DE10336164A1 - Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren durch Schmelzkondensation - Google Patents

Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren durch Schmelzkondensation Download PDF

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Publication number
DE10336164A1
DE10336164A1 DE10336164A DE10336164A DE10336164A1 DE 10336164 A1 DE10336164 A1 DE 10336164A1 DE 10336164 A DE10336164 A DE 10336164A DE 10336164 A DE10336164 A DE 10336164A DE 10336164 A1 DE10336164 A1 DE 10336164A1
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Germany
Prior art keywords
polymers
continuous production
melt condensation
polycondensation
precondensation
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Granted
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DE10336164A
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English (en)
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DE10336164B4 (de
Inventor
Rudolf Kaempf
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Lurgi Zimmer GmbH
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ZiAG Plant Engineering GmbH
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Filing date
Publication date
Priority to DE10336164A priority Critical patent/DE10336164B4/de
Application filed by ZiAG Plant Engineering GmbH filed Critical ZiAG Plant Engineering GmbH
Priority to KR1020067002416A priority patent/KR20060128819A/ko
Priority to EP04734836A priority patent/EP1654303A1/de
Priority to JP2006522242A priority patent/JP2007533769A/ja
Priority to EA200600195A priority patent/EA009105B1/ru
Priority to CNA2004800226252A priority patent/CN1867616A/zh
Priority to US10/569,846 priority patent/US20070112173A1/en
Priority to PCT/EP2004/005653 priority patent/WO2005023905A1/de
Publication of DE10336164A1 publication Critical patent/DE10336164A1/de
Application granted granted Critical
Publication of DE10336164B4 publication Critical patent/DE10336164B4/de
Priority to IL173217A priority patent/IL173217A0/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C08G63/785—Preparation processes characterised by the apparatus used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/04—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/26—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
    • C08G69/28—Preparatory processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G75/00—Macromolecular compounds obtained by reactions forming a linkage containing sulfur with or without nitrogen, oxygen, or carbon in the main chain of the macromolecule
    • C08G75/20—Polysulfones
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G79/00—Macromolecular compounds obtained by reactions forming a linkage containing atoms other than silicon, sulfur, nitrogen, oxygen, and carbon with or without the latter elements in the main chain of the macromolecule
    • C08G79/02—Macromolecular compounds obtained by reactions forming a linkage containing atoms other than silicon, sulfur, nitrogen, oxygen, and carbon with or without the latter elements in the main chain of the macromolecule a linkage containing phosphorus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00184—Controlling or regulating processes controlling the weight of reactants in the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00768—Baffles attached to the reactor wall vertical

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)

Abstract

Bei einem Verfahren zur kontinuierlichen Herstellung von Polymeren durch Schmelzkondensation eines Monomeren jeweils mit sich selbst oder mit mindestens einem anderen Monomeren werden die aufgeschmolzenen Monomeren in Gegenwart eines Katalysators ver- bzw. umgeestert, anschließend wird das Ver-/Umesterungsprodukt zur Vorkondensation einem Ringscheibenreaktor, dananch das Vorkondensationsprodukt einem LVS-Ringscheibenreaktor zur Polykondensation und abschließend das Polykondensationsprodukt einem HVS-Ringscheibenreaktor zur End-Polykondensation aufgegeben.
DE10336164A 2003-08-07 2003-08-07 Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren durch Schmelzkondensation Expired - Lifetime DE10336164B4 (de)

Priority Applications (9)

Application Number Priority Date Filing Date Title
DE10336164A DE10336164B4 (de) 2003-08-07 2003-08-07 Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren durch Schmelzkondensation
EP04734836A EP1654303A1 (de) 2003-08-07 2004-05-26 Verfahren und vorrichtung zur kontinuierlichen herstellung von polymeren durch schmelzkondensation
JP2006522242A JP2007533769A (ja) 2003-08-07 2004-05-26 溶融縮合によるポリマーの連続製造のための方法及び装置
EA200600195A EA009105B1 (ru) 2003-08-07 2004-05-26 Способ и устройство для непрерывного получения полимеров путем конденсации в расплаве
KR1020067002416A KR20060128819A (ko) 2003-08-07 2004-05-26 용융 축합을 통한 폴리머의 연속 생산을 위한 방법 및 장치
CNA2004800226252A CN1867616A (zh) 2003-08-07 2004-05-26 通过熔融缩合而连续制备聚合物的方法和装置
US10/569,846 US20070112173A1 (en) 2003-08-07 2004-05-26 Method and device for the continuous production of polymer
PCT/EP2004/005653 WO2005023905A1 (de) 2003-08-07 2004-05-26 Verfahren und vorrichtung zur kontinuierlichen herstellung von polymeren durch schmelzkondensation
IL173217A IL173217A0 (en) 2003-08-07 2006-01-18 Method and device for the continuous production of polymers by melt condensation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10336164A DE10336164B4 (de) 2003-08-07 2003-08-07 Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren durch Schmelzkondensation

