CN87102805A - Manufacture method of a kind of ceramic glaze and products thereof - Google Patents
Manufacture method of a kind of ceramic glaze and products thereof Download PDFInfo
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- CN87102805A CN87102805A CN 87102805 CN87102805A CN87102805A CN 87102805 A CN87102805 A CN 87102805A CN 87102805 CN87102805 CN 87102805 CN 87102805 A CN87102805 A CN 87102805A CN 87102805 A CN87102805 A CN 87102805A
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Abstract
A kind of iris droplet temmoku glaze that the invention discloses a kind of manufacture method of ceramic temmoku glaze and utilize this method to make.Present method is by the proportioning of appropriately choosing the glaze composition, the proportion and the firing temperature of glaze slip, in traditional kiln, and the ceramic temmoku glaze once-firing that adopts traditional firing process to wish to get.There is the peculiar muffle painting of similar rainbow the black matrix spot inside of the iris droplet temmoku glaze that burns till.
Method of the present invention does not need the special clay raw material, need not follow special cooling cooling system yet, and technology is simple, and processing ease is colour-stable.
Description
A kind of ceramic temmoku glaze product that the present invention relates to the manufacture method of a kind of ceramic glaze, particularly ceramic temmoku glaze and produce in this way.
The black glaze that ceramic industry is used always is a kind of famous and precious color glaze.As far back as the Eastern Han Dynasty, can burn darker black glaze with reducing atmosphere in the Shangyu, Zhejiang.Deqing ware during the Eastern Jin Dynasty has also burnt pure black glaze.These black glaze mainly are to burn till in reducing atmosphere with ferruginous clay, but the colour generation instability, firing process is difficult to grasp.
In Japan, people call temmoku to the ceramic ware of executing black glaze usually.Afterwards, the ceramic ware of not only executing black glaze claimed temmoku, and connected appearance similar " building small cup " (12nd to 13 century Fujian Province's Jianyang County be fired into tea small cup), even do not execute the ceramic ware of black glaze, had been also referred to as temmoku in Japan.This noun of temmoku has become international term (being " TEMMOKU " in the English), known to everybody.
The characteristics of temmoku glaze are: at the bottom of the glaze of black or chocolate, and the crystallization spot that is distributing various, the color difference of spot, its title is also different.The crystallization spot is silver gray person, is called droplet temmoku glaze; Spot is dispersive striated person, is called the spike of rice temmoku glaze; Around the spot avy blue haloing person is arranged, be called yohen Tenmoku ...On the droplet temmoku glaze face, the brilliant point in many silver-gray gardens that distributing, just like night aerial an array of stars, glittering, " pitch-dark night sky Stem and leaf of Hongkong Pavetta " really arranged, the sensitization of " contain tea and dodge golden light, be filled with water and dodge silver-colored light ".Spot in the yohen Tenmoku, appear in one's mind thinly seemingly on pitch-black glaze, the halation that the circle avy blue is arranged around the spot, variation with viewing angle can produce tangible refractive power, be the part of bright blue streak can be along with the change of the angle of observing mobile luminous position, form the fancy effect that the color sunlight becomes.Therefore, ceramic temmoku glaze generally all has very high artistic value.
But, make the ceramic product that is decorated with temmoku glaze and but be not easy, at present, have only four Yao change of weather order tea small cups " to put up a kiln " in the world and be fired into by China Southern Song Dynasty Fujian Province in period Jianyang County.Usually needed the clay of extraordinary composition to make raw material in order to fire the temmoku glaze goods modern age, perhaps needs the intensification and the speed of cooling of strict control kiln, otherwise, be difficult to burn till qualified temmoku glaze ceramic product.China Shandong Province's Boshan ceramics factory is in order to burn rain drop glaze (the similar kind of droplet temmoku glaze), and must adopt a kind of iron-holder is that 5%～8% black glaze soil is made glaze, and blank also need adopt the higher raw clay preparation of iron oxide content.1986 the 6th phases of " Chinese pottery " magazine were also once reported, China National Light Industrial Products Department's ceramic research is cooperated with the Shanghai Silicate Inst., Chinese Academy of Sciences, the preparation technology of temmoku glaze and quality mechanism have been carried out deep research, and to think that Yao becomes the formation and the cooling system of temmoku glaze closely bound up, must be when firing according to a special cooling curve, adopt the cooling system of staged cooling, could obtain to have the yohen Tenmoku ceramic product of avy blue halation.This all makes complex process inevitably, and the manufacturing cost of product is high.
