CN209372724U - The complementary type loading net used in transmission electron microscope - Google Patents

The complementary type loading net used in transmission electron microscope Download PDF

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Publication number
CN209372724U
CN209372724U CN201822229095.0U CN201822229095U CN209372724U CN 209372724 U CN209372724 U CN 209372724U CN 201822229095 U CN201822229095 U CN 201822229095U CN 209372724 U CN209372724 U CN 209372724U
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mesh sheet
support mesh
complementary
shaped
complementary support
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CN201822229095.0U
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王煜
关永鑫
张慧娟
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Chongqing University
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Chongqing University
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Abstract

The utility model discloses one kind complementary type loading net used in transmission electron microscope, it is characterized by: being spliced into disc by semicircle complementary support mesh sheet or fan-shaped complementary support mesh sheet, all semicircle complementary support mesh sheet or fan-shaped complementary support mesh sheet have the mesh of identical or different shape, and adjacent semicircle complementary support mesh sheet or adjacent fan-shaped complementary support mesh sheet are connected together by clamping structure or are bonded together by glued construction.The utility model can improve sample preparation efficiency under the premise of not destroying test sample stability, to achieve the purpose that save time cost.

Description

The complementary type loading net used in transmission electron microscope
Technical field
The utility model relates to one kind loading net used in transmission electron microscope, in particular to it is a kind of to make in transmission electron microscope Complementary type loading net.
Background technique
Usually transmission electron microscope experiment copper mesh used is done, the support grid of sample is as carried.If support grid copper material, just claim copper Net, it is just corresponding to claim nickel screen, molybdenum net, golden net, nylon wire etc. if it is nickel, molybdenum, gold, nylon.
Support grid is used alone, also referred to as " naked net ".It is mainly used in biological sample preparation, slicer can be cooperated, used in the sink " naked net " fishes for sample.Spray carbon or metal spraying processing are carried out again, are observed subsequently into Electronic Speculum.Most of transmission electron microscope sample are in sample preparation When, in order to ensure sample can be mounted in " support grid ", one layer of organic film can be covered in " support grid ", referred to as " support film ".This tool There is the support grid for supporting film, referred to as " support grid support film ".When sample contact support grid supports film, it can firmly be adsorbed on very much support film On, it is unlikely to slide from the hole of support grid.To be observed in Electronic Speculum.
When sample is placed in Electronic Speculum, " support grid support film " can be irradiated by electron beam, will generate charge on organic support film Accumulation, can also cause sample to discharge, and elegant sample occurs, bounce, supports situations such as film rupture.So people consider supporting Carbon is sprayed on film, is improved the electric conductivity for supporting film, is reached good observing effect.It is this to pass through " support grid of spray carbon supports film ", letter Claim " carbon support film ", general film thickness is 7-10nm.
In terms of cost of manufacture and using effect, copper mesh is most economical practical, so being generally used.Therefore, people often mention " the copper mesh support film " that arrives, " carbon support film ", " carbon film ", " China, side film " etc., or even it is referred to as " copper mesh ", refer to this tool mostly There is " the support film of copper mesh spray carbon ".Commonly referred to as " carbon support film ".
With the progress of science and technology, transmission electron microscope is more and more general in enterprise's scientific research field and universities' research institutes And it is 5 years especially nearly, the installation amount of whole world transmission electron microscope is constantly bettered a record.As what China's high level was studied gos deep into, Current installation total amount is also far from satisfying the vigorous scientific research demand in the whole world.Scientificlly and effectively improve the use of transmission electron microscope Efficiency is beneficial to alleviate the testing requirement of current anxiety.
