CN104458479B - A kind of crude oil and weight oil sediments determine device - Google Patents

A kind of crude oil and weight oil sediments determine device Download PDF

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Publication number
CN104458479B
CN104458479B CN201410724858.2A CN201410724858A CN104458479B CN 104458479 B CN104458479 B CN 104458479B CN 201410724858 A CN201410724858 A CN 201410724858A CN 104458479 B CN104458479 B CN 104458479B
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oil
funnel
cutting ferrule
condenser
sediments
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CN201410724858.2A
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CN104458479A (en
Inventor
王群威
林振兴
奚中威
刘名扬
陈铁杉
罗川
王豪
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NINGBO JOYSUN TESTING SERVICE CO., LTD.
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Ningbo Institute of Inspection and Quarantine Science Technology
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Abstract

Device is determined the invention discloses a kind of crude oil and weight oil sediments, in addition to there-necked flask, condenser, extracting sleeve and bush support, also water conservancy diversion funnel, two-way funnel and outer sleeve, the bottom of two-way funnel is provided with wireway and profit pipe, the middle mouth grafting of wireway and there-necked flask, profit pipe is connected with oil water separator, and side connector, one of other mouth grafting of side connector and there-necked flask are provided with oil water separator;Therefore the present invention is that a kind of extracting and cooling velocity are fast, extracts sleeve edges and rinse uniform, flask internal solvent will not bumping and reusable crude oil and weight oil sediments measure device.