Purpose of the present invention will overcome above-mentioned shortcoming exactly, provides a kind of technology simple ceramic temmoku glaze manufacture method, and makes a kind of novel temmoku glaze-iris droplet temmoku glaze in this way.
The invention is characterized in: the proportioning (by weight) of (1) glaze composition is:
SiO
264.3～69.1，Al
2O
310.6～15.6，
Fe
2O
34.5～7.3，CaO 2.4～2.7，
MgO 2.5～3.6，KNaO 9.8～11.5，
NH
4VO
32.0～9.0, water is an amount of;
(2) proportion of glaze slip should be controlled between 1.55～1.65;
(3) firing temperature is 1230 ℃～1250 ℃.
Form agent with ferric oxide as tinting material and spot, form promotor as spot, form dissimilar spots by the amount of controlling the ammonium meta-vanadate that is added, to obtain different artistic effects with ammonium meta-vanadate.
When the proportioning of ingredient is: SiO
269.1, Al
2O
310.6, Fe
2O
34.7 CaO 2.4, MgO 2.9, and KNaO 10.1, NH
4VO
34.9, when water is an amount of, can obtain silver grey droplet temmoku glaze.
When the proportioning of ingredient is: SiO
269.1, Al
2O
310.6, Fe
2O
34.7 CaO 2.4, MgO 2.9, and KNaO 10.1, NH
4VO
36.9, when water is an amount of, can obtain yohen Tenmoku.
When the proportioning of ingredient is: SiO
266.3, Al
2O
311.6, Fe
2O
35.1 CaO 2.7, MgO 3.2, KNaO 11.1.NH
4VO
36.9, when water is an amount of, can obtain a kind of novel temmoku glaze-iris droplet temmoku glaze.The characteristics of this glaze are: at the bottom of the glaze of black, and many oil droplet shape spots that distributing, there is the peculiar muffle painting of similar rainbow the inside of spot.
Material input ball milling altar wet-milling to the 10000-hole sieve (250 order copper wires sieve) of above-mentioned suitable proportion is tailed over about 0.02%, make sieve concentration of glaze slip to be controlled at proportion be 1.55～1.65, take twice glazing (soak glaze or drench glaze all can), treat that promptly the first layer glaze executes second layer glaze after dried slightly immediately, burn till in oxidizing atmosphere under 1230 ℃～1250 ℃ temperature after having executed the product dried of glaze, its firing process (firing operation and cooling curve etc.) is basic identical with traditional ceramics.
The temmoku glaze that the present invention makes, do tinting material and spot formation agent owing to adopt ferric oxide, and be to promote the formation of spot by adding an amount of ammonium meta-vanadate, thereby do not need the special clay raw material, need not follow strict staged cooling cooling system yet, fully can be in traditional kiln, produce qualified temmoku glaze ceramic product by traditional ceramic sintering process, therefore technology is simple, processing ease, low cost of manufacture is colour-stable, and be not subjected to the restriction of regional raw material, be easy to produce in batches.
