CN214174121U - Automatic intelligent synthesis island for digital functional materials - Google Patents

Automatic intelligent synthesis island for digital functional materials Download PDF

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Publication number
CN214174121U
CN214174121U CN202022588482.0U CN202022588482U CN214174121U CN 214174121 U CN214174121 U CN 214174121U CN 202022588482 U CN202022588482 U CN 202022588482U CN 214174121 U CN214174121 U CN 214174121U
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manipulator
operation area
digital functional
functional material
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赵海涛
喻学锋
李龙
何睿
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Shenzhen Institute of Advanced Technology of CAS
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Shenzhen Institute of Advanced Technology of CAS
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Abstract

The utility model relates to the field of high-end equipment manufacturing, new materials, intelligent manufacturing, new generation information technology and biotechnology, in particular to an automatic intelligent synthetic island of digital functional materials, which comprises a first operation area, a second operation area, a third operation area, a first manipulator, a second manipulator and a third manipulator; the first manipulator transfers the materials among the three operation areas; the second manipulator is used for extracting, transferring and mixing the materials in the second operation area; the third manipulator is used for extracting, transferring and mixing the materials in the third operation area. The utility model discloses a manipulator replaces operating personnel to carry out the material and draws, has reduced intensity of labour, saves time and can improve the accuracy of experiment.

Description

Automatic intelligent synthesis island for digital functional materials
Technical Field
The utility model relates to a high-end equipment is made, new material, intelligence is made, new generation information technology and biotechnology field especially relates to a robot and digital manufacturing's novel high performance energy environmental protection, biological medicine and the relevant field functional material structural design of electronic information, preparation and the different function partition's of evaluation island ' and whole platform that combines together.
Background
At present, the energy environmental protection of high-performance materials, the biochemical synthesis and preparation in the fields related to biological medicine and electronic information are still labor-intensive, and some preparation methods and steps have errors or fuzziness, so that the research and development of new materials need to be changed from the traditional mode of scientific intuition and trial and error to the new mode of theoretical prediction and experimental verification, the speed of finding to application of functional materials is comprehensively improved, and the cost is reduced.
In addition, the traditional research and development process of the functional material has high cost and long time consumption, has high requirements on the efficiency and repeatability of the experiment, and the low efficiency and waste of the experiment can be great consumption on research cost and talents. If only the manual operation is relied on, the time and the physical strength are consumed, and errors are more easily generated, so that the repeatability of the experimental result is greatly influenced. On the other hand, the conventional method has obvious defects in the relationship of predicting the characteristics and components of the material, processing conditions and the like. In addition, some toxic solid reagents have great risks in the process of extracting and weighing samples, which may not only cause harm to laboratory staff, but also cause uncontrollable pollution to the environment.
With the vigorous development of information science in the 21 st century, Data-intensive Scientific Discovery (Data-intensive Scientific Discovery) is becoming the "fourth research paradigm". The method explores the cross fusion of the fourth model and the technical fields of high-end equipment manufacturing, new materials, intelligent manufacturing, new-generation information technology, biology and the like, and provides a brand-new methodology for solving key scientific problems in the fields of biomedicine, electronic information and the like and breaking through the neck clamping technology. The research and development of functional materials in the fields of traditional biomedicine, electronic information and the like needs to be subjected to synthesis and test of massive molecules, and is one of the key bottlenecks of research and development.
Therefore, the digital functional material automatic intelligent synthesis island with cooperation of human-artificial intelligence-robot is developed by combining the most advanced technology of current subject development; a robotics digital automation multifunctional platform; the intelligent island prepared by the digitalized biochemical functional material has great significance, the rapid development of the novel functional material in the fields of energy environmental protection, electronic information, biomedical technology and intersection thereof is started, a solid theoretical foundation and technical support are provided for the development of new industries such as energy, information, high-end equipment manufacturing and human health, and the establishment of a biochemical material synthesis cloud end, IT, datamation, AI, automation and high-performance material data element market is promoted.
Disclosure of Invention
An object of the utility model is to provide an automatic intelligent synthetic island of digital functional material has solved the biochemical synthesis of the high performance material that exists among the prior art and has had mistake or ambiguity with preparation intensive, method and step, lacks the problem of digital standardization.
