DE102011109454A1 - Verfahren zur Behandlung von Produktfluidströmen - Google Patents

Verfahren zur Behandlung von Produktfluidströmen Download PDF

Info

Publication number
DE102011109454A1
DE102011109454A1 DE102011109454A DE102011109454A DE102011109454A1 DE 102011109454 A1 DE102011109454 A1 DE 102011109454A1 DE 102011109454 A DE102011109454 A DE 102011109454A DE 102011109454 A DE102011109454 A DE 102011109454A DE 102011109454 A1 DE102011109454 A1 DE 102011109454A1
Authority
DE
Germany
Prior art keywords
range
nitrogen
reaction
inert gas
product fluid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE102011109454A
Other languages
German (de)
English (en)
Inventor
Armin Brenner
Josef Find
Alfred Haas
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HTE GmbH the High Throughput Experimentation Co
Original Assignee
HTE GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HTE GmbH filed Critical HTE GmbH
Priority to DE102011109454A priority Critical patent/DE102011109454A1/de
Priority to PCT/EP2012/064850 priority patent/WO2013017556A1/de
Priority to US14/236,994 priority patent/US9708553B2/en
Priority to JP2014523296A priority patent/JP6324890B2/ja
Priority to EP12743437.1A priority patent/EP2739387B1/de
Priority to CN201280038507.5A priority patent/CN103781542B/zh
Publication of DE102011109454A1 publication Critical patent/DE102011109454A1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G65/00Treatment of hydrocarbon oils by two or more hydrotreatment processes only
    • C10G65/14Treatment of hydrocarbon oils by two or more hydrotreatment processes only plural parallel stages only
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G29/00Refining of hydrocarbon oils, in the absence of hydrogen, with other chemicals
    • C10G29/02Non-metals
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/22Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing with hydrogen dissolved or suspended in the oil
    • CCHEMISTRY; METALLURGY
    • C40COMBINATORIAL TECHNOLOGY
    • C40BCOMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B30/00Methods of screening libraries
    • C40B30/08Methods of screening libraries by measuring catalytic activity
    • CCHEMISTRY; METALLURGY
    • C40COMBINATORIAL TECHNOLOGY
    • C40BCOMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B60/00Apparatus specially adapted for use in combinatorial chemistry or with libraries
    • C40B60/12Apparatus specially adapted for use in combinatorial chemistry or with libraries for screening libraries
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00279Features relating to reactor vessels
    • B01J2219/00281Individual reactor vessels
    • B01J2219/00286Reactor vessels with top and bottom openings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00279Features relating to reactor vessels
    • B01J2219/00306Reactor vessels in a multiple arrangement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00351Means for dispensing and evacuation of reagents
    • B01J2219/00389Feeding through valves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00351Means for dispensing and evacuation of reagents
    • B01J2219/00418Means for dispensing and evacuation of reagents using pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00477Means for pressurising the reaction vessels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00495Means for heating or cooling the reaction vessels
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583Features relative to the processes being carried out
    • B01J2219/00585Parallel processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068Means for controlling the apparatus of the process
    • B01J2219/00698Measurement and control of process parameters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068Means for controlling the apparatus of the process
    • B01J2219/00702Processes involving means for analysing and characterising the products
    • B01J2219/00707Processes involving means for analysing and characterising the products separated from the reactor apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718Type of compounds synthesised
    • B01J2219/0072Organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718Type of compounds synthesised
    • B01J2219/00745Inorganic compounds
    • B01J2219/00747Catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Molecular Biology (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DE102011109454A 2011-08-04 2011-08-04 Verfahren zur Behandlung von Produktfluidströmen Withdrawn DE102011109454A1 (de)

Priority Applications (6)

Application Number Priority Date Filing Date Title
DE102011109454A DE102011109454A1 (de) 2011-08-04 2011-08-04 Verfahren zur Behandlung von Produktfluidströmen
PCT/EP2012/064850 WO2013017556A1 (de) 2011-08-04 2012-07-30 Verfahren zur behandlung von produktfluidströmen
US14/236,994 US9708553B2 (en) 2011-08-04 2012-07-30 Method for handling product fluid flows
JP2014523296A JP6324890B2 (ja) 2011-08-04 2012-07-30 生成流体の流動制御方法
EP12743437.1A EP2739387B1 (de) 2011-08-04 2012-07-30 Verfahren zur behandlung von produktfluidströmen
CN201280038507.5A CN103781542B (zh) 2011-08-04 2012-07-30 处理产物流体物流的方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102011109454A DE102011109454A1 (de) 2011-08-04 2011-08-04 Verfahren zur Behandlung von Produktfluidströmen