Embodiment one:
Press following prescription: 3.27 kilograms of feldspars (Ziyuan County, Guangxi product); 0.21 kilogram in Wingdale (Liuzhou product); burn talcum (Guilin product) 0.32 kilogram; quartzy (Jiangxi product) 1.20 kilograms; 0.25 kilogram of ferric oxide (Changsha product); 0.25 kilogram of ammonium meta-vanadate (Shanghai chemical reagent factory product); (wherein ferric oxide is the technical pure level; ≮ 90%; ammonium meta-vanadate is the technical pure level, ≮ 94%) and, water is an amount of; accurately behind the above-mentioned material of weighing; dropped in the ball milling altar wet-milling 20～45 hours, will grinding liquid through 10000-hole sieve then, to be sieved to residuum be about 0.02%, sieve concentration of glaze slip to be controlled at proportion be 1.6; the blank of ceramic ware is executed glaze (soak execute or drench Shi Junke) earlier; treat that the glaze layer is dried slightly when not touching with one's hand, execute second layer glaze immediately, executed the product dried of glaze after; under 1230 ℃～1250 ℃ temperature, in oxidizing atmosphere, press traditional ceramic sintering process once-firing, just can obtain the ceramic of silver grey droplet temmoku glaze.
Embodiment two:
Proportioning raw materials among the embodiment one is changed into: 3.27 kilograms of feldspars, 0.21 kilogram in Wingdale burns 0.32 kilogram in talcum, and quartzy 1.20 kilograms, 0.25 kilogram of ferric oxide, 0.35 kilogram of ammonium meta-vanadate, water is an amount of.By the step processing of last example, make Yao change of weather order glaze ceramic.
Embodiment three:
Proportioning raw materials among the embodiment one is changed into: 3.27 kilograms of feldspars, 0.21 kilogram in Wingdale burns 0.32 kilogram in talcum, quartzy 0.75 kilogram, 0.25 kilogram of ferric oxide, 0.35 kilogram of ammonium meta-vanadate, water is an amount of, presses the step processing of precedent, makes iris droplet temmoku glaze ceramic.
Claims (4)
1, a kind of manufacture method of ceramic temmoku glaze contains SiO in the glaze
2, Al
2O
3Fe
2O
3, CaO, MgO, KNaO, NH
4VO
3Deng composition, after the wet-milling of ball milling altar, filter with 10000-hole sieve, blank with traditional ceramic sintering process, burn till in oxidizing atmosphere, is characterized in that after twice glazing:
(1) proportioning of ingredient (weight ratio) is SiO
264.3～69.1, Al
2O
310.6～15.6, Fe
2O
34.5～7.3, CaO2.4～2.7, MgO2.5～3.6, KNaO9.8～11.5, NH
4VO
32.0～9.0, water is an amount of,
(2) proportion of glaze slip is 1.55～1.65,
(3) firing temperature is 1230 ℃～1250 ℃.
2, the manufacture method of ceramic temmoku glaze according to claim 1 is characterized in that the proportioning (weight ratio) of ingredient is SiO
269.1, Al
2O
310.6, Fe
2O
34.7, CaO2.4, MgO2.9, KNaO10.1, NH
4VO
34.9 water is an amount of.
3, the manufacture method of ceramic temmoku glaze according to claim 1 is characterized in that the proportioning of ingredient is: SiO
269.1, Al
2O
310.6, Fe
2O
34.7, CaO2.4, MgO2.9, KNaO10.1, NH
4VO
36.9 water is an amount of.