For current copper mesh as shown in Figure 1, for a round mesh sheet, periphery has round volume circle.One branch copper mesh is only capable of holding Carry a sample.Cause to be wasted in sample preparation using the time there are about the transmission electron microscope of one third and vary, it is especially current High pressure transmission electron microscope can only test a sample every time, put again after sample is placed on typical circular copper mesh and carry out taking out in vacuum chamber very Do-nothing operation.And the transmission electron microscope of mainstream can not accomplish rapid vacuumizing at present, the pumpdown time is long, varies to waste significantly Efficiency and testing efficiency.And rapid vacuumizing equipment purchase and maintenance and its valuableness, it can not popularize at present.How transmission is improved The service efficiency of Electronic Speculum becomes us and is badly in need of the problem of thinking deeply.
Utility model content
In view of the deficiencies of the prior art, the utility model provides a kind of complementary type loading used in transmission electron microscope Net.Sample preparation efficiency is improved, and achievees the purpose that save time cost.
In order to achieve the above object, the utility model is achieved by the following technical programs: one kind makes in transmission electron microscope Complementary type loading net, it is characterised in that: disk is spliced by semicircle complementary support mesh sheet or fan-shaped complementary support mesh sheet Shape, all semicircle complementary support mesh sheet or fan-shaped mesh of the complementary support mesh sheet with identical or different shape, adjacent half Round complementary support mesh sheet or adjacent fan-shaped complementary support mesh sheet are connected together by clamping structure or are glued by glued construction It is combined.
Using the above scheme, in test can optional two edges can the complementary semicircle complementary support mesh sheet being overlapped Either multiple fan-shaped complementary support mesh sheet, in the either fan-shaped complementary support mesh sheet of different semicircle complementary support mesh sheet Different test samples is loaded, then member is surrounded by two semicircle complementary support mesh sheet and swindles or three fan-shaped complementary branch Support mesh sheet surrounds circular piece, and perhaps four fan-shaped complementary support mesh sheet surround circular piece or a semicircle complementary support net Piece and two fan-shaped complementary support mesh sheet surround circular piece.To reach a sample preparation and vacuumizing can test simultaneously two with The purpose of upper sample, and then our time cost is saved, alleviate testing time slow pressure.
In above scheme: all semicircle complementary support mesh sheet and fan-shaped complementary support mesh sheet all have net of different shapes Hole.By mesh of different shapes come the sample of distinguishing tests.
In above scheme: the outer ledge of the semicircle complementary support mesh sheet and fan-shaped complementary support mesh sheet is equipped with arc The arc-shaped side edge of shape edge, all semicircle complementary support mesh sheet and fan-shaped complementary support mesh sheet surrounds a round flange.Have Arc-shaped side edge facilitates clamping.
In above scheme: at the both ends on the arc-shaped side edge of the semicircle complementary support mesh sheet and fan-shaped complementary support mesh sheet Upper and lower sides be respectively arranged with card hole, adjacent semicircle complementary support mesh sheet and fan-shaped complementary support mesh sheet pass through U-shaped clamp It is connected, two supporting legs of the U-shaped clamp are inserted into respectively in adjacent card hole.
In above scheme: wherein the one of the arc-shaped side edge of the semicircle complementary support mesh sheet and fan-shaped complementary support mesh sheet End setting is fluted, and the other end is provided with the protrusion with matching grooves, and in splicing, the protrusion is caught in groove.
In above scheme: the semicircle complementary support mesh sheet docks side difference with another semicircle complementary support mesh sheet It is provided with protrusion and recess, the splicing side of the sector complementary support mesh sheet and another fan-shaped complementary support mesh sheet is respectively arranged with Protrusion and recess, it is described convex in multiple fan-shaped complementary support mesh sheet splicings or when two semicircle complementary support mesh sheet docking It rises and is caught in recess.
In above scheme: the semicircle complementary support mesh sheet is in the side of docking of another semicircle complementary support mesh sheet Zigzag, the equal indention in splicing side of the sector complementary support mesh sheet and another fan-shaped complementary support mesh sheet.
In above scheme: the semicircle complementary support mesh sheet and fan-shaped complementary support mesh sheet by copper or nickel or molybdenum or gold or Nylon is made.
In above scheme: the shape of the mesh is triangle, circle, rectangle, square, any one in diamond shape Kind.
For beneficial effect the utility model compared in the prior art, the utility model can be before not destroying test sample stability It puts and improves sample preparation efficiency, to achieve the purpose that save time cost.
Detailed description of the invention
Fig. 1 is prior art construction schematic diagram.