Publications (1)

Publication Number Publication Date
DE102011109454A1 true DE102011109454A1 (de) 2013-02-07

Family

ID=46614474

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102011109454A Withdrawn DE102011109454A1 (de) 2011-08-04 2011-08-04 Verfahren zur Behandlung von Produktfluidströmen

Country Status (6)

Country Link
US (1) US9708553B2 (enExample)
EP (1) EP2739387B1 (enExample)
JP (1) JP6324890B2 (enExample)
CN (1) CN103781542B (enExample)
DE (1) DE102011109454A1 (enExample)
WO (1) WO2013017556A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102013016585A1 (de) * 2013-10-08 2015-04-09 Hte Gmbh The High Throughput Experimentation Company Apparatur und Verfahren zur Untersuchung von diskontinuierllichen Produktfluidströmen bei der Umsetzung von Eduktfluidströmen an Feststoffkatalysatoren

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19855910A1 (de) * 1998-12-03 2000-06-08 Basf Ag Spülvorrichtung zur Entfernung von Rückständen
WO2005063372A2 (en) 2003-12-23 2005-07-14 Hte Aktiengesellschaft The High Throughput Experimentation Company Device and method for pressure and flow control in parallel reactors
WO2006107187A1 (en) 2005-04-04 2006-10-12 Avantium International B.V. System and method for performing a chemical experiment
DE102006034172B3 (de) * 2006-07-24 2007-09-20 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur Handhabung von Multikomponenten-Gemischen
DE102006053078A1 (de) * 2006-11-10 2008-05-15 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur kontinuierlichen Überführung und Analyse von Fluiden

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2795512B1 (fr) 1999-06-28 2001-08-03 Inst Francais Du Petrole Methode et dispositif multi-reacteurs automatique d'evaluation de catalyseurs avec analyse en ligne sans separation liquide/gaz
EP1256377A1 (en) * 2001-05-11 2002-11-13 Avantium International B.V. Apparatus, suitable for high throughput experimentation
US20030173205A1 (en) * 2002-03-12 2003-09-18 Arne Karlsson Process vessel with integral evaporator
WO2008080365A1 (en) * 2006-12-29 2008-07-10 Accelergy Shanghai R & D Center Co., Ltd. High throughput development method for catalytic hydroprocessing of dirty feedstocks
EP2334428B1 (en) * 2007-11-28 2018-04-04 Chevron U.S.A., Inc. Process for recovering base metals from used hydroprocessing catalyst

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19855910A1 (de) * 1998-12-03 2000-06-08 Basf Ag Spülvorrichtung zur Entfernung von Rückständen
WO2005063372A2 (en) 2003-12-23 2005-07-14 Hte Aktiengesellschaft The High Throughput Experimentation Company Device and method for pressure and flow control in parallel reactors
WO2006107187A1 (en) 2005-04-04 2006-10-12 Avantium International B.V. System and method for performing a chemical experiment
DE102006034172B3 (de) * 2006-07-24 2007-09-20 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur Handhabung von Multikomponenten-Gemischen
WO2008012073A1 (de) 2006-07-24 2008-01-31 Hte Aktiengesellschaft The High Throughput Experimentation Company Vorrichtung und ein verfahren zur handhabung von multikomponenten-gemischen
DE102006053078A1 (de) * 2006-11-10 2008-05-15 Hte Ag The High Throughput Experimentation Company Vorrichtung und Verfahren zur kontinuierlichen Überführung und Analyse von Fluiden
WO2008055585A1 (de) 2006-11-10 2008-05-15 Hte Aktiengesellschaft The High Throughput Experimentation Company Vorrichtung und verfahren zur kontinuierlichen überführung und analyse von fluiden

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102013016585A1 (de) * 2013-10-08 2015-04-09 Hte Gmbh The High Throughput Experimentation Company Apparatur und Verfahren zur Untersuchung von diskontinuierllichen Produktfluidströmen bei der Umsetzung von Eduktfluidströmen an Feststoffkatalysatoren