4, a kind of iris droplet temmoku glaze that makes with the manufacture method of the described ceramic temmoku glaze of claim 1 contains SiO in the glaze
2, Al
2O
3, Fe
2O
3, CaO, MgO, KNaO, NH
4VO
3Deng composition, it is characterized in that the proportioning (weight ratio) of ingredient is SiO
266.3, Al
2O
311.6, Fe
2O
35.1 CaO 2.7, MgO 3.2, and KNaO 11.1, NH
4VO
36.9 and water is an amount of, the glaze that burns till at the bottom of the glaze of black, many oil droplet shape spots that distributing, there is the peculiar muffle painting of similar rainbow the inside of spot.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 87102805 CN87102805A (en) | 1987-04-13 | 1987-04-13 | Manufacture method of a kind of ceramic glaze and products thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 87102805 CN87102805A (en) | 1987-04-13 | 1987-04-13 | Manufacture method of a kind of ceramic glaze and products thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN87102805A true CN87102805A (en) | 1988-11-02 |
Family
ID=4814126
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 87102805 Pending CN87102805A (en) | 1987-04-13 | 1987-04-13 | Manufacture method of a kind of ceramic glaze and products thereof |
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|---|---|
| CN (1) | CN87102805A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1036516C (en) * | 1994-01-29 | 1997-11-26 | 邢良坤 | Hongtianmu glaze ceramic and producing method |
| CN1098229C (en) * | 2000-07-10 | 2003-01-08 | 吴锦强 | Process for preparing crystal-like relief brick |
| CN1303026C (en) * | 2002-10-31 | 2007-03-07 | 福建省双旗山金矿 | Ceramic coloured enamel produced using gold tail ore and its technological method |
| CN1328223C (en) * | 2005-05-25 | 2007-07-25 | 广东全福陶瓷实业有限公司 | Manufacturing method of redyohen tenmoku ceramic and ceramic glaze used therefor |
| CN100429181C (en) * | 2005-12-23 | 2008-10-29 | 胡武强 | Ceramic glaze material preparation method and ceramic glaze firing method |
| CN100453009C (en) * | 2005-06-27 | 2009-01-21 | 江苏省陶瓷研究所有限公司 | Western tableware of iron and ceramic and its making process |
| CN102501700A (en) * | 2011-09-30 | 2012-06-20 | 常州市武进区掐丝珐琅画艺术研究所 | Process of making cloisonne enamel with natural texture |
| CN102504621A (en) * | 2011-09-30 | 2012-06-20 | 常州市武进区掐丝珐琅画艺术研究所 | Formula of blue pigment for cloisonn |
| CN109095884A (en) * | 2018-08-29 | 2018-12-28 | 巫贵豪 | Build a preparation process |
| CN111777402A (en) * | 2020-07-17 | 2020-10-16 | 高谟和 | Xiayguangdian cup |
-
1987
- 1987-04-13 CN CN 87102805 patent/CN87102805A/en active Pending
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1036516C (en) * | 1994-01-29 | 1997-11-26 | 邢良坤 | Hongtianmu glaze ceramic and producing method |
| CN1098229C (en) * | 2000-07-10 | 2003-01-08 | 吴锦强 | Process for preparing crystal-like relief brick |
| CN1303026C (en) * | 2002-10-31 | 2007-03-07 | 福建省双旗山金矿 | Ceramic coloured enamel produced using gold tail ore and its technological method |
| CN1328223C (en) * | 2005-05-25 | 2007-07-25 | 广东全福陶瓷实业有限公司 | Manufacturing method of redyohen tenmoku ceramic and ceramic glaze used therefor |
| CN100453009C (en) * | 2005-06-27 | 2009-01-21 | 江苏省陶瓷研究所有限公司 | Western tableware of iron and ceramic and its making process |
| CN100429181C (en) * | 2005-12-23 | 2008-10-29 | 胡武强 | Ceramic glaze material preparation method and ceramic glaze firing method |
| CN102501700A (en) * | 2011-09-30 | 2012-06-20 | 常州市武进区掐丝珐琅画艺术研究所 | Process of making cloisonne enamel with natural texture |
| CN102504621A (en) * | 2011-09-30 | 2012-06-20 | 常州市武进区掐丝珐琅画艺术研究所 | Formula of blue pigment for cloisonn |
| CN109095884A (en) * | 2018-08-29 | 2018-12-28 | 巫贵豪 | Build a preparation process |
| CN109095884B (en) * | 2018-08-29 | 2021-06-15 | 巫贵豪 | Process for preparing cup |
| CN111777402A (en) * | 2020-07-17 | 2020-10-16 | 高谟和 | Xiayguangdian cup |
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