CN2074456U - Submersible fat extractor - Google Patents
Submersible fat extractor Download PDFInfo
- Publication number
- CN2074456U CN2074456U CN 90218106 CN90218106U CN2074456U CN 2074456 U CN2074456 U CN 2074456U CN 90218106 CN90218106 CN 90218106 CN 90218106 U CN90218106 U CN 90218106U CN 2074456 U CN2074456 U CN 2074456U
- Authority
- CN
- China
- Prior art keywords
- leaching
- solvent
- pumping
- tube
- sample
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Landscapes
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
The utility model relates to a submersible fat extractor and belongs to an apparatus measuring oil content of the oil-bearing material, such as soybean, etc., and oil content of the cake of the oil-bearing material. The utility model is composed of a condenser, a dissolvent receiver and a dipping-sucking bottom bottle which are sheathed with each other in sequence. The dissolvent receiver is provided with a dissolvent storeroom, a side pipe and a dissolvent reflux pipe which is sheathed with a silicone tube which is provided with a stop liquid clamp. The dipping-sucking bottom bottle is provided with a dipping-sucking bottom bottle flank and a dipping-sucking barrel which is used for placing the sample packet barrel. The sample filter barrel is arranged in the dipping extractor, the upper part of the sample filter barrel is provided with a bale handle, and the bottom of the sample filter barrel is provided with a through hole. The abstracting perch of the sample packet barrel is used for hooking the bale handle of the sample packet barrel and causing the sample packet barrel to be lifted and put down. The vaporization amount of the utility model is 4.5 times larger than that of a Soxhlet's extractor, and the measuring speed is 7 times faster than that of the Soxhlet's extractor.
Description
The utility model belongs to the instrument of oil plants such as measuring soybean and grouts oleaginousness thereof.
General fat-extraction device is the soxhlet apparatus with German chemurgy scholar rope Gus Li Te name at present, be by reflux condensing tube, the flask that has the extractor of side pipe and the splendid attire solvent composition that socket-connects successively, one end of side pipe and the upside of extractor join, the drain pipe of its lower end and extractor joins, the sample that is leached places in the extractor, solvent in the heating flask, its steam is risen by side pipe, through reflux condenser, splash in the sample, after immersion liquid is amassed completely, promptly overflow by the siphon side pipe, all flow in the flask of bottom, circulation repeatedly like this, just available less solvent reaches the purpose of extraction fully, but it exists the flask heating surface area little, the solvent vaporization is slow with backflow, and per minute only has 4 milliliters 145, and the extraction solvent temperature can only remain between 17-18 ℃ in addition, cause the power of impregnation and the dissolving power of sample low, moreover sample is placed in the extractor, need do once intermittent extraction in per 6.5 minutes, complicated operation, efficient is low, also the extraction time greater than eight hours, can not be in time provide science data for instructing to produce.The straight method fat-extraction device that drips of grease Science Institute of former Ministry of Food development, its structure and soxhlet apparatus are roughly the same, the extraction time to the grouts oleaginousness shortened to about 1 hour, but the extraction time to the high oil plants such as soybean of oleaginousness still needs especially when extraction, need add the glass sand with sample equivalent in sample more than 2 hours, bath temperature must keep 97 ℃ constant temperature, be awkward, easily cause instrument damage, power consumption is also big simultaneously.
The purpose of this utility model is to provide a kind of diving fat extractor of fast measuring oil plant fat content.
The purpose of this utility model is to realize like this, be provided with the solvent storeroom on the top of solvent recycler, the silicone tube that has liquid stopping clamp is connected with solvent refluxing pipe two ends, the two ends of the side pipe of solvent recycler communicate with the bottom of solvent storeroom and solvent recovery pipe respectively, the middle part of leaching pumping bottom bottle is provided with the leaching pumping bottom bottle flank, and its bottom is provided with leaching pumping tube, on the sample filtering packet tube bale handle is arranged, under through hole is arranged, be placed in the inner chamber of leaching pumping tube.Condenser, solvent recycler and the leaching pumping bottom bottle formation one that socket-connects successively, sample filtering packet tube extract bar by the condenser top along solvent recycler, and stretch under the leaching pumping bottom bottle through hole and hook the filtering packet tube bale handle and carry or transfer on carrying out.
