DD146183A5 - Verfahren zur gewinnung von cyanurchlorid(ii) - Google Patents
Verfahren zur gewinnung von cyanurchlorid(ii) Download PDFInfo
- Publication number
- DD146183A5 DD146183A5 DD215677A DD21567779A DD146183A5 DD 146183 A5 DD146183 A5 DD 146183A5 DD 215677 A DD215677 A DD 215677A DD 21567779 A DD21567779 A DD 21567779A DD 146183 A5 DD146183 A5 DD 146183A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- cyanuric chloride
- liquid
- chloride
- solid
- stripping column
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 30
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 claims abstract description 65
- 239000007788 liquid Substances 0.000 claims abstract description 32
- 239000007787 solid Substances 0.000 claims abstract description 24
- QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000011084 recovery Methods 0.000 claims abstract description 7
- 238000005829 trimerization reaction Methods 0.000 claims abstract description 7
- 230000007423 decrease Effects 0.000 claims abstract description 3
- 239000011541 reaction mixture Substances 0.000 claims abstract 5
- 239000007789 gas Substances 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 19
- 239000012495 reaction gas Substances 0.000 claims description 12
- 239000000460 chlorine Substances 0.000 claims description 10
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 7
- 229910052801 chlorine Inorganic materials 0.000 claims description 7
- 239000003990 capacitor Substances 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 2
- 230000005494 condensation Effects 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 239000000344 soap Substances 0.000 claims 1
- 230000008021 deposition Effects 0.000 abstract description 9
- 238000001816 cooling Methods 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 239000012265 solid product Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- JGZVUTYDEVUNMK-UHFFFAOYSA-N 5-carboxy-2',7'-dichlorofluorescein Chemical compound C12=CC(Cl)=C(O)C=C2OC2=CC(O)=C(Cl)C=C2C21OC(=O)C1=CC(C(=O)O)=CC=C21 JGZVUTYDEVUNMK-UHFFFAOYSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 125000004093 cyano group Chemical group *C#N 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/28—Only halogen atoms, e.g. cyanuric chloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treating Waste Gases (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2843381A DE2843381B2 (de) | 1978-10-05 | 1978-10-05 | Verfahren zur Gewinnung von Cyanurchlorid in fester und flüssiger Form |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD146183A5 true DD146183A5 (de) | 1981-01-28 |
Family
ID=6051426
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD215677A DD146183A5 (de) | 1978-10-05 | 1979-09-20 | Verfahren zur gewinnung von cyanurchlorid(ii) |
Country Status (23)
| Country | Link |
|---|---|
| US (1) | US4245091A (cs) |
| JP (1) | JPS5551074A (cs) |
| AT (1) | AT364370B (cs) |
| BE (1) | BE879181A (cs) |
| BR (1) | BR7905299A (cs) |
| CA (1) | CA1105018A (cs) |
| CH (1) | CH641787A5 (cs) |
| CS (1) | CS219906B2 (cs) |
| DD (1) | DD146183A5 (cs) |
| DE (1) | DE2843381B2 (cs) |
| ES (1) | ES481918A1 (cs) |
| FR (1) | FR2439776A1 (cs) |
| GB (1) | GB2035305B (cs) |
| HU (1) | HU182945B (cs) |
| IL (1) | IL58263A (cs) |
| IN (1) | IN153152B (cs) |
| IT (1) | IT1119120B (cs) |
| MX (1) | MX152745A (cs) |
| NL (1) | NL7904980A (cs) |
| RO (1) | RO77778A (cs) |
| SE (1) | SE446000B (cs) |
| YU (1) | YU40221B (cs) |
| ZA (1) | ZA794823B (cs) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10123072B4 (de) * | 2001-05-11 | 2004-12-30 | Degussa Ag | Vorrichtung zur Aufreinigung von Cyanurchlorid |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE599669A (fr) * | 1960-02-02 | 1961-05-16 | Lonza Usines Electr Et Chim Sa | Procédé de purification du chlorure de cyanuryle par distillation |