The utility model provides a technical scheme of above-mentioned problem is: an automatic intelligent synthesis island of digital functional materials is characterized in that:
the manipulator comprises a first operation area, a second operation area, a third operation area and a first manipulator;
the first operation area comprises a storage area, a temperature control area, an analysis area and a centrifugation area;
the second operation area comprises a second manipulator, an illumination area, a preparation area, a reaction area, a vibration area, a pipetting head collecting area, a pipetting head placing area, a raw material box and a substrate box;
the third operation area comprises an interaction area and a third manipulator;
the first manipulator is used for transferring materials among the first operation area, the second operation area and the third operation area;
the second manipulator is used for extracting, transferring and mixing the materials in the second operation area;
the third manipulator is used for extracting and transferring the materials in the third operation area.
Further, still include monitoring devices, monitoring devices sets up in the lower part of first operation district, second operation district, and monitoring devices includes camera and telecontrol equipment, telecontrol equipment drives the camera and removes.
Further, the storage areas include a pipetting head storage area, a substrate storage area and a waste storage area.
Further, above-mentioned temperature control district includes thermostatic zone and room temperature district, and the thermostatic zone includes the thermostated container, and the thermostated container adopts first cylinder to control to open and close.
Further, the first manipulator comprises a movable base, a rotating mechanism, a vertical movement mechanism, a telescopic mechanism and a clamping jaw;
the rotating mechanism is fixed on the movable base, the vertical moving mechanism is arranged on the rotating mechanism, the telescopic mechanism is arranged on the vertical moving mechanism, and the clamping jaw is fixed at the tail end of the telescopic mechanism.
The movable base drives the rotating mechanism to move, the rotating mechanism drives the vertical moving mechanism and the telescopic mechanism which are arranged on the rotating mechanism to perform angle adjustment, the vertical moving mechanism drives the telescopic mechanism to move up and down to enable the telescopic mechanism to reach a preset height, and the telescopic mechanism drives the clamping jaw to grab a material and then transfers the material.
Further, the third robot has the same configuration as the first robot.
Further, the second manipulator comprises a three-axis mechanism and a material extraction device arranged on the three-axis mechanism, and the material extraction device is used for extracting and transferring materials in the second operation area;
the three-axis mechanism comprises an x-direction movement mechanism, a y-direction movement mechanism and a z-direction movement mechanism, the z-direction movement mechanism comprises a fixed plate, and the material extraction device is arranged on the fixed plate.
Furthermore, the quantity of the material extraction devices is at least two, the material extraction devices comprise moving rods, moving cylinders and liquid-transferring guns, the moving rods and the moving cylinders are fixed on the fixed plate, the moving cylinders drive the moving rods to move up and down, and the liquid-transferring guns are arranged at the tail ends of the moving rods.
Further, the illumination area comprises UV lamps, and shadowless lamps are arranged at the upper parts of the preparation area and the reaction area.
Further, a vibration motor is arranged at the bottom of the vibration area.
Furthermore, a plurality of transparent porous reaction plates are arranged on the illumination area, the preparation area, the reaction area and the vibration area, and a plurality of reaction holes are arranged on the porous reaction plates.
Furthermore, the raw material box is used for placing different stock solutions and/or raw materials, the raw material box is transparent and cuboid, and the upper end of the raw material box is open.
Further, the waste storage area includes a waste collection area slot, the waste collection slot being rectangular.
The utility model has the advantages that:
the utility model adopts the manipulator to replace the operator to extract materials and prepare samples, greatly reducing the labor intensity of the operator, saving time and improving the accuracy of the experiment;
the utility model can adopt the manipulator to replace the operator to operate, thereby avoiding the operator from being hurt in the experiment process;
the utility model carries out high-throughput (i.e. a large number of repeated operations in a short time) tests, thereby saving cost and time consumption, and shortening the research and development of functional materials which originally can be completed by years or even decades to months;
the utility model discloses can also be through the independent assortment of each subregion module to the realization not only can research and develop biological medicine, can also research and develop the material of aspects such as electronic information and energy environmental protection, and provide the instruction data.