Publications (2)

Publication Number Publication Date
DE10336164A1 true DE10336164A1 (de) 2005-03-10
DE10336164B4 DE10336164B4 (de) 2005-08-25

Family

ID=34177344

Family Applications (1)

Application Number Title Priority Date Filing Date
DE10336164A Expired - Lifetime DE10336164B4 (de) 2003-08-07 2003-08-07 Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Polymeren durch Schmelzkondensation

Country Status (9)

Country Link
US (1) US20070112173A1 (de)
EP (1) EP1654303A1 (de)
JP (1) JP2007533769A (de)
KR (1) KR20060128819A (de)
CN (1) CN1867616A (de)
DE (1) DE10336164B4 (de)
EA (1) EA009105B1 (de)
IL (1) IL173217A0 (de)
WO (1) WO2005023905A1 (de)

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008073254A2 (en) * 2006-12-07 2008-06-19 Eastman Chemical Company Polyester production system employing short residence time esterification
WO2008073288A2 (en) * 2006-12-07 2008-06-19 Eastman Chemical Company Polyester production system employing horizontally elongated esterification vessel
US7649109B2 (en) 2006-12-07 2010-01-19 Eastman Chemical Company Polyester production system employing recirculation of hot alcohol to esterification zone
US7718759B2 (en) 2000-12-07 2010-05-18 Eastman Chemical Company Polyester process using a pipe reactor
US7829653B2 (en) 2007-07-12 2010-11-09 Eastman Chemical Company Horizontal trayed reactor
US7842777B2 (en) 2007-07-12 2010-11-30 Eastman Chemical Company Sloped tubular reactor with divided flow
US7847053B2 (en) 2007-07-12 2010-12-07 Eastman Chemical Company Multi-level tubular reactor with oppositely extending segments
US7858730B2 (en) 2007-07-12 2010-12-28 Eastman Chemical Company Multi-level tubular reactor with dual headers
US7863477B2 (en) 2007-03-08 2011-01-04 Eastman Chemical Company Polyester production system employing hot paste to esterification zone
US7868130B2 (en) 2007-07-12 2011-01-11 Eastman Chemical Company Multi-level tubular reactor with vertically spaced segments
US7868129B2 (en) 2007-07-12 2011-01-11 Eastman Chemical Company Sloped tubular reactor with spaced sequential trays
US7872090B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Reactor system with optimized heating and phase separation
US7872089B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Multi-level tubular reactor with internal tray
US7892498B2 (en) 2007-03-08 2011-02-22 Eastman Chemical Company Polyester production system employing an unagitated esterification reactor

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102004034708B4 (de) * 2004-07-17 2008-04-10 Lurgi Zimmer Gmbh Verfahren zur absatzweisen Herstellung von Polymeren durch Schmelzekondensation
US7834109B2 (en) * 2007-12-07 2010-11-16 Eastman Chemical Company System for producing low impurity polyester
DE102008000432A1 (de) * 2008-02-28 2009-09-03 Evonik Röhm Gmbh Rührkesselreaktor sowie Verfahren zur Durchführung einer Polymerisationsreaktion unter Verwendung eines solchen Rührkesselreaktors
KR102184849B1 (ko) * 2017-10-12 2020-12-01 가부시끼가이샤 구레하 중합체의 연속 제조 장치 및 연속 제조 방법
CN109806814B (zh) * 2019-03-11 2021-08-20 安庆市虹泰新材料有限责任公司 一种二聚酸生产用固定床反应器
WO2020204558A1 (ko) * 2019-04-04 2020-10-08 주식회사 엘지화학 에스터계 조성물의 제조방법 및 제조 시스템
US11512166B2 (en) 2019-04-04 2022-11-29 Lg Chem, Ltd. Method and system for manufacturing ester-based composition
CN114656638B (zh) * 2022-03-03 2024-06-25 万华化学集团股份有限公司 一种聚砜的连续化合成方法及装置
CN114832763A (zh) * 2022-04-20 2022-08-02 阜阳市金地橡塑股份有限公司 一种防老化剂ble生产用原料混料机