The middle part of leaching pumping bottom bottle of the present utility model is provided with the leaching pumping bottom bottle flank, the bottom is provided with the leaching pumping tube of energy splendid attire sample filtering packet tube, and with in the potential hot bath under it, to increase end bottle heating surface area, improve the solvent vaporization rate, the per minute evaporating capacity can reach 22 milliliters, be 4.5 times of soxhlet apparatus, the leaching pumping bottom bottle flank is used to store and is soaked the fat of releasing and can not be vaporized, because solvent temperature higher (75 ℃), quickened to sample fatty seepage force and dissolving power, solvent passes through sample, gap between the through hole of filtering packet tube bottom side and sample filtering packet tube and the leaching pumping tube, under the effect of solvent downforce, flow in the leaching pumping bottom bottle flank, in potential hot bath under the leaching pumping tube, thereby quickened the vaporization of solvent, the top of solvent recycler is provided with the solvent storeroom, and communicate by side pipe and the solvent refluxing pipe and the solvent recycler bottom that are with silicone tube, establish liquid stopping clamp on the silicone tube, backflow with the control solvent, the solvent storeroom can be stored the solvent that is cooled and refluxes, the filtering packet tube bale handle is set to be convenient to wash carrying on the filtering packet tube on time, thereby improved the extraction and determination precision, finding speed improves more than seven times than soxhlet apparatus, and data are accurate.
Concrete structure of the present utility model is done further narration in conjunction with the accompanying drawings.
Fig. 1 is the utility model structural drawing.
Have condenser 1 solvent recycler 2 of chilled water inlet 12 and cooling water outlet 13 and the leaching pumping bottom bottle 3 formation one that socket-connects successively, the two ends of solvent recycler 2 are provided with opening, its top is solvent storeroom 15, by solvent refluxing pipe 7, the bottom of side pipe 8 and solvent recycler 2 communicates, and composition one, recirculatory pipe 7 socket-connects with the silicone tube 9 that liquid stopping clamp 10 is housed, the upper end of leaching pumping bottom bottle 3 is an opening, the middle part is provided with leaching pumping bottom bottle flank 14, its underpart is provided with leaching pumping tube 5, and with 1,2 successively socket constitute one, filtering packet tube bale handle 16 is equipped with in the upper end of sample filtering packet tube 4, its bottom is provided with through hole, bag filter 11, in sample be housed place in the sample filtering packet tube 4, sample filtering packet tube 4 places in the leaching pumping tube 5, the sample filtering packet tube extracts bar 6, is stretched for 7 times along the solvent refluxing pipe of solvent recycler 2 by condenser 1 top, hooks 16 pairs of filtering packet tubes of filtering packet tube bale handle and puts on carrying out and put.Principle of work is, at first the bag filter that sample is housed is placed in the sample filtering packet tube 4, in leaching pumping bottom bottle 3, inject solvent (ether) simultaneously, subsequently with solvent recycler, condenser overlaps successively and connects, connect cooling water pipe, at last in 5 times potential 75 ℃ of water-baths of the leaching pumping tube of leaching pumping bottom bottle 3 lower ends, solvent (the ether evaporation point is 35 ℃) is vaporized, enter the 15 continuation risings of solvent storeroom through solvent refluxing pipe 7 and side pipe 8 respectively, solvent through condenser 1 cooling, inject sample filtering packet tube 4 by silicone tube 9 and the solvent refluxing pipe 7 that liquid stopping clamp 10 is housed, bag filter 11 is washed extraction, the potpourri that contains fat and solvent, flow out through the through hole on sample filtering packet tube 4 bottom sides, after the immersion liquid of leaching pumping tube 5 is amassed completely, overflowed into leaching pumping bottom bottle flank 14 places, because fat is different with the solvent evaporation point, solvent is vaporized and becomes steam, fat is then accumulated in leaching pumping bottom bottle flank 14 places, after extraction after a while, extracting bar 6 with filtering packet tube hooks on the filtering packet tube bale handle 16 and carries, sample filtering packet tube 4 is fully washed near solvent refluxing pipe 7, screw liquid stopping clamp 10 then, stop washing, treat residual solvent in the leaching pumping bottom bottle 3 all be vaporized accumulate in the solvent storeroom 15 till, at last each parts is decomposed, leaching pumping bottom bottle 3 is dried with cooling and is weighed, and just can calculate the oil content of sample.