Fig. 2 is the structural schematic diagram of the utility model embodiment 1.
Fig. 3 is the structural schematic diagram of embodiment 2.
Fig. 4 is the structural schematic diagram of embodiment 3.
Fig. 5 is the structural schematic diagram of embodiment 4.
Fig. 6 is the structural schematic diagram of embodiment 5.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Embodiment 1 is as shown in Fig. 2, the complementary type loading net used in transmission electron microscope, by two semicircle complementary supports Mesh sheet 1 docks back wall into circle, and it is semicircle complementary along 2, two that the outer ledge of semicircle complementary support mesh sheet 1 is equipped with arc-shaped side The arc-shaped side of mesh sheet 1 is supported to surround a round flange along 2.
The mesh of one of semicircle complementary support mesh sheet 1 is circle, the net of another semicircle complementary support mesh sheet 1 Hole is square, and two semicircle complementary support mesh sheet 1 dock the equal indention in side, and two semicircle complementary support mesh sheet 1 are right Their jagged edge clamping when connecing.
Embodiment 2, as described in Figure 3, the complementary type loading net used in transmission electron microscope, by two semicircle complementary supports Mesh sheet 1 docks back wall into circle, and it is semicircle complementary along 2, two that the outer ledge of semicircle complementary support mesh sheet 1 is equipped with arc-shaped side The arc-shaped side edge of mesh sheet 1 is supported to surround a round flange.It is in linear that two semicircle complementary support mesh sheet 1, which dock side,.
The mesh of one of semicircle complementary support mesh sheet 1 is circle, the net of another semicircle complementary support mesh sheet 1 Hole is square, and the arc-shaped side that two semicircle complementary support mesh sheet 1 dock side passes through along 2 bonds two-sided glue sticking.
Embodiment 3, as described in Figure 4, the complementary type loading net used in transmission electron microscope, by two semicircle complementary supports Mesh sheet 1 docks back wall into circle, and it is semicircle complementary along 2, two that the outer ledge of semicircle complementary support mesh sheet 1 is equipped with arc-shaped side The arc-shaped side edge of mesh sheet 1 is supported to surround a round flange.It is in linear that two semicircle complementary support mesh sheet 1, which dock side,.
The mesh of one of semicircle complementary support mesh sheet 1 is circle, the net of another semicircle complementary support mesh sheet 1 Hole is square, and fluted 2a is arranged along 2 wherein one end in the arc-shaped side that two semicircle complementary support mesh sheet 1 dock side, separately One end be provided with the matched protrusion 2b of groove 2a, splicing when, the protrusion 2b is caught in groove 2a.
Embodiment 4, as described in Figure 5, the complementary type loading net used in transmission electron microscope, by two semicircle complementary supports Mesh sheet 1 docks back wall into circle, and it is semicircle complementary along 2, two that the outer ledge of semicircle complementary support mesh sheet 1 is equipped with arc-shaped side The arc-shaped side edge of mesh sheet 1 is supported to surround a round flange.It is in linear that two semicircle complementary support mesh sheet 1, which dock side,.
The mesh of two semicircle complementary support mesh sheet 1 is rectangular, the arc of two semicircle 1 docking sides of complementary support mesh sheet The upper and lower sides at 2 both ends of shape edge are respectively arranged with card hole, and two semicircle complementary support mesh sheet 1 are connected by U-shaped clamp 4, U-shaped Two supporting legs of clamp 4 are inserted into respectively in adjacent card hole.
Embodiment 5 is as shown in fig. 6, the complementary type loading net used in transmission electron microscope, by four fan-shaped complementary support nets The splicing of piece 3 surrounds circle, and the outer ledge of four fan-shaped complementary support mesh sheet 3 is equipped with arc-shaped side along 2, four fan-shaped complementary branch The arc-shaped side for supportting mesh sheet 3 surrounds a round flange along 2.
The mesh of one of sector complementary support mesh sheet 3 is circle, another fan-shaped 3 mesh of complementary support mesh sheet is positive Rectangular, the mesh of third sector complementary support mesh sheet 3 is triangle, and the mesh of the 4th fan-shaped complementary support mesh sheet 3 is length Rectangular, upper and lower sides of the arc-shaped side of four fan-shaped complementary support mesh sheet 3 along 2 both ends are respectively arranged with card hole, and adjacent sector is mutually It mends support mesh sheet 3 to be connected by U-shaped clamp 4, two supporting legs of U-shaped clamp 4 are inserted into respectively in adjacent card hole.
Semicircle complementary support mesh sheet 1 and fan-shaped complementary support mesh sheet 3 in above embodiments is by copper or nickel or molybdenum or gold Or nylon is made.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art, It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.