Drawings
Fig. 1 is an overall structure diagram of the digital functional material automatic intelligent synthesis island of the utility model;
FIG. 2 is another directional view of FIG. 1;
FIG. 3 is a flow chart of the operation of the present invention;
FIG. 4 is a diagram illustrating a second operation area of FIG. 1;
FIG. 5 is another directional view of FIG. 4;
FIG. 6 is a schematic view of the material extraction apparatus of FIG. 1;
FIG. 7 is a block diagram of the monitoring device of FIG. 1;
fig. 8 is a structural view of a first robot in fig. 1;
FIG. 9 is a view showing the structure of the illumination area in FIG. 1;
fig. 10 is a structural view of the constant temperature area in fig. 1.
1. A first operating area, 2, a second operating area, 3, a third operating area, 4, a first manipulator, 5, an analysis area, 6, a centrifugation area, 7, a second manipulator, 8, an illumination area, 9, a preparation area, 10, a reaction area, 11, a vibration area, 12, a pipetting head collection area, 13, a pipetting head placement area, 14, a raw material cassette, 15, a substrate cassette, 16, an interaction area, 17, a third manipulator, 18, a camera, 19, a movement device, 20, a pipetting head storage area, 21, a substrate storage area, 22, a waste storage area, 23, a constant temperature area, 24, a chamber temperature area, 25, a moving base, 26, a rotation mechanism, 27, a vertical movement mechanism, 28, a telescoping mechanism, 29, a clamping jaw, 30, an x-direction movement mechanism, 31, a y-direction movement mechanism, 32, a z-direction movement mechanism, 33, a fixing plate, 34, a moving rod, 35, a moving cylinder, 36, a vibration area, a substrate placement area, 16, an interaction area, 17, a camera, a moving base, a rotating mechanism, a moving mechanism, and a moving mechanism for moving a, The liquid-transferring gun comprises a liquid-transferring gun body 37, a vibration motor 38, a porous reaction plate 39, a constant-temperature box cover 40, a first air cylinder 41, a UV lamp 42, a synchronous belt 43, a motor 44, a second air cylinder 45, a U-shaped rail 46 and a refrigerator.
Detailed Description
To make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the drawings of the embodiments of the present invention are combined to clearly and completely describe the technical solutions of the embodiments of the present invention, and obviously, the described embodiments are some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work all belong to the protection scope of the present invention. Thus, the following detailed description of the embodiments of the present invention, presented in the accompanying drawings, is not intended to limit the scope of the invention, as claimed, but is merely representative of selected embodiments of the invention.
Referring to fig. 1 to 3, the automated intelligent digital functional material synthesis island comprises a desktop platform, wherein a first operation area 1, a second operation area 2, a third operation area 3, a first manipulator 4 and a monitoring device are arranged on the desktop platform. The first operation area 1 comprises a storage area, a temperature control area, an analysis area 5 and a centrifugation area 6; the second operation area 2 comprises a second manipulator 7, an illumination area 8, a preparation area 9, a reaction area 10, a vibration area 11, a pipetting head collecting area 12, a pipetting head placing area 13, a raw material box 14 and a substrate box 15; the third operating area 3 comprises an interaction area 16, a third manipulator 17. The first manipulator 4 is used for transferring materials among the first operation area 1, the second operation area 2 and the third operation area 3; the second manipulator 7 is used for extracting, transferring and mixing the materials in the second operation area 2; the third manipulator 17 is used for extracting, transferring and mixing the material in the third operating area 3.
The bottom of desktop platform is equipped with the gyro wheel, conveniently removes.
Referring to fig. 1-3 and 10, as a preferred embodiment of the present invention, the storage areas include a pipetting head storage area 20, a substrate storage area 21 and a waste storage area 22.
The temperature controlled zone includes a constant temperature zone 23 and a room temperature zone 24. The thermostatic zone 23 comprises three thermostats, allowing the simultaneous testing of different temperatures on the sample. A temperature adjusting device and a temperature sensor are arranged in the constant temperature box, and the temperature sensor acquires temperature parameters of the constant temperature box. The thermostat cover 39 of the thermostat is controlled by means of an air cylinder, which opens or closes it.