Also Published As

Publication number Publication date
CN103781542B (zh) 2017-02-15
JP2014524486A (ja) 2014-09-22
EP2739387B1 (de) 2024-02-21
US20140174987A1 (en) 2014-06-26
JP6324890B2 (ja) 2018-05-16
EP2739387A1 (de) 2014-06-11
WO2013017556A1 (de) 2013-02-07
US9708553B2 (en) 2017-07-18
CN103781542A (zh) 2014-05-07

Similar Documents

Publication Publication Date Title
DE102019133911B4 (de) Verfahren zur Co-Verarbeitung
DE112007001743T5 (de) Hydrocracking-Verfahren
DE69030758T2 (de) Verfahren zur Verminderung von H2S in Asphalt
DE60122210T2 (de) Verbessertes flexibles verfahren zur herstellung von grundölen und destillaten durch hydroisomerisierung-konversion an einem schwach dispergierten katalysator und anschliessende katalytische entparaffinierung
EP3242923B1 (de) Apparatur und verfahren zur untersuchung von naphtha-reformierunsprozessen
EP3703849B1 (de) Vorrichtung und verfahren zur charakterisierung von katalytischen prozessen
DE69902275T2 (de) Integriertes verfahren zur umwandlung von erdgas und erdgaskondensat zu hochwertigen produkten
DE1770264A1 (de) Verfahren zur Reinigung von Erdoel
DE102011109454A1 (de) Verfahren zur Behandlung von Produktfluidströmen
DE69117433T2 (de) Hydrodenitrifizierungsverfahren
DE2148155C3 (de) Verfahren zur Sulfidierung von Katalysatoren für die hydrierende Verarbeitung von Kohlenwasserstoffen und deren Verwendung zur hydrierenden Umwandlung von Kohlenwasserstoffen
EP2325632B1 (de) Verfahren zur Sauerstoffelementaranalyse und zur Sauerstoffisotopenmessung stickstoffhaltiger, organischer Substanzen
DE102013016585A1 (de) Apparatur und Verfahren zur Untersuchung von diskontinuierllichen Produktfluidströmen bei der Umsetzung von Eduktfluidströmen an Feststoffkatalysatoren
AT509812B1 (de) Vorrichtung und verfahren zur künstlichen alterung eines fluids
DE10297760T5 (de) Verbessertes Hydrocrackverfahren
CH454808A (de) Verfahren zur Regenerierung eines mit Schwefel verunreinigten Katalysators
DE69302595T2 (de) Verfahren zur Aufarbeitung eines Kohlenwasserstoffeinsatzes
DE1645816C3 (de) Verfahren zum Hydrofinieren mit einhergehender Hydrokrackung von Kohlenwasserstoffgemischen
DE1950788A1 (de) Verfahren zur Entfernung von Eisenverunreinigungen aus Kohlenwasserstoffoelen
DE2055728C3 (enExample)
DE102011012445A1 (de) Verfahren zur Bestimmung des Gehalts an Schwefelwasserstoff in Roh- und Rückstandsölen
DE2017287A1 (de) Hydrocrack-Verfahren mit zwei Katalysatoren
DE2064394A1 (de) Aromatenarmes, im UV Wellenlängenbereich nur schwach absorbierendes Mineral olkohlenwasserstoffgemisch und Verfahren zu seiner Herstellung
DE2701105C3 (de) Verfahren zur katalytischen Behandlung von Kohlenwasserstoffen
AT234251B (de) Verfahren zur Herstellung von rohem Fliegerbenzin

Legal Events

Date Code Title Description
R163 Identified publications notified
R082 Change of representative

Representative=s name: WALLINGER RICKER SCHLOTTER TOSTMANN PATENT- UN, DE

R081 Change of applicant/patentee

Owner name: HTE GMBH THE HIGH THROUGHPUT EXPERIMENTATION C, DE

Free format text: FORMER OWNER: HTE AKTIENGESELLSCHAFT, 69123 HEIDELBERG, DE

Effective date: 20131126

R082 Change of representative

Representative=s name: WALLINGER RICKER SCHLOTTER TOSTMANN PATENT- UN, DE

Effective date: 20131126

R119 Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee

Effective date: 20140301