Claims (1)
- A kind of diving fat extractor that constitutes by condenser 1, it is characterized in that solvent recycler 2 tops are provided with a solvent storeroom 15, having the silicone tube 9 of liquid stopping clamp 10 and the two ends of solvent refluxing pipe 7 socket-connects, the two ends of the side pipe 8 of solvent recycler 2, bottom with solvent storeroom 15 and solvent recycler 2 communicates respectively, the middle part of leaching pumping bottom bottle 3 is provided with leaching pumping bottom bottle flank 14, its bottom is provided with leaching pumping tube 5, and constitute one with leaching pumping bottom bottle 3, sample filtering packet tube 4 upper ends are provided with filtering packet tube bale handle 16, through hole is arranged at its bottom, be placed in the inner chamber of leaching pumping tube 5, condenser 1 solvent recycler 2 and the leaching pumping bottom bottle 3 formation one that socket-connects successively, the sample filtering packet tube extracts bar 6 and is carried or transfer along stretching under solvent recycler 2 and leaching pumping bottom bottle 3 mesopores filtering packet tube bale handle 16 hooked up by condenser 1 top, in 5 times potential hot baths of the bottom leaching pumping tube of leaching pumping bottom bottle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90218106 CN2074456U (en) | 1990-08-15 | 1990-08-15 | Submersible fat extractor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90218106 CN2074456U (en) | 1990-08-15 | 1990-08-15 | Submersible fat extractor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN2074456U true CN2074456U (en) | 1991-04-03 |
Family
ID=4896983
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 90218106 Withdrawn CN2074456U (en) | 1990-08-15 | 1990-08-15 | Submersible fat extractor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN2074456U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104458479A (en) * | 2014-12-03 | 2015-03-25 | 宁波检验检疫科学技术研究院 | Device for measuring sediments in crude oil and heavy oil |
| CN106706464A (en) * | 2015-11-13 | 2017-05-24 | 上海纤检仪器有限公司 | Milk fat analyzer |
-
1990
- 1990-08-15 CN CN 90218106 patent/CN2074456U/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104458479A (en) * | 2014-12-03 | 2015-03-25 | 宁波检验检疫科学技术研究院 | Device for measuring sediments in crude oil and heavy oil |
| CN104458479B (en) * | 2014-12-03 | 2017-07-04 | 宁波检验检疫科学技术研究院 | A kind of crude oil and weight oil sediments determine device |
| CN106706464A (en) * | 2015-11-13 | 2017-05-24 | 上海纤检仪器有限公司 | Milk fat analyzer |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206561007U (en) | A kind of automatic cleaning drying device of photovoltaic solar silicon chip | |
| CN1028281C (en) | Dynamically circulating processing apparatus for preparing Chinese medicine | |
| CN113576912A (en) | Extraction element of chinese-medicinal material | |
| CN2074456U (en) | Submersible fat extractor | |
| CN204428853U (en) | A kind of new medicine concentrator | |
| CN216404327U (en) | Device of natural plant essential oil of quick solvent-free extraction | |
| CN2777541Y (en) | Vacuum degassing instrument | |
| CN206292095U (en) | A kind of device based on soxhlet extraction inspection fat content | |
| CN214096855U (en) | Quick wash oil device of rock core | |
| CN207505868U (en) | Vacuum frying dehydration device | |
| CN203281063U (en) | Efficient circulating filtration type drug extraction device | |
| CN221850906U (en) | Steam drying mechanism for producing nitrile latex gloves | |
| CN206934790U (en) | A kind of device for improving backflow efficiency | |
| CN2279946Y (en) | Hot dipping type quick fat extractor | |
| CN207101962U (en) | A kind of outer circulation dual control temperature extraction equipment | |
| CN201115793Y (en) | Miniaturization extracting concentrating machine unit | |
| CN206184040U (en) | Full -automatic closed circulation formula extraction device | |
| CN203989950U (en) | A kind of grease extractor | |
| CN107860635A (en) | Rock core displacement device for washing oil and method | |
| CN204601685U (en) | A kind of full automatic drum type extracts, concentrated and solvent reclaimer | |
| CN221206877U (en) | High-efficient extraction element based on soxhlet draws | |
| CN2693330Y (en) | Automatic extraction apparatus for light extracting agent | |
| CN212864441U (en) | Waste liquid treatment equipment | |
| CN203694656U (en) | Ether recovery device | |
| CN221894937U (en) | Dewatering device of rapeseed oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |