CS221545B2 - Method of obtaining the ammonia and carbon dioxide from the mixtures containing ammonium,carbon dioxide and water - Google Patents
Method of obtaining the ammonia and carbon dioxide from the mixtures containing ammonium,carbon dioxide and water Download PDFInfo
- Publication number
- CS221545B2 CS221545B2 CS802615A CS261580A CS221545B2 CS 221545 B2 CS221545 B2 CS 221545B2 CS 802615 A CS802615 A CS 802615A CS 261580 A CS261580 A CS 261580A CS 221545 B2 CS221545 B2 CS 221545B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- ammonia
- carbon dioxide
- separation
- zone
- water
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 110
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 71
- 229910001868 water Inorganic materials 0.000 title claims abstract description 66
- 238000000034 method Methods 0.000 title claims abstract description 58
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims description 428
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 title claims description 347
- 229910021529 ammonia Inorganic materials 0.000 title claims description 212
- 239000001569 carbon dioxide Substances 0.000 title claims description 173
- 229910002092 carbon dioxide Inorganic materials 0.000 title claims description 173
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 title claims description 21
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 title description 4
- 238000000926 separation method Methods 0.000 claims abstract description 134
- 230000008569 process Effects 0.000 claims abstract description 41
- 239000007791 liquid phase Substances 0.000 claims abstract description 38
- 238000003795 desorption Methods 0.000 claims abstract description 20
- 239000011261 inert gas Substances 0.000 claims abstract description 17
- 239000008246 gaseous mixture Substances 0.000 claims abstract description 16
- 239000007789 gas Substances 0.000 claims description 31
- 239000007788 liquid Substances 0.000 claims description 21
- 238000010586 diagram Methods 0.000 claims description 6
- 230000035945 sensitivity Effects 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 18
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 9
- 229910052799 carbon Inorganic materials 0.000 description 9
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 8
- 239000004202 carbamide Substances 0.000 description 8
- 238000010790 dilution Methods 0.000 description 7
- 239000012895 dilution Substances 0.000 description 7
- 238000003113 dilution method Methods 0.000 description 7
- 230000008901 benefit Effects 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 6
- 238000005265 energy consumption Methods 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 238000003786 synthesis reaction Methods 0.000 description 6
- 239000012071 phase Substances 0.000 description 5
- 229920000877 Melamine resin Polymers 0.000 description 4
- BVCZEBOGSOYJJT-UHFFFAOYSA-N ammonium carbamate Chemical group [NH4+].NC([O-])=O BVCZEBOGSOYJJT-UHFFFAOYSA-N 0.000 description 4
- KXDHJXZQYSOELW-UHFFFAOYSA-N carbonic acid monoamide Natural products NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
- 239000002689 soil Substances 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 229910002091 carbon monoxide Inorganic materials 0.000 description 2
- 230000006835 compression Effects 0.000 description 2
- 238000007906 compression Methods 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000007865 diluting Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- GSWAOPJLTADLTN-UHFFFAOYSA-N oxidanimine Chemical compound [O-][NH3+] GSWAOPJLTADLTN-UHFFFAOYSA-N 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- DBGIVFWFUFKIQN-UHFFFAOYSA-N (+-)-Fenfluramine Chemical compound CCNC(C)CC1=CC=CC(C(F)(F)F)=C1 DBGIVFWFUFKIQN-UHFFFAOYSA-N 0.000 description 1
- -1 0.3 why Chemical compound 0.000 description 1
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 1
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 1
- 241000238876 Acari Species 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- 108030001720 Bontoxilysin Proteins 0.000 description 1
- 229910052684 Cerium Inorganic materials 0.000 description 1
- 229940123973 Oxygen scavenger Drugs 0.000 description 1
- 241000534944 Thia Species 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- ZEYWAHILTZGZBH-UHFFFAOYSA-N azane;carbon dioxide Chemical compound N.O=C=O ZEYWAHILTZGZBH-UHFFFAOYSA-N 0.000 description 1
- 229910002056 binary alloy Inorganic materials 0.000 description 1
- CREMABGTGYGIQB-UHFFFAOYSA-N carbon carbon Chemical compound C.C CREMABGTGYGIQB-UHFFFAOYSA-N 0.000 description 1
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 210000005069 ears Anatomy 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000007792 gaseous phase Substances 0.000 description 1
- 238000009499 grossing Methods 0.000 description 1
- 210000003128 head Anatomy 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- OETHQSJEHLVLGH-UHFFFAOYSA-N metformin hydrochloride Chemical compound Cl.CN(C)C(=N)N=C(N)N OETHQSJEHLVLGH-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000002161 passivation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 210000001747 pupil Anatomy 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 238000001577 simple distillation Methods 0.000 description 1
- 230000003381 solubilizing effect Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- ZZIZZTHXZRDOFM-XFULWGLBSA-N tamsulosin hydrochloride Chemical compound [H+].[Cl-].CCOC1=CC=CC=C1OCCN[C@H](C)CC1=CC=C(OC)C(S(N)(=O)=O)=C1 ZZIZZTHXZRDOFM-XFULWGLBSA-N 0.000 description 1
- WJCNZQLZVWNLKY-UHFFFAOYSA-N thiabendazole Chemical compound S1C=NC(C=2NC3=CC=CC=C3N=2)=C1 WJCNZQLZVWNLKY-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0068—General arrangements, e.g. flowsheets
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/50—Carbon dioxide
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
- C01C1/00—Ammonia; Compounds thereof
- C01C1/02—Preparation, purification or separation of ammonia
- C01C1/12—Separation of ammonia from gases and vapours
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02C—CAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
- Y02C20/00—Capture or disposal of greenhouse gases
- Y02C20/40—Capture or disposal of greenhouse gases of CO2
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Gas Separation By Absorption (AREA)
- Treating Waste Gases (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/030,374 US4256471A (en) | 1979-04-16 | 1979-04-16 | Process for the separation of ammonia and carbon dioxide from mixtures containing ammonia, carbon dioxide and water |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS221545B2 true CS221545B2 (en) | 1983-04-29 |
Family
ID=21853917
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS802615A CS221545B2 (en) | 1979-04-16 | 1980-04-15 | Method of obtaining the ammonia and carbon dioxide from the mixtures containing ammonium,carbon dioxide and water |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US4256471A (de) |
| EP (1) | EP0018028B1 (de) |
| JP (1) | JPS55139815A (de) |
| AR (1) | AR225627A1 (de) |
| AT (1) | ATE2311T1 (de) |
| BR (1) | BR8002342A (de) |
| CA (1) | CA1123176A (de) |
| CS (1) | CS221545B2 (de) |
| DE (1) | DE3061735D1 (de) |
| ES (1) | ES490383A0 (de) |
| HU (1) | HU181694B (de) |
| IN (1) | IN152909B (de) |
| NO (1) | NO801092L (de) |
| PL (1) | PL124736B1 (de) |
| RO (1) | RO79842A (de) |
| SU (1) | SU1058503A3 (de) |
| YU (1) | YU94480A (de) |
| ZA (1) | ZA801912B (de) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4975205B2 (ja) * | 2000-04-28 | 2012-07-11 | 日揮株式会社 | ガス状混合物からのアンモニア回収方法 |
| US6706093B2 (en) * | 2000-05-23 | 2004-03-16 | Rohm And Haas Company | Method and apparatus for preventing iron contamination in corrosive service |
| CN100475970C (zh) * | 2002-12-27 | 2009-04-08 | 味之素株式会社 | 通过塔技术生产氨基酸或其盐的方法及其生产装置 |
| RU2372568C1 (ru) * | 2008-03-26 | 2009-11-10 | ОАО "Тольяттиазот" | Способ извлечения аммиака из продувочных газов |
| RU2372567C1 (ru) * | 2008-03-26 | 2009-11-10 | ОАО "Тольяттиазот" | Способ извлечения аммиака из продувочных и танковых газов |
| US8500868B2 (en) * | 2009-05-01 | 2013-08-06 | Massachusetts Institute Of Technology | Systems and methods for the separation of carbon dioxide and water |
| CN102538394B (zh) * | 2011-12-27 | 2014-08-06 | 尤彪 | 一种低温精馏分离氨和二氧化碳的方法 |
| CN104129802B (zh) * | 2014-08-06 | 2015-10-28 | 中国成达工程有限公司 | 一种分离含nh3和co2混合气的装置及其分离工艺 |
| JP6948677B2 (ja) * | 2016-10-05 | 2021-10-13 | 株式会社ササクラ | 低沸点物質の回収装置及び回収方法 |
