CN208823983U - A kind of full-automatic part collection device of column chromatography for separation - Google Patents
A kind of full-automatic part collection device of column chromatography for separation Download PDFInfo
- Publication number
- CN208823983U CN208823983U CN201821425150.7U CN201821425150U CN208823983U CN 208823983 U CN208823983 U CN 208823983U CN 201821425150 U CN201821425150 U CN 201821425150U CN 208823983 U CN208823983 U CN 208823983U
- Authority
- CN
- China
- Prior art keywords
- axis
- column chromatography
- test tube
- full
- collection device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
The utility model discloses a kind of full-automatic part collection device of column chromatography for separation, including bottom plate, there is test tube disk above bottom plate, rack for test tube is placed with above test tube disk, is equipped with waste liquid tank on the left of rack for test tube.Bottom plate is vertical with cabinet to be connect, box house is equipped with X-axis slideway, X-axis slideway is vertical with Y-axis suspension arm to be connect, Y-axis slideway is equipped on the right side of Y-axis suspension arm, electromagnetism time switch is connected on Y-axis slideway, the left back top of cabinet is equipped with triple valve, and triple valve is equipped with triple valve input terminal, effective liquid output nozzle, waste liquid and exports nozzle.The present apparatus is designed using square and underslung X-Y move mode, changes pipe registration；It collects solution to separate with circuit, use is safer.By solenoid valve control, the phenomenon of leakage changed in pipe handoff procedure is prevented.The utility model can replace the manually collection to sample, easy to operate, improve work quality and working efficiency, while reducing harm of the organic solvent to experimenter.
Description
Technical field
The utility model belongs to full-automatic part assembling sphere more particularly to a kind of column chromatography for separation is automatically partly collected
Device.
Background technique
When the departments such as scientific research, medical treatment, institution of higher learning and industrial enterprise laboratory carry out liquid chromatogram layer analysis；In petroleum
Chemical field: to just/isoparaffin, paraxylene/other xylene isomers, meta-xylene/other xylene isomers
Separation；In sugar, alcohol separation: fructose/glucose sugar, sorbitol, mannitol, glucose/oligosaccharide, maltose/oligosaccharide, sucrose/
Fructose, glucose, sucrose/molasses, the separation of xylose/arabinose；In pharmaceuticals industry: chiral object separation；In Food Chemistry: rouge
The separation of fat acid；In biochemistry: citric acid, phenylalanine separation；Use column chromatography for separation.In column chromatography for separation experiment,
Generally require interval the short time continuously take many samples, if frequently do condition experiment needs manually look at sampling always, sampling
Interval time is shorter, and people's timing sampling error is bigger, often will cause cross contamination, or sequence confusion, to experimental result shadow
Sound is very big.Task efficiency is limited, and people's Long Term Contact organic solvent increases the harm of body.
Summary of the invention
It is automatically partly received the purpose of this utility model is that providing a kind of column chromatography for separation to solve the above-mentioned problems
Acquisition means.The technical solution is as follows:
A kind of full-automatic part collection device of column chromatography for separation, including bottom plate, are placed with test tube disk above bottom plate, on test tube disk
Fang Fangyou rack for test tube, rack for test tube left side are equipped with waste liquid tank.Bottom plate is vertical with cabinet to be connect, and liquid crystal display is equipped with right above cabinet
And key, box house are equipped with X-axis slideway, X-axis slideway is vertical with Y-axis suspension arm to be connect, and it is sliding that Y-axis is equipped on the right side of Y-axis suspension arm
Road, connects electromagnetism time switch on Y-axis slideway, and electromagnetism time switch is equipped with that electromagnetism time switch is suitable for reading, under electromagnetism time switch
Mouthful, the left back top of cabinet is equipped with triple valve, and triple valve is equipped with triple valve input terminal, effective liquid exports nozzle, waste liquid efferent duct
Mouthful, the right back lower place of cabinet is equipped with power supply and switch.
The triple valve input terminal waits for that collection liquid body mouth is connected with column chromatography for separation by hose.
The electromagnetism time switch by process control electromagnetism time switch；The effective liquid output nozzle by hose with
Electromagnetism time switch is suitable for reading to be connected；Mouth is connected with test tube is collected under the electromagnetism time switch.
The waste liquid output nozzle is connected by hose with waste liquid tank.
The rack for test tube both ends are equipped with handle.
The X-axis slideway includes X screw rod and sliding rail, and X screw rod one end connection X-axis holds piece, and the other end connects X shaft coupling
Device, the X shaft coupling are connected with X stepper motor, and the sliding rail both ends are fixed on X-axis and hold on piece and X shaft coupling, the X screw rod
It is equipped with X sliding block, the X sliding block is equipped with X threaded hole.