| US3256070A (en) * | 1960-10-12 | 1966-06-14 | Geigy Chem Corp | Desublimation using a rotating cooling drum containing particulate tumbling and grinding media |
| FR1411816A (fr) * | 1964-08-11 | 1965-09-24 | Electro Chimie Soc D | Procédé d'obtention de chlorure de cyanuryle purifié à partir de mélanges gazeux le contenant |
| GB1095454A (cs) | 1965-08-21 | |||
| US3539565A (en) * | 1968-01-29 | 1970-11-10 | Geigy Chem Corp | Method for producing a solution of cyanuric chloride from gaseous cyanuric chloride |
| CH534686A (de) * | 1970-02-13 | 1973-03-15 | Ciba Geigy Ag | Kontinuierliches Verfahren zur Herstellung von Cyanurchlorid |
| DD111378A5 (cs) * | 1973-06-27 | 1975-02-12 | ||
| DE2537673C2 (de) * | 1975-08-23 | 1977-09-29 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zur Herstellung von feinteiligem, festem Cyanurchlorid |
-
1978
- 1978-10-05 DE DE2843381A patent/DE2843381B2/de not_active Ceased
-
1979
- 1979-06-12 YU YU1376/76A patent/YU40221B/xx unknown
- 1979-06-26 ES ES481918A patent/ES481918A1/es not_active Expired
- 1979-06-26 NL NL7904980A patent/NL7904980A/nl not_active Application Discontinuation
- 1979-08-01 MX MX178732A patent/MX152745A/es unknown
- 1979-08-06 IT IT68619/79A patent/IT1119120B/it active
- 1979-08-17 BR BR7905299A patent/BR7905299A/pt not_active IP Right Cessation
- 1979-08-29 IN IN891/CAL/79A patent/IN153152B/en unknown
- 1979-09-12 ZA ZA00794823A patent/ZA794823B/xx unknown
- 1979-09-18 IL IL58263A patent/IL58263A/xx unknown
- 1979-09-20 DD DD215677A patent/DD146183A5/de not_active IP Right Cessation
- 1979-09-24 CS CS796449A patent/CS219906B2/cs unknown
- 1979-09-25 US US06/078,832 patent/US4245091A/en not_active Expired - Lifetime
- 1979-10-01 GB GB7933913A patent/GB2035305B/en not_active Expired
- 1979-10-03 BE BE6/46960A patent/BE879181A/fr not_active IP Right Cessation
- 1979-10-04 CA CA336,982A patent/CA1105018A/en not_active Expired
- 1979-10-04 AT AT0648879A patent/AT364370B/de not_active IP Right Cessation
- 1979-10-04 CH CH896479A patent/CH641787A5/de not_active IP Right Cessation
- 1979-10-04 HU HU79DE1016A patent/HU182945B/hu not_active IP Right Cessation
- 1979-10-04 SE SE7908236A patent/SE446000B/sv not_active IP Right Cessation
- 1979-10-05 RO RO7998862A patent/RO77778A/ro unknown
- 1979-10-05 JP JP12810079A patent/JPS5551074A/ja active Granted
- 1979-10-05 FR FR7924909A patent/FR2439776A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| FR2439776B1 (cs) | 1983-04-01 |
| IL58263A (en) | 1982-12-31 |
| IT7968619A0 (it) | 1979-08-06 |
| HU182945B (en) | 1984-03-28 |
| IN153152B (cs) | 1984-06-09 |
| RO77778A (ro) | 1982-02-26 |
| JPH0127067B2 (cs) | 1989-05-26 |
| BE879181A (fr) | 1980-04-03 |
| IL58263A0 (en) | 1979-12-30 |
| NL7904980A (nl) | 1980-04-09 |
| US4245091A (en) | 1981-01-13 |
| AT364370B (de) | 1981-10-12 |
| DE2843381B2 (de) | 1980-07-10 |
| GB2035305B (en) | 1983-03-23 |
| ZA794823B (en) | 1981-01-28 |
| MX152745A (es) | 1985-11-07 |
| SE446000B (sv) | 1986-08-04 |
| ATA648879A (de) | 1981-03-15 |
| CS219906B2 (en) | 1983-03-25 |
| CH641787A5 (de) | 1984-03-15 |
| ES481918A1 (es) | 1980-02-16 |
| GB2035305A (en) | 1980-06-18 |
| IT1119120B (it) | 1986-03-03 |
| JPS5551074A (en) | 1980-04-14 |
| YU137679A (en) | 1982-08-31 |
| CA1105018A (en) | 1981-07-14 |
| SE7908236L (sv) | 1980-04-06 |
| BR7905299A (pt) | 1980-04-29 |
| DE2843381A1 (de) | 1980-04-17 |
| FR2439776A1 (fr) | 1980-05-23 |
| YU40221B (en) | 1985-08-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ENJ | Ceased due to non-payment of renewal fee |