| JP6681964B2 (ja) * | 2018-01-12 | 2020-04-15 | 木村化工機株式会社 | アンモニア水溶液の蒸留装置 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE669314C (de) | 1934-11-22 | 1938-12-22 | I G Farbenindustrie Akt Ges | Trennung von Kohlensaeure und Ammoniak |
| GB664375A (de) * | 1954-07-27 | 1952-01-02 | ||
| US3112177A (en) * | 1959-11-11 | 1963-11-26 | Toyo Koatsu Ind Inc | Method of separating ammonia from hydrogen cyanide |
| NL264624A (de) | 1960-05-10 | |||
| US3225519A (en) * | 1962-12-13 | 1965-12-28 | Hydrocarbon Research Inc | Gas absorption |
| AT261638B (de) | 1966-05-02 | 1968-05-10 | Chemie Linz Ag | Verfahren zur Aufarbeitung eines Ammoniak-Kohlensäure-Gasgemisches |
| DE1592349B1 (de) * | 1966-05-04 | 1971-08-26 | Lentia Gmbh | Verfahren zur Trennung eines Ammoniak-Kohlendioxid-Gasgemisches |
| NL143063B (nl) | 1967-07-06 | 1974-08-15 | Stamicarbon | Werkwijze voor het bereiden van ferromagnetisch materiaal. |
| DE2229213C2 (de) * | 1972-06-15 | 1982-12-02 | Metallgesellschaft Ag, 6000 Frankfurt | Verfahren zur Aufarbeitung der bei der Entgasung oder Vergasung von Kohlen anfallenden Abwässer |
| DE2262457A1 (de) * | 1972-12-20 | 1974-06-27 | Linde Ag | Verfahren und vorrichtung zum auswaschen von kohlendioxid, schwefelwasserstoff und gegebenenfalls kohlenoxisulfid |
| DE2317603C3 (de) * | 1973-04-07 | 1982-03-25 | Basf Ag, 6700 Ludwigshafen | Verfahren zur zumindest teilweisen Trennung von Ammoniak und Kohlendioxid enthaltenden Gasgemischen |
| US3920419A (en) * | 1974-04-10 | 1975-11-18 | Republic Steel Corp | Method of removing ammonia from ammonia containing liquor |
| GB1533462A (en) * | 1975-02-05 | 1978-11-22 | Sterling Drug Inc | Method and apparatus for ammonia removal from wastewaters |
| DE2527985C3 (de) * | 1975-06-24 | 1981-04-16 | Metallgesellschaft Ag, 6000 Frankfurt | Kontinuierliches Verfahren zur Gewinnung von reinem Ammoniak |
| DE2646804C3 (de) * | 1976-10-16 | 1982-03-11 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Gewinnung von reinem Ammoniak aus Ammoniak und Kohlendioxid enthaltenden Gasgemischen |
| NL168196C (nl) * | 1976-11-03 | 1982-03-16 | Stamicarbon | Werkwijze voor het afscheiden van nh&013 en co&012 uit een mengsel van nh&013, co&012 en h&012o. |
| NL7804668A (nl) * | 1978-04-29 | 1979-10-31 | Stamicarbon | Werkwijze voor het scheiden van nh3 en co2 uit meng- sels van nh3 ,co2 en water. |
-
1979
- 1979-04-16 US US06/030,374 patent/US4256471A/en not_active Expired - Lifetime
-
1980
- 1980-03-24 IN IN340/CAL/80A patent/IN152909B/en unknown
- 1980-03-29 EP EP80200296A patent/EP0018028B1/de not_active Expired
- 1980-03-29 AT AT80200296T patent/ATE2311T1/de not_active IP Right Cessation
- 1980-03-29 DE DE8080200296T patent/DE3061735D1/de not_active Expired
- 1980-03-31 ZA ZA00801912A patent/ZA801912B/xx unknown
- 1980-04-03 SU SU802901346A patent/SU1058503A3/ru active
- 1980-04-07 YU YU00944/80A patent/YU94480A/xx unknown
- 1980-04-09 ES ES490383A patent/ES490383A0/es active Granted
- 1980-04-14 AR AR280684A patent/AR225627A1/es active
- 1980-04-15 NO NO801092A patent/NO801092L/no unknown
- 1980-04-15 BR BR8002342A patent/BR8002342A/pt unknown
- 1980-04-15 JP JP5021780A patent/JPS55139815A/ja active Pending
- 1980-04-15 CA CA349,921A patent/CA1123176A/en not_active Expired
- 1980-04-15 HU HU80917A patent/HU181694B/hu unknown
- 1980-04-15 CS CS802615A patent/CS221545B2/cs unknown
- 1980-04-16 PL PL1980223507A patent/PL124736B1/pl unknown
- 1980-04-16 RO RO80100855A patent/RO79842A/ro unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES8104141A1 (es) | 1981-04-16 |
| PL223507A1 (de) | 1981-02-13 |
| PL124736B1 (en) | 1983-02-28 |
| EP0018028A1 (de) | 1980-10-29 |
| ATE2311T1 (de) | 1983-02-15 |
| CA1123176A (en) | 1982-05-11 |
| US4256471A (en) | 1981-03-17 |
| EP0018028B1 (de) | 1983-01-26 |
| SU1058503A3 (ru) | 1983-11-30 |
| NO801092L (no) | 1980-10-17 |
| BR8002342A (pt) | 1980-12-02 |
| YU94480A (en) | 1983-01-21 |
| JPS55139815A (en) | 1980-11-01 |
| ZA801912B (en) | 1981-03-25 |
| AR225627A1 (es) | 1982-04-15 |
| ES490383A0 (es) | 1981-04-16 |
| IN152909B (de) | 1984-04-28 |
| HU181694B (en) | 1983-11-28 |
| DE3061735D1 (en) | 1983-03-03 |
| RO79842A (ro) | 1982-12-06 |
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