The illumination area 8, the preparation area 9, the reaction area 10 and the vibration area 11 are provided with a plurality of transparent porous reaction plates 38, the porous reaction plates 38 are provided with a plurality of reaction holes, and the porous reaction plates 38 can be 96-hole plates. The raw material box 14 is used for placing different stock solutions and/or raw materials, the raw material box 14 is in a transparent cuboid shape, and the upper end of the raw material box 14 is opened; the waste storage area 22 includes a waste collection chute that is rectangular in shape. The analysis zone 5 comprises a microplate reader.
Referring to fig. 8, as a preferred embodiment of the present invention, the first robot 4 includes a moving base 25, a rotating mechanism 26, a vertical moving mechanism 27, a telescoping mechanism 28, and a clamping jaw 29. The rotating mechanism 26 is fixed on the moving base 25, the vertical moving mechanism 27 is arranged on the rotating mechanism 26, the telescopic mechanism 28 is arranged on the vertical moving mechanism 27, and the clamping jaw 29 is fixed at the tail end of the telescopic mechanism 28.
The power device and the transmission device of the movable base 25 can be realized in a mode that a motor drives a roller; the rotating mechanism 26 adopts a stepping motor to realize the accurate control of the rotating angle; the vertical movement mechanism 27 is realized by a linear motor, a stator of the vertical movement mechanism is vertically arranged on the rotating mechanism 26, and a rotor base is connected with the telescopic mechanism 28; the telescopic mechanism 28 comprises three rotating arms, two adjacent rotating arms are connected through a stepping motor to control the rotating precision, and the clamping jaw 29 is connected with the last rotating arm.
The first robot 4 is used to transfer the pipetting head, the substrate, the source material, the sample, and the like in the first, second, and third operation sections 2 and 3. For example, the first manipulator 4 transfers the sample in the preparation zone 9 in the second manipulation zone 2 to the interaction zone of the third manipulation zone 3 using the gas gripping jaw 29.
Referring to fig. 1 and 2, the third manipulator 17 has a similar structure to the first manipulator 4, except that its moving base moves on a preset U-shaped track 45, a film sticking machine or a refrigerator 46 is further disposed on the third operating area 3, and the third manipulator 17 is used for transferring the articles in the interactive area 16 and sending the articles to the film sticking machine or the refrigerator 46 for storage.
As an embodiment of the present invention, referring to fig. 4 and 5, the second manipulator 7 includes a three-axis mechanism and a material extraction device disposed on the three-axis mechanism, and the material extraction device is used for extracting and transferring the material in the second operation area 2. The three-axis mechanism comprises an x-direction movement mechanism 30, a y-direction movement mechanism 31 and a z-direction movement mechanism 32, the z-direction movement mechanism 32 comprises a fixing plate 33, and the material extraction device is arranged on the fixing plate 33.
The three-axis mechanism is arranged on a frame, the frame is positioned at the upper part of the second operation area 2, the x-direction movement mechanism 30, the y-direction movement mechanism 31 and the z-direction movement mechanism 32 all adopt linear motors, a stator guide rail of the x-direction movement mechanism 30 is arranged on the frame, the y-direction movement mechanism 31 is arranged on a rotor seat, in order to increase stability, a guide rail parallel to the stator guide rail is further arranged on the frame, a stator guide rail of the y-direction movement mechanism 31 is perpendicular to the stator guide rail of the x-direction movement mechanism 30, a stator guide rail of the z-direction movement mechanism 32 is fixed on the rotor seat of the y-direction movement mechanism 31, and the material extraction device is fixed on the rotor seat of the z-direction movement mechanism 32 through a fixing plate 33.
Referring to fig. 4 and 6, as a preferred embodiment of the present invention, in order to improve the pipetting efficiency and shorten the experimental time, the number of the material extracting devices is at least two, and the material extracting devices include a moving rod 34, a moving cylinder 35 and a pipetting gun 36. The moving rod 34 and the moving cylinder 35 are fixed on the fixing plate 33, the moving cylinder 35 drives the moving rod 34 to move up and down, and the liquid-transferring gun 36 is arranged at the tail end of the moving rod 34.