The Y-axis suspension arm is fixed on X sliding block by X threaded hole, and sliding rail plays Auxiliary support to Y-axis suspension arm.
The Y-axis slideway includes Y screw rod, and Y screw rod one end connection Y-axis holds piece, and the other end connects Y shaft coupling, the Y
Shaft coupling is connected with Y stepping motor, and the Y screw rod is equipped with Y sliding block, and the Y sliding block is equipped with Y threaded hole.
The electromagnetism time switch is fixed on Y sliding block by Y threaded hole.
Good effect using the above scheme: the utility model can replace the manually collection to sample, and collect sample
It is more accurate, while reducing harm of the organic solvent to experimenter.
Detailed description of the invention
This patent is further described with reference to the accompanying drawings and embodiments:
Attached drawing 1 is the overall structure diagram of the utility model.
Attached drawing 2 is the rear panel schematic diagram of the utility model.
Attached drawing 3 is the X-axis slideway schematic diagram of internal structure of the utility model.
Attached drawing 4 is the Y-axis slideway schematic diagram of internal structure of the utility model.
In figure: 1 key, 2 liquid crystal displays, 3 cabinets, 4 bottom plates, 5X axis slideway, 6Y axle suspension hanger, 7Y axis slideway, 8 electromagnetism
Time switch, 9 electromagnetism time switches are suitable for reading, mouth under 10 electromagnetism time switches, 11 rack for test tubes, 12 waste liquid tanks, 13 test tube disks, and 14
Hand, 15 triple valves, 16 triple valve input terminals, 17 effectively output nozzle, 18 waste liquids export nozzle, 19 power supplys, 20 switches, 21X step
Into motor, 22X shaft coupling, 23X screw rod, 24 sliding rails, 25X sliding block, 26X threaded hole, 27X bearing plate, 28Y stepper motor, 29Y connection
Axis device, 30Y screw rod, 31Y threaded hole, 32Y sliding block, 33Y bearing plate.
Specific embodiment
The utility model is described in further detail with reference to the accompanying drawing, but the protection scope of the utility model is not limited to reality
Apply content described in example.
Refering to fig. 1 shown in -4, a kind of full-automatic part collection device of column chromatography for separation and method, including bottom plate 4, bottom plate 4
Top is placed with test tube disk 13, and rack for test tube 11 is placed with above test tube disk 13, is equipped with waste liquid tank 12 on the left of rack for test tube 11.Bottom plate 4 and case
Body 3 vertically connects, and liquid crystal display 2 and key 1 are equipped with right above cabinet 3, is equipped with X-axis slideway 5, X-axis slideway 5 inside cabinet 3
It is vertical with Y-axis suspension arm 6 to connect, it is equipped with Y-axis slideway 7 on the right side of Y-axis suspension arm 6, connects electromagnetism time switch 8 on Y-axis slideway 7,
Electromagnetism time switch 8 is equipped with that electromagnetism time switch is suitable for reading 9, mouth 10 under electromagnetism time switch, and the left back top of cabinet 3 is equipped with triple valve
15, triple valve 15 is equipped with triple valve input terminal 16, effective liquid output nozzle 17, waste liquid and exports nozzle 18, the right back lower place of cabinet 3
Equipped with power supply 19 and switch 20.
The triple valve input terminal 16 waits for that collection liquid body mouth is connected with column chromatography for separation by hose.
The electromagnetism time switch 8 is the electromagnetism time switch by process control；Effective liquid output nozzle 17 passes through
Hose is connected with electromagnetism time switch suitable for reading 9；Mouth 10 is connected with test tube is collected under the electromagnetism time switch.
The waste liquid output nozzle 18 is connected by hose with waste liquid tank 12.
11 both ends of rack for test tube are equipped with handle 14.
The X-axis slideway 5 includes X screw rod 23 and sliding rail 24, and 23 one end of X screw rod connection X-axis holds piece 27, and the other end connects
X shaft coupling 22 is connect, the X shaft coupling 22 is connected with X stepper motor 21, and 24 both ends of sliding rail are fixed on X-axis and hold piece 27 and X connection
On axis device 22, the X screw rod 23 is equipped with X sliding block 25, and the X sliding block 25 is equipped with X threaded hole 26.
The Y-axis suspension arm 6 is fixed on X sliding block 25 by X threaded hole 26, and sliding rail 24 plays auxiliary branch to Y-axis suspension arm 6
Support effect.
The Y-axis slideway 7 includes Y screw rod 30, and 30 one end of Y screw rod connection Y-axis holds piece 33, and the other end connects Y shaft coupling
Device 29, the Y shaft coupling 29 are connected with Y stepping motor 28, and the Y screw rod 30 is equipped with Y sliding block 32, set on the Y sliding block 32
There is Y threaded hole 31.
The electromagnetism time switch 8 is fixed on Y sliding block 32 by Y threaded hole 31.