Claims (9)

1. a kind of complementary type loading net used in transmission electron microscope, it is characterised in that: by semicircle complementary support mesh sheet or fan Shape complementary support mesh sheet is spliced into disc, and all semicircle complementary support mesh sheet or fan-shaped complementary support mesh sheet have identical Or mesh of different shapes, adjacent semicircle complementary support mesh sheet or adjacent fan-shaped complementary support mesh sheet are clamped by clamping structure It is bonded together together or by glued construction.
2. the complementary type loading net used in transmission electron microscope according to claim 1, it is characterised in that: all semicircle mutual It mends support mesh sheet and fan-shaped complementary support mesh sheet all has mesh of different shapes.
3. the complementary type loading net according to claim 1 or claim 2 used in transmission electron microscope, it is characterised in that: the semicircle The outer ledge of shape complementary support mesh sheet and fan-shaped complementary support mesh sheet is equipped with arc-shaped side edge, all semicircle complementary support nets The arc-shaped side edge of piece and fan-shaped complementary support mesh sheet surrounds a round flange.
4. the complementary type loading net used in transmission electron microscope according to claim 3, it is characterised in that: in the semicircle The upper and lower sides at the both ends on the arc-shaped side edge of complementary support mesh sheet and fan-shaped complementary support mesh sheet are respectively arranged with card hole, and adjacent half Round complementary support mesh sheet is connected with fan-shaped complementary support mesh sheet by U-shaped clamp, and two supporting legs of the U-shaped clamp are inserted into respectively In adjacent card hole.
5. the complementary type loading net used in transmission electron microscope according to claim 3, it is characterised in that: described semicircle mutual The wherein one end setting for mending the arc-shaped side edge of support mesh sheet and fan-shaped complementary support mesh sheet is fluted, and the other end is provided with and groove Matched protrusion, in splicing, the protrusion is caught in groove.
6. the complementary type loading net used in transmission electron microscope according to claim 3, it is characterised in that: described semicircle mutual It mends support mesh sheet and is respectively arranged with protrusion and recess, the fan-shaped complementary branch with the side of docking of another semicircle complementary support mesh sheet The splicing side of support mesh sheet and another fan-shaped complementary support mesh sheet is respectively arranged with protrusion and recess, in multiple fan-shaped complementary support nets When piece splices or when two semicircle complementary support mesh sheet docking, the protrusion is caught in recess.
7. the complementary type loading net used in transmission electron microscope according to claim 6, it is characterised in that: described semicircle mutual That mends support mesh sheet and another semicircle complementary support mesh sheet docks the equal indention in side, the sector complementary support mesh sheet with separately The equal indention in splicing side of one fan-shaped complementary support mesh sheet.
8. the complementary type loading net used in transmission electron microscope according to claim 3, it is characterised in that: described semicircle mutual It mends support mesh sheet and fan-shaped complementary support mesh sheet is made of copper or nickel or molybdenum or gold or nylon.
9. the complementary type loading net used in transmission electron microscope according to claim 8, it is characterised in that: the shape of the mesh Shape is triangle, circle, rectangle, square, any one in diamond shape.
CN201822229095.0U 2018-12-28 2018-12-28 The complementary type loading net used in transmission electron microscope Active CN209372724U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109470730A (en) * 2018-12-28 2019-03-15 重庆大学 One kind complementary type loading net used in transmission electron microscope
CN114088496A (en) * 2021-11-25 2022-02-25 内蒙古工业大学 Device for preparing transmission electron microscope powder sample

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109470730A (en) * 2018-12-28 2019-03-15 重庆大学 One kind complementary type loading net used in transmission electron microscope
CN114088496A (en) * 2021-11-25 2022-02-25 内蒙古工业大学 Device for preparing transmission electron microscope powder sample

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