According to needs, can shift up through removing the liquid-transfering gun that the cylinder 35 was not used, when avoiding the liquid-transfering gun to remove about, the liquid-transfering gun that does not use interferes the experiment. When a plurality of pipette guns are required, the pipette guns 36 are moved down by the moving cylinder 35.
Referring to fig. 9, as a preferred embodiment of the present invention, the illumination area 8 includes 365nm UV lamps 41 and a perforated reaction plate, the UV lamps 41 are located on the perforated reaction plate, and the UV lamps 41 are connected to the telescopic rod of the first cylinder 40, and the telescopic rod drives the UV lamps 41 to move back and forth on the corresponding perforated reaction plate for providing UV illumination.
As a preferred embodiment of the present invention, the vibration area 11 comprises a perforated reaction plate, the bottom of which is provided with a vibration motor 37, the vibration motor 37 vibrates to accelerate the mixing of the liquid, and the time required for the test is shortened.
Referring to fig. 4 and 7, as a preferred embodiment of the present invention, the monitoring device is disposed at the lower portion of the first operating area 1 and the second operating area 2, the monitoring device includes a camera 18 and a moving device 19, and the moving device 19 drives the camera 18 to move. Shadowless lamps are arranged at the upper parts of the first operation area 1 and the second operation area 2. The shadowless lamp can make when shooing light influence each other and cause the condition that the photo formation of image can present more shadow when making each reaction hole shoot because of the difference of light between the reaction hole of porous reaction plate, and the shadow that will be originally covers through the shadowless lamp makes the photo of shooing in real time more clear.
Taking the monitoring device in the lower part of the second operating area 2 as an example, the moving device 19 includes a lateral moving mechanism and a longitudinal moving mechanism, the longitudinal moving mechanism is disposed on the bottom plate, and the lateral moving mechanism is disposed on the longitudinal moving mechanism. The longitudinal moving mechanism comprises a second air cylinder 44, the transverse moving mechanism comprises a motor 43, the motor 43 drives a synchronous belt 42 to rotate, the synchronous belt drives the camera 18 to move, and the second air cylinder 44 drives the transverse moving mechanism to move back and forth. The camera 18 is a 500w color camera, and the lens is a fixed focus lens, and the focal length cannot be changed along with the change of the image brightness, so that the comparability between images is ensured, and meanwhile, an anti-distortion lens is configured.
Example 1:
use of the utility model for the preparation of MOFs proteins
The first step is as follows: five metal ions (Cu) were added to the solution of each of the ligands A, B and C in an amount of 1000. mu.l by using the first robot 42+,Zn2 +,Co2+,Ni2+And Cd2+) Mu.l each of the enzyme solutions (500. mu.l) was transferred to a 96-well deep-well plate in the stock section of the raw material cartridge 14 as a raw material section mother liquor.
The second step is that: five metal ions (Cu) in the raw material cartridge 14 are sucked and transferred by the second robot 72+,Zn2+, Co2+,Ni2+And Cd2+) Place in a 96-well plate in preparation 9, repeat 3 times.
The third step: a second robot arm 7 was used to suck and place 50. mu.l of the transferase solution into the same well position as each of the second-step preparation regions.
The fourth step: a second manipulator 7 is used for sucking and transferring 50 mu l of each solution of the ligands A, B and C into a 96-well plate of the preparation area 9, the solution is mixed with metal ions, the three ligands are fully mixed and reacted with each metal ion, and the solution is moved to a vibration area through a robot arm to vibrate.
The fifth step: the motor 43 is started to drive the camera 18 to take a picture to observe the color change of the solution in the 96-well plate in the different preparation areas 9.
And a sixth step: 50ul syringaldazine and 10ul buffer solution were transferred to the same well of the 96-well plate of the reaction zone 10 at a time by the second manipulator 7 and repeated 15 times.
The seventh step: the 15 reaction liquids generated in the fourth step are sucked and transferred to the 15 holes of the sixth step reaction area 10 by the second manipulator 7 to be fully mixed.