Description

A kind of crude oil and weight oil sediments determine device
Technical field
The present invention relates to the detection of oil product, and in particular to a kind of crude oil and weight oil sediments determine device.
Background technology
The sediment of oil field definition refers to be present in all precipitations insoluble in regulation solvent in crude oil and heavy oil etc. Or suspension.Sediment or come from crude oil in oil product, or be mixed into transport and process, former oil sediments is difficult to lead to Cross following process effectively to be utilized, and processing cost can be increased, so as to influence crude quality.The precipitate particles in oil product Oil cleaner screen can be blocked, causes fuel feeding not smooth, influence mechanical efficiency;After entering cylinder such as heavy oil, inorganic particle aggravation in sediment The abrasion of cylinder liner-piston group, sediment turns into inorganic little particle after high-temp combustion, high under high-temperature and high-pressure conditions in cylinder Fast blow cylinder surface, declines cylinder surface slickness, causes the reduction of cylinder air-tightness, while these little particles can be attached to Cylinder surface, corrodes to it, and not enough so as to ultimately result in engine power, efficiency declines.Sediment in boiler oil Meeting plug nozzle, causes atomization incomplete, and efficiency of combustion declines, and the inorganic salts that inorganic impurity is formed after high-temp combustion can be gathered In the inner surface of boiler, boiler is heated inequality, and corrosion is produced to it, so that the service life of boiler is influenceed, can when serious The blast of boiler can be caused, the serious person and property injury is caused.Conventional sediment device is in a big conical flask It is linked into extracting sleeve, bottleneck condenser coil(Condenser)Integral structure is sealed and cooled down.There is repetition in this device Property and repeatability it is poor, extracting and cooling velocity it is slow, it is impossible to discharge moisture in time, inconvenient operation, environment-friendly degree it is low lack Point.Publication No. CN102338723A, a kind of entitled crude oil and fuel oil sediments determine the patent of invention of device, flask In increased guiding device, the guiding device include a diameter be slightly smaller than extracting sleeve diameter circular deflector and a connection The connector of deflector and condenser coil, the guiding device is conducive to the flushing of sleeve edges, but because the guiding device is hung Relative position between condenser pipe, with sleeve easily offsets, and is still easily caused sleeve edges and rinses uneven, the moisture in sample Easily flow into the solvent of flask, cause the bumping of solvent.The other guiding device is the improvement in flask, there is space in flask Limit, extracting and cooling velocity are slow.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of extracting and cooling velocity is fast, and extracting sleeve edges rinse equal It is even, flask internal solvent will not bumping crude oil and weight oil sediments determine device.
The present invention solve the technical scheme that is used of above-mentioned technical problem for:A kind of crude oil and weight oil sediments determine dress Put, including there-necked flask, condenser, extracting sleeve and bush support, the condenser is trapezoidal condenser, the trapezoidal condensation Water conservancy diversion funnel is provided between device and the extracting sleeve, the bottom of the trapezoidal condenser is just gone up positioned at the water conservancy diversion funnel Side, the water conservancy diversion funnel is located at directly over the extracting sleeve, and the bush support bottom is provided with two-way funnel, the two-way The bottom of funnel is provided with wireway and profit pipe, the middle mouth grafting of the wireway and the there-necked flask, the profit pipe Oil water separator is connected with, side connector, the side connector and the there-necked flask are provided with the oil water separator One of other mouth grafting, the bottom of the oil water separator is provided with valve, and the trapezoidal condenser is connected with cutting ferrule, institute State and the outer sleeve being placed on outside the bush support be provided between cutting ferrule and the two-way funnel, the outer sleeve with it is described on Cutting ferrule and the two-way funnel are flexibly connected.
Vortex shape guiding gutter is provided with the water conservancy diversion funnel;Vortex shape guiding gutter can preferably allow condensed fluid along set Cylinder edge is flowed into extracting sleeve.
The outer sleeve is spirally connected with the upper cutting ferrule and the two-way funnel.
The outer sleeve and the upper cutting ferrule and the two-way funnel clamping.
The upper cutting ferrule and the two-way funnel are both provided with least two fixed ears connected with screw rod, the outer sleeve In upper cutting ferrule and the two-way funnel described in grafting;Then fixed with the screw rod upper and lower fixed ear that is spirally connected.
Compared with prior art, the advantage of the invention is that a kind of crude oil and weight oil sediments determine device, including three Mouth flask, condenser, extracting sleeve and bush support, condenser are trapezoidal condenser, between trapezoidal condenser and extracting sleeve Water conservancy diversion funnel is provided with, the bottom of trapezoidal condenser is located at directly over water conservancy diversion funnel, and water conservancy diversion funnel is located at directly over extracting sleeve, Bush support bottom is provided with two-way funnel, and the bottom of two-way funnel is provided with wireway and profit pipe, wireway and three mouthfuls of burnings The middle mouth grafting of bottle, profit pipe is connected with oil water separator, is provided with side connector on oil water separator, side connector and three mouthfuls The one of other mouth grafting of flask, the bottom of oil water separator is provided with valve, and trapezoidal condenser is connected with cutting ferrule, upper card The outer sleeve being placed on outside bush support is provided between set and two-way funnel, outer sleeve is with upper cutting ferrule and the activity of two-way funnel even Connect;So extracting is carried out in independent extracting sleeve, and extracting and cooling velocity are fast, and condensate liquid flows into extracting set along water conservancy diversion funnel In cylinder, extracting sleeve edges rinse uniform, and due to Action of Gravity Field, oil and solvent etc. are back to there-necked flask by side connector Interior, moisture is placed in oil water separator bottom, can be discharged, and will not cause flask internal solvent bumping, therefore the present invention is a kind of Extracting and cooling velocity are fast, and extracting sleeve edges rinse uniform, flask internal solvent will not bumping and reusable crude oil and Weight oil sediments determines device.
Brief description of the drawings
Fig. 1 is the structural representation of embodiment 1.
Specific embodiment
The present invention is described in further detail below in conjunction with accompanying drawing, embodiment.
Embodiment 1
A kind of crude oil and weight oil sediments as shown in Figure 1 determines device, including there-necked flask 1(There-necked flask lower section There is electric jacket 13), trapezoidal condenser 2(It is provided with high efficient heat exchanging fan blades), extracting sleeve 3 and bush support 4, trapezoidal condenser 2 with It is provided between extracting sleeve 3 in water conservancy diversion funnel 5, water conservancy diversion funnel 5 and is provided with vortex shape guiding gutter 51, trapezoidal condenser 2 is located at Directly over water conservancy diversion funnel 5, water conservancy diversion funnel 5 is located at directly over extracting sleeve 3, and the bottom of bush support 4 is provided with two-way funnel 6, double The bottom of road funnel 6 is provided with wireway 61 and profit pipe 62, the grafting of middle mouth 11 of wireway 61 and there-necked flask 1, profit pipe 62 are connected with oil water separator 7(Inside there is centrifugation structure), side connector 71, side connector are provided with oil water separator 7 71 are provided with valve 72 with one of other grafting of mouth 12 of there-necked flask 1, the bottom of oil water separator 7, and trapezoidal condenser 2 connects Cutting ferrule 8 is connected to, the outer sleeve 9 being placed on outside bush support 4 is provided between upper cutting ferrule 8 and two-way funnel 6, upper cutting ferrule 8 is equipped with The three upper fixed ears 83 connected with screw rod, two-way funnel 6 is also equipped with fixing ear 63, outer sleeve with three of screw rod connection 9 are plugged in cutting ferrule 8 and two-way funnel 6, are screwed together with ear 83, lower fixed ear 63 is fixed on Jiang of screw rod 10.Flask exists After heating devices heat, so extracting is separated with flask, and extracting is carried out in independent extracting sleeve, and the increase of extracting space is taken out The amount of carrying is big, and trapezoidal condenser contact surface is bigger, and more preferably, extracting and condensation rate speed condensation effect, and water conservancy diversion funnel makes condensate liquid Flowed into extracting sleeve along sleeve edges, sleeve edges rinse uniform, improve extracting benefit, and two-way funnel makes gas-liquid separation, Oil water separator more makes water-oil separating, and moisture is sunk in oil water separator, will not be back in there-necked flask, and solvent would not be sent out Raw bumping, the device is separated due to extracting with flask, and operation is also convenient for.
Embodiment 2
Simply outer sleeve and upper cutting ferrule and two-way funnel clamping substantially the same manner as Example 1, different.
Embodiment 3
Substantially the same manner as Example 1, different simply outer sleeves are spirally connected with upper cutting ferrule and two-way funnel.

