CS220766B2 - Method of preparation of melamine - Google Patents
Method of preparation of melamine Download PDFInfo
- Publication number
- CS220766B2 CS220766B2 CS803102A CS310280A CS220766B2 CS 220766 B2 CS220766 B2 CS 220766B2 CS 803102 A CS803102 A CS 803102A CS 310280 A CS310280 A CS 310280A CS 220766 B2 CS220766 B2 CS 220766B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- melamine
- gas mixture
- urea
- ammonia
- desublimator
- Prior art date
Links
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 title claims abstract description 47
- 229920000877 Melamine resin Polymers 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 29
- 239000000203 mixture Substances 0.000 claims abstract description 26
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 24
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000004202 carbamide Substances 0.000 claims abstract description 18
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 14
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 12
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 12
- 238000005979 thermal decomposition reaction Methods 0.000 claims abstract description 5
- 239000007789 gas Substances 0.000 claims description 29
- 239000002912 waste gas Substances 0.000 claims description 23
- 239000013543 active substance Substances 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 7
- 230000006835 compression Effects 0.000 claims description 6
- 238000007906 compression Methods 0.000 claims description 6
- 239000000428 dust Substances 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 abstract description 13
- 239000012535 impurity Substances 0.000 abstract description 5
- 239000011149 active material Substances 0.000 abstract 2
- 239000002245 particle Substances 0.000 description 8
- 239000003054 catalyst Substances 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000000498 cooling water Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- 241000219112 Cucumis Species 0.000 description 2
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 239000003337 fertilizer Substances 0.000 description 2
- 239000008246 gaseous mixture Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- YZEZMSPGIPTEBA-UHFFFAOYSA-N 2-n-(4,6-diamino-1,3,5-triazin-2-yl)-1,3,5-triazine-2,4,6-triamine Chemical compound NC1=NC(N)=NC(NC=2N=C(N)N=C(N)N=2)=N1 YZEZMSPGIPTEBA-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 241000238017 Astacoidea Species 0.000 description 1
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- ILRRQNADMUWWFW-UHFFFAOYSA-K aluminium phosphate Chemical compound O1[Al]2OP1(=O)O2 ILRRQNADMUWWFW-UHFFFAOYSA-K 0.000 description 1
- YSKUZVBSHIWEFK-UHFFFAOYSA-N ammelide Chemical compound NC1=NC(O)=NC(O)=N1 YSKUZVBSHIWEFK-UHFFFAOYSA-N 0.000 description 1
- MASBWURJQFFLOO-UHFFFAOYSA-N ammeline Chemical compound NC1=NC(N)=NC(O)=N1 MASBWURJQFFLOO-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- YZYDPPZYDIRSJT-UHFFFAOYSA-K boron phosphate Chemical compound [B+3].[O-]P([O-])([O-])=O YZYDPPZYDIRSJT-UHFFFAOYSA-K 0.000 description 1
- 229910000149 boron phosphate Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 108010038270 melain Proteins 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 238000010517 secondary reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
- C07D251/56—Preparation of melamine
- C07D251/60—Preparation of melamine from urea or from carbon dioxide and ammonia
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Catalysts (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Saccharide Compounds (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Cosmetics (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Treating Waste Gases (AREA)
- Fertilizers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7903473A NL7903473A (nl) | 1979-05-03 | 1979-05-03 | Werkwijze voor het bereiden van melamine. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CS220766B2 true CS220766B2 (en) | 1983-04-29 |
Family
ID=19833094
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CS803102A CS220766B2 (en) | 1979-05-03 | 1980-05-04 | Method of preparation of melamine |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US4348520A (ro) |
| EP (1) | EP0018695B1 (ro) |
| JP (2) | JPS55149267A (ro) |
| AT (1) | ATE1504T1 (ro) |
| BR (1) | BR8002683A (ro) |
| CA (1) | CA1128515A (ro) |
| CS (1) | CS220766B2 (ro) |
| DE (1) | DE3060795D1 (ro) |
| EG (1) | EG14499A (ro) |
| ES (1) | ES491105A0 (ro) |
| HU (1) | HU184276B (ro) |
| IN (1) | IN153077B (ro) |
| NL (1) | NL7903473A (ro) |
| NO (1) | NO154393C (ro) |
| PL (1) | PL223958A1 (ro) |
| RO (1) | RO79649A (ro) |
| SU (1) | SU1060109A3 (ro) |
| YU (1) | YU40776B (ro) |
| ZA (2) | ZA802417B (ro) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL8201479A (nl) * | 1982-04-07 | 1983-11-01 | Stamicarbon | Werkwijze voor het bereiden van melamine. |