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3544551C2 (de) * 1985-12-17 2002-02-28 Zimmer Ag Verfahren zur kontinuierlichen Herstellung von hochmolekularem Polybutylenterephthalat
DE10001477B4 (de) * 2000-01-15 2005-04-28 Zimmer Ag Diskontinuierliches Polykondensationsverfahren und Rührscheibenreaktor hierfür
DE10059616A1 (de) * 2000-12-01 2002-06-06 Zimmer Ag Verfahren zum Erzeugen von Polycarbonaten
DE10219671A1 (de) * 2002-05-02 2003-11-20 Zimmer Ag Verfahren und Vorrichtung zur Herstellung von Polyestern, Copolyestern und Polycarbonaten
DE10322106B4 (de) * 2003-05-09 2006-05-11 Aquafil Engineering Gmbh Verfahren und Reaktor zur kontinuierlichen Herstellung von Polymeren

Cited By (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7718759B2 (en) 2000-12-07 2010-05-18 Eastman Chemical Company Polyester process using a pipe reactor
US7842778B2 (en) 2000-12-07 2010-11-30 Eastman Chemical Company Polyester process using a pipe reactor
US8114954B2 (en) 2000-12-07 2012-02-14 Grupo Petrotemex, S.A. De C.V. Polyester process using a pipe reactor
WO2008073288A2 (en) * 2006-12-07 2008-06-19 Eastman Chemical Company Polyester production system employing horizontally elongated esterification vessel
WO2008073254A3 (en) * 2006-12-07 2008-08-14 Eastman Chem Co Polyester production system employing short residence time esterification
WO2008073288A3 (en) * 2006-12-07 2008-08-21 Eastman Chem Co Polyester production system employing horizontally elongated esterification vessel
US7649109B2 (en) 2006-12-07 2010-01-19 Eastman Chemical Company Polyester production system employing recirculation of hot alcohol to esterification zone
US8470250B2 (en) 2006-12-07 2013-06-25 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
US7943094B2 (en) 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
WO2008073254A2 (en) * 2006-12-07 2008-06-19 Eastman Chemical Company Polyester production system employing short residence time esterification
US7892498B2 (en) 2007-03-08 2011-02-22 Eastman Chemical Company Polyester production system employing an unagitated esterification reactor
US7863477B2 (en) 2007-03-08 2011-01-04 Eastman Chemical Company Polyester production system employing hot paste to esterification zone
US7858730B2 (en) 2007-07-12 2010-12-28 Eastman Chemical Company Multi-level tubular reactor with dual headers
US7868129B2 (en) 2007-07-12 2011-01-11 Eastman Chemical Company Sloped tubular reactor with spaced sequential trays
US7872090B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Reactor system with optimized heating and phase separation
US7872089B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Multi-level tubular reactor with internal tray
US7868130B2 (en) 2007-07-12 2011-01-11 Eastman Chemical Company Multi-level tubular reactor with vertically spaced segments
US7847053B2 (en) 2007-07-12 2010-12-07 Eastman Chemical Company Multi-level tubular reactor with oppositely extending segments
US7842777B2 (en) 2007-07-12 2010-11-30 Eastman Chemical Company Sloped tubular reactor with divided flow
US7829653B2 (en) 2007-07-12 2010-11-09 Eastman Chemical Company Horizontal trayed reactor

Also Published As

Publication number Publication date
IL173217A0 (en) 2006-06-11
DE10336164B4 (de) 2005-08-25
EA009105B1 (ru) 2007-10-26
CN1867616A (zh) 2006-11-22
JP2007533769A (ja) 2007-11-22
KR20060128819A (ko) 2006-12-14
EP1654303A1 (de) 2006-05-10
WO2005023905A1 (de) 2005-03-17
EA200600195A1 (ru) 2006-08-25
US20070112173A1 (en) 2007-05-17

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Owner name: LURGI ZIMMER GMBH, 60388 FRANKFURT, DE

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