ringe oder Scheiben sich leicht aus der Form lösen und auch unbegrenzt gelagert werden können, wenn die Formkörper ein Porenvolumen von etwa 30 % aufweisen. Die gewünschte Dichte kann durch Mischen von feinem und grobem Alkalikarbonatpulver hergestellt werden.In the event that the mass should shrink too little during sintering, it sticks in the mold. It has been shown to be the sintered Rings or discs can easily be removed from the mold and can also be stored indefinitely can be if the shaped bodies have a pore volume of about 30%. the Desired density can be achieved by mixing fine and coarse alkali carbonate powder getting produced.

Werden z. B. etwa zwei Drittel grobkörnige (»schwere«) Soda mit einem Drittel feinkörniger (»leichter«) Soda unter Zugabe von etwa 3 Gewichtsprozent Natriumnitrat gemischt, so werden Formkörper erhalten, die nach dem Brennen sehr gut haltbar sind. weise 0,3 bis 3 Gewichtsprozent, eines Salzes mit niedrigerem Schmelzpunkt, z. B. Natriumnitrat, in an sich bekannter Weise unter leichtem Druck bei Raumtemperatur in eine Form gepreßt und hierin bei einer Temperatur zwischen 400 und 800° C, vorzugsweise zwischen 550 und 600° C, gesintert wird.Are z. B. about two-thirds of coarse-grained ("heavy") soda with a Third fine-grain ("lighter") soda with the addition of about 3 percent by weight sodium nitrate mixed, moldings are obtained which are very durable after firing. wise 0.3 to 3 percent by weight, of a salt with a lower melting point, e.g. B. Sodium nitrate, in a manner known per se, under slight pressure at room temperature pressed into a mold and stored therein at a temperature between 400 and 800 ° C, preferably between 550 and 600 ° C, is sintered.

2. Verfahren nach Anspruch 1, dadurch gekennzeichnet, daß eine Mischung von pulverförmigem Alkalikarbonat oder Alkalihalogenid und einer pulverisierten Schmelze einer aus verschiedenen Alkalisalzen, vorzugsweise aus Natrium- und Kaliumkarbonat, bestehenden eutektischen Verbindung gesintert wird.2. The method according to claim 1, characterized in that a mixture of powdered alkali carbonate or alkali halide and a powdered one Melt one of various alkali salts, preferably sodium and potassium carbonate, existing eutectic connection is sintered.

3. Verfahren nach den Ansprüchen 1 und 2, dadurch gekennzeichnet, daß eine Mischung gesintert wird, die 3 bis 5 Gewichtsprozent Wasser enthält.3. The method according to claims 1 and 2, characterized in that that a mixture is sintered which contains 3 to 5 percent by weight of water.

Claims (1)

Patentansprüche: 1. Verfahren zum Herstellen von Schmierkörpern, -wie Scheiben oder Ringen, durch Zusammensintern pulverförmiger Schmierstoffe für das Wärmstrangpressen von Stahlblöcken, d a -durch gekennzeichnet, daß ein Gemisch aus pulverförmigem Alkalikarbonat oder -halogenid und 0,5 bis 5 Gewichtsprozent, vorzugs-In Betracht gezogene Druckschriften: Deutsche Patentschrift Nr. 570 948; britische Patentschriften Nr. 795 889, 903 957.Claims: 1. A method for producing lubricating bodies, -like Discs or rings, by sintering together powdered lubricants for the Hot extrusion of steel blocks, d a -characterized in that a mixture of powdered alkali carbonate or halide and 0.5 to 5 percent by weight, preferably In Documents considered: German Patent No. 570 948; British Patent Nos. 795 889, 903 957.
DEM60706A 1964-03-20 1964-04-21 Method of manufacturing lubricants for use in hot extrusion of steel blocks Pending DE1228016B (en)

Priority Applications (10)

Application Number Priority Date Filing Date Title
DEM60373A DE1204767B (en) 1964-03-20 1964-03-20 Use of salts or mixtures of salts to lubricate when extruding steel
DEM60706A DE1228016B (en) 1964-04-21 1964-04-21 Method of manufacturing lubricants for use in hot extrusion of steel blocks
DE19651594495 DE1594495A1 (en) 1964-03-20 1965-01-26 Process for the manufacture of a lubricant for the extrusion of steel blocks
AT205565A AT257794B (en) 1964-03-20 1965-03-08 Process for lubricating during hot working of metals and for producing a lubricant
NL6503091A NL6503091A (en) 1964-03-20 1965-03-11
ES0310730A ES310730A1 (en) 1964-03-20 1965-03-18 A procedure for the lubrication in the hot deformation of metals, especially in the extrusion of steel. (Machine-translation by Google Translate, not legally binding)
GB11798/65A GB1107183A (en) 1964-03-20 1965-03-19 Lubrication method for the hot working of metals
SE03574/65A SE325981B (en) 1964-03-20 1965-03-19
FR10086A FR1448029A (en) 1964-03-20 1965-03-20 Lubrication process during heat forming of metals
BE661471D BE661471A (en) 1964-03-20 1965-03-22

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEM60706A DE1228016B (en) 1964-04-21 1964-04-21 Method of manufacturing lubricants for use in hot extrusion of steel blocks

Publications (1)

Publication Number Publication Date
DE1228016B true DE1228016B (en) 1966-11-03

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DEM60706A Pending DE1228016B (en) 1964-03-20 1964-04-21 Method of manufacturing lubricants for use in hot extrusion of steel blocks

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE570948C (en) * 1931-11-13 1933-02-22 Mannesmann Ag Method of lubricating pilgrim thorns
GB795889A (en) * 1954-09-14 1958-06-04 Fmc Corp Preparation of peracetic acid
GB903957A (en) * 1960-02-03 1962-08-22 Ti Group Services Ltd Lubrication of hot deformation processes on metals

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE570948C (en) * 1931-11-13 1933-02-22 Mannesmann Ag Method of lubricating pilgrim thorns
GB795889A (en) * 1954-09-14 1958-06-04 Fmc Corp Preparation of peracetic acid
GB903957A (en) * 1960-02-03 1962-08-22 Ti Group Services Ltd Lubrication of hot deformation processes on metals

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