Eighth step: and (4) transferring the 96-well plate obtained in the step seven to a microplate reader of an analysis area 5 by using a first manipulator 4, and performing data analysis and kinetic monitoring.
The ninth step: data were derived from the microplate reader for enzyme activity analysis.
The tenth step: the remaining reaction solution of the 96-well plate was transferred to the centrifugation section 6 by the first robot 4 for centrifugation, followed by evaluation analysis of the solid.
In the above steps, different liquids are sucked by the pipette gun 36 according to requirements, and then the pipette gun is moved to the pipette head storage area 20 to replace the pipette head.
Example 2:
1. the second manipulator 7 operates the pipette 36 to respectively suck 1-10ml of PbX in the substrate box 152And CsX (X ═ F, Cl, or Br), were added to the precursor solution sample cell in the raw material cartridge 14.
2. The second manipulator 7 operates the pipette 36 to suck the long carbon chain organic acid (carbon content 10-20) and the long carbon chain small molecule amine (carbon content 10-20) in the substrate box 15, the suction volume is between 0.1 ml and 2ml, and the sucked liquid is added into the precursor liquid sample groove in the raw material box 14.
3. The second robot 7 operates the pipette gun 36 to repeatedly suck and discharge the precursor liquid sample in the raw material cartridge 15 to mix it uniformly.
4. The second manipulator 7 operates the pipette 36 to draw a solvent (including but not limited to toluene, chloroform, n-hexane, ethyl acetate, etc.) into the 96-well plate of the vibration zone 11, with a feeding volume of 1-20ml, as a poor solvent for subsequent perovskite quantum dot preparation.
5. The vibration motor 37 starts a vibration mode, the second manipulator 7 operates the liquid-transferring gun to absorb 0.1-1ml of precursor liquid in the raw material box, and the precursor liquid is added into a poor solvent at a preset speed to rapidly synthesize the perovskite quantum dots.
6. Every minute, the vibration was stopped, the material was photographed under visible light using the camera 18, and then the first robot 4 placed the 96-well plate in the UV lamp 41 illumination area and photographed the material in the 365-.
7. After each shooting, the first manipulator 4 puts the 96-well plate back to the vibration area to continue the vibration reaction, and the total reaction time is 30 minutes.
8. After the reaction is finished, the first manipulator 4 puts the 96-well plate into an enzyme-labeling instrument to test the light absorption performance of the material.
9. After all tests are completed, the first manipulator 4 transfers the 96-well plate to the interaction zone 16, the third manipulator 17 performs pad sealing on the 96-well plate, and the sample is stored in the refrigerator 46.
10. And then, analyzing the shot photo, converting all the shot information into data and performing graphical processing to obtain the change curve of the luminous and light absorption properties of the sample along with time and the property difference among different materials.
Note: the whole operation process is completed by the manipulator, and the pipette can be moved to the pipette head storage area 20 to replace the pipette head after different liquids are sucked by the pipette at each time.
The utility model adopts the manipulator to replace the operator to extract materials and prepare samples, greatly reducing the labor intensity of the operator, saving time and improving the accuracy of the experiment; the utility model carries out high-throughput (i.e. a large number of repeated operations in a short time) tests, thereby saving cost and time consumption, and shortening the research and development of functional materials which originally can be completed by years or even decades to months; the utility model discloses can also be through the independent assortment of each subregion module to the realization not only can research and develop biological medicine, can also research and develop the material of aspects such as electronic information and energy environmental protection, and provide the instruction data.
The above is only the embodiment of the present invention, not the limitation of the protection scope of the present invention, all the equivalent structures or equivalent processes that are used in the specification and the attached drawings or directly or indirectly applied to other related system fields are included in the protection scope of the present invention.

Claims (11)

1. The utility model provides an automatic intelligent synthetic island of digital functional material which characterized in that:
the manipulator comprises a first operation area (1), a second operation area (2), a third operation area (3) and a first manipulator (4);
the first operation area (1) comprises a storage area, a temperature control area, an analysis area (5) and a centrifugation area (6); the second operation area (2) comprises a second manipulator (7), an illumination area (8), a preparation area (9), a reaction area (10), a vibration area (11), a pipetting head collecting area (12), a pipetting head placing area (13), a raw material box (14) and a substrate box (15); the third operation area (3) comprises an interaction area (16) and a third manipulator (17);
the first manipulator (4) is used for transferring materials among the first operation area (1), the second operation area (2) and the third operation area (3);
the second manipulator (7) is used for extracting, transferring and mixing the materials in the second operation area (2);
the third manipulator (17) is used for extracting, transferring and mixing the materials in the third operation area (3).
2. The automated intelligent digital functional material synthesis island according to claim 1, wherein:
the monitoring device is arranged at the lower parts of the first operation area (1) and the second operation area (2) and comprises a camera (18) and a motion device (19), and the motion device (19) drives the camera (18) to move.
3. The automated intelligent digital functional material synthesis island according to claim 2, wherein:
the storage areas include a pipetting head storage area (20), a substrate storage area (21) and a waste storage area (22).
4. The automated intelligent digital functional material synthesis island according to any one of claims 1 to 3, wherein:
the temperature control area comprises a constant temperature area (23) and a room temperature area (24), the constant temperature area (23) comprises a constant temperature box, the constant temperature box comprises a constant temperature box 39, and the constant temperature box 39 is controlled to be opened and closed by a first air cylinder (40).
5. The automated intelligent digital functional material synthesis island according to any one of claims 1 to 3, wherein:
the first manipulator (4) comprises a moving base (25), a rotating mechanism (26), a vertical movement mechanism (27), a telescopic mechanism (28) and a clamping jaw (29);
the rotating mechanism (26) is fixed on the moving base (25), the vertical moving mechanism (27) is arranged on the rotating mechanism (26), the telescopic mechanism (28) is arranged on the vertical moving mechanism (27), and the clamping jaw (29) is fixed at the tail end of the telescopic mechanism (28).
6. The automated intelligent digital functional material synthesis island according to any one of claims 1 to 3, wherein:
the second manipulator (7) comprises a three-axis mechanism and a material extraction device arranged on the three-axis mechanism, and the material extraction device is used for extracting and transferring materials in the second operation area (2);
the three-axis mechanism comprises an x-direction movement mechanism (30), a y-direction movement mechanism (31) and a z-direction movement mechanism (32), the z-direction movement mechanism (32) comprises a fixing plate (33), and the material extraction device is arranged on the fixing plate (33).
7. The automated intelligent digital functional material synthesis island according to claim 6, wherein:
the number of the material extraction devices is at least two, the material extraction devices comprise a moving rod (34), a moving cylinder (35) and a liquid-transferring gun (36),
the movable rod (34) and the movable cylinder (35) are fixed on the fixed plate (33), the movable cylinder (35) drives the movable rod (34) to move up and down, and the liquid transferring gun (36) is arranged at the tail end of the movable rod (34).
8. The automated intelligent digital functional material synthesis island according to any one of claims 1 to 3, wherein:
illumination district (8) are equipped with the shadowless lamp including UV lamp (41), preparation district (9) and reaction zone (10) upper portion, and UV lamp (41) are connected with the telescopic link of first cylinder (40), and the telescopic link drives UV lamp (41) back-and-forth movement for provide UV illumination.
9. The automated intelligent digital functional material synthesis island according to any one of claims 1 to 3, wherein:
and a vibration motor (37) is arranged at the bottom of the vibration area (11).
10. The automated intelligent digital functional material synthesis island according to any one of claims 1 to 3, wherein:
the illumination area (8), the preparation area (9), the reaction area (10) and the vibration area (11) are provided with a plurality of transparent porous reaction plates (38), and a plurality of reaction holes are formed in the porous reaction plates (38).
11. The automated intelligent digital functional material synthesis island according to any one of claims 1 to 3, wherein:
the raw material box (14) is used for placing different stock solutions and/or raw materials, the raw material box (14) is transparent and cuboid, and the upper end of the raw material box (14) is open;
the waste storage area (22) includes a waste collection chute, which is rectangular in shape.
CN202022588482.0U 2020-11-10 2020-11-10 Automatic intelligent synthesis island for digital functional materials Active CN214174121U (en)

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