It is as follows that process is collected using the full-automatic part collection device of above-mentioned column chromatography for separation:
By in 19 socket of power supply of power-line plug insertion apparatus rear panel, rack for test tube 11 and waste liquid tank 12 are put into test tube
In disk 13, test tube disk 13 is placed on bottom plate 4, and it is leaned on into foot to cabinet 3.It is soft that column chromatography for separation is waited for that collection liquid body mouth passes through
Pipe is connected with triple valve input terminal 16, and effective liquid output nozzle 17 is connected by hose with electromagnetism time switch suitable for reading 9, will be given up
Liquid output nozzle 18 connects hose and is put into waste liquid tank 12.20 are turned on the switch, by the setting of mouth 10 alignment the under electromagnetism time switch
One test tube, setting program, first setting waste liquid section time, then the time that each test tube is collected is set, range is 1 second~99 small
When 59 divide in 59 seconds and be arbitrarily arranged, while being set as needed and collecting test tubes using how many.Start to collect after setting, first
What is started is waste liquid section, and 15 switching three-way valve input terminal 16 of triple valve is connected to waste liquid output nozzle 18 at this time, the waste liquid section time
The main waste collection time useless including emptying time early period and early period, it is discharged into waste liquid tank 12.It is after waste liquid section
Collection section, 15 switching three-way valve input terminal 16 of triple valve is connected to effective output nozzle 17 at this time, and collection liquid is opened from electromagnetism timing
It closes lower mouth 10 and instills first test tube, after the completion of the acquisition time by the single test tube of program setting, electromagnetism time switch 8 is along Y-axis
Slideway 7 is mobile to second, 3 direction of cabinet test tube, and so on, it is collected until completing the last one test tube of Y direction, then Y
Axle suspension hanger 6 is moved to second row test tube along X-axis slideway 5, and mouth 10 is directed at the last one test tube of second row under electromagnetism time switch
Start to collect from back to front, 8 running track of electromagnetism time switch is serpentine track.After completing the test tube number of setting collection, receive
Collection is automatically stopped, and is turned off the switch 20, is successively analyzed sample, disposes waste liquid, and test tube is cleaned.
The utility model is designed using square and underslung X-Y move mode, changes pipe registration；Collect solution and electricity
Road separation, use are safer.By triple valve and control program, waste liquid is automatically flowed into waste liquid tank.By solenoid valve control, prevent
Only change the phenomenon of leakage in pipe handoff procedure.The utility model can replace the manually collection to sample, and collect sample more
Precisely, while harm of the organic solvent to experimenter is reduced.
The above embodiments are only for explaining the technical ideas and features of the present invention, and its object is to allow be familiar with technique
Personage can understand the content of the utility model and implement accordingly, do not limit the protection scope of the present invention.
All equivalent change or modifications according to made by the spirit of the present invention essence, should all cover the protection scope of the utility model it
It is interior.
Claims (9)
1. a kind of full-automatic part collection device of column chromatography for separation, it is characterised in that: including bottom plate (4), be placed with above bottom plate (4)
Test tube disk (13), test tube disk (13) top are placed with rack for test tube (11), are equipped with waste liquid tank (12) on the left of rack for test tube (11)；Bottom plate (4)
Side is vertical with cabinet (3) bottom to be connect, and liquid crystal display (2) and key (1), cabinet (3) top are equipped with right above cabinet (3)
Inside is equipped with X-axis slideway (5), and X-axis slideway (5) is vertical with Y-axis suspension arm (6) to be connect, and it is sliding that Y-axis is equipped on the right side of Y-axis suspension arm (6)
Road (7) connects electromagnetism time switch (8) on Y-axis slideway (7), electromagnetism time switch (8) be equipped with electromagnetism time switch (9) suitable for reading,
Mouth (10) under electromagnetism time switch, cabinet (3) left back top are equipped with triple valve (15), and triple valve (15) is inputted equipped with triple valve
(16), effective liquid output nozzle (17), waste liquid output nozzle (18) are held, cabinet (3) the right back lower place is equipped with power supply (19) and switchs
(20)。
2. the full-automatic part collection device of a kind of column chromatography for separation according to claim 1, it is characterised in that: the threeway
Valve input terminal (16) waits for that collection liquid body mouth is connected with column chromatography for separation by hose.
3. the full-automatic part collection device of a kind of column chromatography for separation according to claim 1, it is characterised in that: the electromagnetism
Time switch (8) is the electromagnetism time switch by process control；Effective liquid output nozzle (17) is fixed by hose and electromagnetism
Shi Kaiguan (9) suitable for reading is connected；Mouth (10) is connected with test tube is collected under the electromagnetism time switch.
4. the full-automatic part collection device of a kind of column chromatography for separation according to claim 1, it is characterised in that: the waste liquid
Output nozzle (18) is connected by hose with waste liquid tank (12).