Claims (5)

1. a kind of crude oil and weight oil sediments determine device, including there-necked flask, condenser, extracting sleeve and bush support, It is characterized in that the condenser is trapezoidal condenser, water conservancy diversion leakage is provided between the trapezoidal condenser and the extracting sleeve Bucket, the bottom of the trapezoidal condenser is located at directly over the water conservancy diversion funnel, and the water conservancy diversion funnel is being located at the extracting sleeve just Top, the bush support bottom is provided with two-way funnel, and the bottom of the two-way funnel is provided with wireway and profit pipe, institute The middle mouth grafting of wireway and the there-necked flask is stated, the profit pipe is connected with oil water separator, on the oil water separator It is provided with side connector, one of other mouth grafting of the side connector and the there-necked flask, the oil water separator Bottom is provided with valve, and the trapezoidal condenser is connected with cutting ferrule, is provided between the upper cutting ferrule and the two-way funnel The outer sleeve outside the bush support is placed on, the outer sleeve is flexibly connected with the upper cutting ferrule and the two-way funnel.
2. a kind of crude oil as claimed in claim 1 and weight oil sediments determine device, it is characterised in that the water conservancy diversion funnel Inside it is provided with vortex shape guiding gutter.
3. a kind of crude oil as claimed in claim 1 and weight oil sediments determine device, it is characterised in that the outer sleeve with The upper cutting ferrule and the two-way funnel are spirally connected.
4. a kind of crude oil as claimed in claim 1 and weight oil sediments determine device, it is characterised in that the outer sleeve with The upper cutting ferrule and the two-way funnel clamping.
5. a kind of crude oil as claimed in claim 1 and weight oil sediments determine device, it is characterised in that the upper cutting ferrule and The two-way funnel is both provided with least two fixed ears connected with screw rod, and cutting ferrule and described is gone up described in the outer sleeve grafting In two-way funnel, connected with screw rod and fix ear up and down.
CN201410724858.2A 2014-12-03 2014-12-03 A kind of crude oil and weight oil sediments determine device Active CN104458479B (en)

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Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4299798A (en) * 1978-12-19 1981-11-10 Commissariat A L'energie Atomique Apparatus for the treatment of solids by liquids
DE2337917C2 (en) * 1973-07-26 1985-04-18 Blaw-Knox Chemical Plants, Inc., Pittsburgh, Pa. Solvent extraction device for extracting a liquid from a liquid / solid particle mixture
CN87200913U (en) * 1987-01-23 1987-12-02 杨运才 Stirring-extraction device
CN2074456U (en) * 1990-08-15 1991-04-03 敦化市植物油厂 Submersible fat extractor
CN2569868Y (en) * 2002-05-31 2003-09-03 中国石油化工股份有限公司 Test instrument for liquid-solid extraction separation
CN102338723A (en) * 2011-06-01 2012-02-01 中华人民共和国钦州出入境检验检疫局 Apparatus used for determining sediments in crude oil and fuel oil
CN103405943A (en) * 2013-07-26 2013-11-27 中国石油天然气股份有限公司 Multi-stage extractor for separating oil from water in solid
CN103513017A (en) * 2013-09-05 2014-01-15 宁波检验检疫科学技术研究院 Determinator for mechanical impurities in crude oil and petroleum products
CN103792342A (en) * 2014-02-27 2014-05-14 北京英斯派克科技有限公司 Toluene insoluble substance measuring device
CN103837423A (en) * 2014-03-24 2014-06-04 北京英斯派克科技有限公司 Device for simultaneously measuring plurality of types of insoluble substances

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2337917C2 (en) * 1973-07-26 1985-04-18 Blaw-Knox Chemical Plants, Inc., Pittsburgh, Pa. Solvent extraction device for extracting a liquid from a liquid / solid particle mixture
US4299798A (en) * 1978-12-19 1981-11-10 Commissariat A L'energie Atomique Apparatus for the treatment of solids by liquids
CN87200913U (en) * 1987-01-23 1987-12-02 杨运才 Stirring-extraction device
CN2074456U (en) * 1990-08-15 1991-04-03 敦化市植物油厂 Submersible fat extractor
CN2569868Y (en) * 2002-05-31 2003-09-03 中国石油化工股份有限公司 Test instrument for liquid-solid extraction separation
CN102338723A (en) * 2011-06-01 2012-02-01 中华人民共和国钦州出入境检验检疫局 Apparatus used for determining sediments in crude oil and fuel oil
CN103405943A (en) * 2013-07-26 2013-11-27 中国石油天然气股份有限公司 Multi-stage extractor for separating oil from water in solid
CN103513017A (en) * 2013-09-05 2014-01-15 宁波检验检疫科学技术研究院 Determinator for mechanical impurities in crude oil and petroleum products
CN103792342A (en) * 2014-02-27 2014-05-14 北京英斯派克科技有限公司 Toluene insoluble substance measuring device
CN103837423A (en) * 2014-03-24 2014-06-04 北京英斯派克科技有限公司 Device for simultaneously measuring plurality of types of insoluble substances

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
GB/T 6531-86 原油和燃料油中沉淀物测定法(抽提法);国家标准局;《中华人民共和国国家标准》;19860625;第537-540页 *

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Effective date of registration: 20180725

Address after: 315000 228, room 043, 66 Qingyi Road, hi tech Zone, Ningbo, Zhejiang.

Patentee after: NINGBO JOYSUN TESTING SERVICE CO., LTD.

Address before: 315012 Ma Yuan Road, Haishu District, Ningbo, Zhejiang Province, No. 9

Patentee before: Ningbo Institute of Inspection and Quarantine Science Technology

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