| DE3500188C2 (de) * | 1984-01-05 | 1994-08-18 | Melamine Chemicals Inc | Wasserfreie Hochdruck-Melamin-Synthese |
| US4565867A (en) * | 1984-01-05 | 1986-01-21 | Melamine Chemicals, Inc. | Anhydrous high-pressure melamine synthesis |
| IE57911B1 (en) * | 1984-01-05 | 1993-05-19 | Melamine Chemicals Inc | Production of melamine |
| JP2684409B2 (ja) * | 1988-03-31 | 1997-12-03 | コニカ株式会社 | シアノ基および／またはハロゲン原子で置換されたアニリン類の製造方法およびその製造のために使用される化合物 |
| BE1008133A3 (nl) * | 1994-03-15 | 1996-01-23 | Dsm Nv | Werkwijze voor de afscheiding van verontreinigingen uit een heet synthesegasmengsel bij de melaminebereiding. |
| US5389134A (en) * | 1994-07-18 | 1995-02-14 | Xerox Corporation | Ink compositions for ink jet printing |
| US20030028020A1 (en) * | 2001-07-27 | 2003-02-06 | Gupta Ram B. | Process for the synthesis of high purity melamine |
| DE102005023042B4 (de) * | 2005-05-06 | 2007-10-31 | Lurgi Ag | Verfahren zur Herstellung von Melamin |
| DE102005023041B4 (de) * | 2005-05-06 | 2007-10-11 | Lurgi Ag | Verfahren zum Herstellen von Melamin mit Wärmerückgewinnung |
| EP2050740A1 (de) * | 2007-10-15 | 2009-04-22 | Basf Se | Verfahren zur Herstellung von Melamin |
| DE102008032425B4 (de) * | 2008-07-10 | 2015-07-30 | Air Liquide Global E&C Solutions Germany Gmbh | Verfahren und Anlage zur Herstellung von Melamin |
| DE102009052420C5 (de) * | 2009-11-10 | 2014-05-22 | Lurgi Gmbh | Verfahren zur kontinuierlichen Herstellung von Melamin |
| CN113375133A (zh) * | 2021-06-23 | 2021-09-10 | 四川金象赛瑞化工股份有限公司 | 利用三聚氰胺生产系统生产高品位蒸汽生产装置及其生产高品位蒸汽的方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1670126A1 (de) * | 1966-08-09 | 1970-10-29 | Basf Ag | Verfahren zur Kuehlung der bei der Melaminsynthese erhaltenen Abgase |
| DE1670286A1 (de) * | 1967-11-11 | 1971-01-28 | Basf Ag | Verfahren zur Aufarbeitung der bei der Melaminsynthese anfallenden Abgase |
| DE1812120C3 (de) * | 1968-12-02 | 1974-02-28 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Melamin |
| US3700672A (en) * | 1969-04-15 | 1972-10-24 | Nissan Chemical Ind Ltd | Process for recovering by-product gases at high pressure in melamine production |
| US3723430A (en) * | 1970-10-28 | 1973-03-27 | Nissan Chemical Ind Ltd | Method for reclamation of melamine waste gas |
| US3895007A (en) * | 1972-04-28 | 1975-07-15 | Basf Ag | Manufacture of melamine |
| NL178487C (nl) * | 1976-03-26 | 1986-04-01 | Stamicarbon | Inrichting en werkwijze voor het versproeien van een vloeistof. |
| RO74590A (ro) * | 1977-01-19 | 1981-08-30 | Stamicarbon Bv,Nl | Procedeu de preparare a melaminei din uree |
-
1979
- 1979-05-03 NL NL7903473A patent/NL7903473A/nl not_active Application Discontinuation
-
1980
- 1980-04-22 ZA ZA00802417A patent/ZA802417B/xx unknown
- 1980-04-22 ZA ZA00802416A patent/ZA802416B/xx unknown
- 1980-04-29 SU SU802913806A patent/SU1060109A3/ru active
- 1980-04-29 HU HU801064A patent/HU184276B/hu unknown
- 1980-04-30 EG EG80265A patent/EG14499A/xx active
- 1980-04-30 BR BR8002683A patent/BR8002683A/pt unknown
- 1980-04-30 YU YU1178/80A patent/YU40776B/xx unknown
- 1980-04-30 RO RO80101025A patent/RO79649A/ro unknown
- 1980-05-01 DE DE8080200403T patent/DE3060795D1/de not_active Expired
- 1980-05-01 AT AT80200403T patent/ATE1504T1/de active
- 1980-05-01 EP EP80200403A patent/EP0018695B1/en not_active Expired
- 1980-05-02 US US06/146,181 patent/US4348520A/en not_active Expired - Lifetime
- 1980-05-02 JP JP5937280A patent/JPS55149267A/ja active Pending
- 1980-05-02 PL PL22395880A patent/PL223958A1/xx unknown
- 1980-05-02 ES ES491105A patent/ES491105A0/es active Granted
- 1980-05-02 NO NO801283A patent/NO154393C/no unknown
- 1980-05-02 JP JP5937380A patent/JPS55149268A/ja active Pending
- 1980-05-03 IN IN510/CAL/80A patent/IN153077B/en unknown
- 1980-05-04 CS CS803102A patent/CS220766B2/cs unknown
- 1980-05-09 CA CA351,210A patent/CA1128515A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| US4348520A (en) | 1982-09-07 |
| ZA802416B (en) | 1981-04-29 |
| RO79649A (ro) | 1982-08-17 |
| EG14499A (en) | 1985-03-31 |
| ZA802417B (en) | 1981-04-29 |
| JPS55149268A (en) | 1980-11-20 |
| NO154393B (no) | 1986-06-02 |
| IN153077B (ro) | 1984-05-26 |
| ATE1504T1 (de) | 1982-09-15 |
| YU117880A (en) | 1983-10-31 |
| DE3060795D1 (en) | 1982-10-28 |
| ES8101057A1 (es) | 1980-12-01 |
| CA1128515A (en) | 1982-07-27 |
| EP0018695A1 (en) | 1980-11-12 |
| JPS55149267A (en) | 1980-11-20 |
| NO154393C (no) | 1986-09-10 |
| EP0018695B1 (en) | 1982-09-01 |
| SU1060109A3 (ru) | 1983-12-07 |
| PL223958A1 (ro) | 1981-02-13 |
| BR8002683A (pt) | 1980-12-16 |
| YU40776B (en) | 1986-06-30 |
| NO801283L (no) | 1980-11-04 |
| HU184276B (en) | 1984-07-30 |
| NL7903473A (nl) | 1980-11-05 |
| ES491105A0 (es) | 1980-12-01 |
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