5. the full-automatic part collection device of a kind of column chromatography for separation according to claim 1, it is characterised in that: the test tube
Frame (11) both ends are equipped with handle (14).
6. the full-automatic part collection device of a kind of column chromatography for separation according to claim 1, it is characterised in that: the X-axis
Slideway (5) includes X screw rod (23) and sliding rail (24), and X screw rod (23) one end connection X-axis is held piece (27), and the other end connects X connection
Axis device (22), the X shaft coupling (22) are connected with X stepper motor (21), and sliding rail (24) both ends are fixed on X-axis and hold piece (27)
On X shaft coupling (22), the X screw rod (23) is equipped with X sliding block (25), and the X sliding block (25) is equipped with X threaded hole (26).
7. the full-automatic part collection device of a kind of column chromatography for separation according to claim 6, it is characterised in that: the Y-axis
Suspension arm (6) is fixed on X sliding block (25) by X threaded hole (26), and sliding rail (24) plays Auxiliary support to Y-axis suspension arm (6) and makees
With.
8. the full-automatic part collection device of a kind of column chromatography for separation according to claim 1, it is characterised in that: the Y-axis
Slideway (7) includes Y screw rod (30), and Y screw rod (30) one end connection Y-axis is held piece (33), and the other end connects Y shaft coupling (29),
The Y shaft coupling (29) is connected with Y stepping motor (28), and the Y screw rod (30) is equipped with Y sliding block (32), the Y sliding block (32)
It is equipped with Y threaded hole (31).
9. the full-automatic part collection device of a kind of column chromatography for separation according to claim 8, it is characterised in that: the electromagnetism
Time switch (8) is fixed on Y sliding block (32) by Y threaded hole (31).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821425150.7U CN208823983U (en) | 2018-08-31 | 2018-08-31 | A kind of full-automatic part collection device of column chromatography for separation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821425150.7U CN208823983U (en) | 2018-08-31 | 2018-08-31 | A kind of full-automatic part collection device of column chromatography for separation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN208823983U true CN208823983U (en) | 2019-05-07 |
Family
ID=66311583
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201821425150.7U Active CN208823983U (en) | 2018-08-31 | 2018-08-31 | A kind of full-automatic part collection device of column chromatography for separation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN208823983U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108786179A (en) * | 2018-08-31 | 2018-11-13 | 中触媒新材料股份有限公司 | A kind of full-automatic part collection device of column chromatography for separation and method |
-
2018
- 2018-08-31 CN CN201821425150.7U patent/CN208823983U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108786179A (en) * | 2018-08-31 | 2018-11-13 | 中触媒新材料股份有限公司 | A kind of full-automatic part collection device of column chromatography for separation and method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101590333B (en) | Nanofiber adsorption based array solid-phase extraction device | |
| US3752651A (en) | Method and apparatus for extraction of solvent extracts | |
| CN206168896U (en) | Appearance bottle automatic cleaning machine and cleaning system are advanced to chromatogram | |
| CN202362187U (en) | Liquid-based cell slide preparation and dyeing machine based on injection pipetting principle | |
| CN208823983U (en) | A kind of full-automatic part collection device of column chromatography for separation | |
| CN111624277A (en) | Full-automatic comprehensive sample pretreatment instrument | |
| CN205538411U (en) | Automatic smear dyeing apparatus | |
| CN211112037U (en) | High-flux nucleic acid extraction system | |
| CN213221055U (en) | Solid phase extraction device | |
| CN201099665Y (en) | Nucleic acid automatic extraction instrument | |
| CN208766031U (en) | A kind of full-automatic heavy metal separation and concentration abstraction instrument | |
| CN101143884B (en) | Nucleic acid automatic extracting instrument | |
| CN108786179A (en) | A kind of full-automatic part collection device of column chromatography for separation and method | |
| CN206362811U (en) | A kind of automatic sampler for quantitative capillary tube electrophoresis apparatus | |
| CN101587127A (en) | Full automatic urine analyzer | |
| CN215611754U (en) | Sample adding box for sampling water quality in water environment monitoring | |
| CN104492773B (en) | Cleaning device for chromatography sample bottle of laboratory | |
| CN205538675U (en) | Portable pesticide residue detector | |
| CN209684273U (en) | A kind of biological reagent storage box | |
| CN203881784U (en) | Novel full-automatic biochemical analyzer | |
| CN218382842U (en) | Full-automatic glycosylated hemoglobin detection device | |
| CN220271238U (en) | Product quality inspection fingerprint analysis device | |
| CN211801028U (en) | Medical science inspection test-tube rack | |
| CN220231746U (en) | Detection device for immunology experiments | |
| CN220525843U (en) | Full-automatic blood analyzer sampling equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant |