CN206642390U - Pyrolkigneous liquid distilling apparatus - Google Patents
Pyrolkigneous liquid distilling apparatus Download PDFInfo
- Publication number
- CN206642390U CN206642390U CN201720294918.0U CN201720294918U CN206642390U CN 206642390 U CN206642390 U CN 206642390U CN 201720294918 U CN201720294918 U CN 201720294918U CN 206642390 U CN206642390 U CN 206642390U
- Authority
- CN
- China
- Prior art keywords
- pipeline
- condenser
- pyrolkigneous liquid
- liquid
- packed tower
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 88
- 238000004821 distillation Methods 0.000 claims abstract description 37
- 238000010992 reflux Methods 0.000 claims abstract description 29
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 22
- 239000007921 spray Substances 0.000 claims description 6
- 239000000945 filler Substances 0.000 claims 1
- 238000007670 refining Methods 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 abstract description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 15
- 238000000034 method Methods 0.000 description 13
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 238000001914 filtration Methods 0.000 description 4
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000000052 vinegar Substances 0.000 description 3
- 235000021419 vinegar Nutrition 0.000 description 3
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- GFAZHVHNLUBROE-UHFFFAOYSA-N 1-hydroxybutan-2-one Chemical compound CCC(=O)CO GFAZHVHNLUBROE-UHFFFAOYSA-N 0.000 description 1
- XSJVWZAETSBXKU-UHFFFAOYSA-N 2-ethoxypropane Chemical class CCOC(C)C XSJVWZAETSBXKU-UHFFFAOYSA-N 0.000 description 1
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 210000000780 bap Anatomy 0.000 description 1
- 229930188620 butyrolactone Natural products 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- LPIQUOYDBNQMRZ-UHFFFAOYSA-N cyclopentenylidene Natural products C1CC=CC1 LPIQUOYDBNQMRZ-UHFFFAOYSA-N 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 230000002363 herbicidal effect Effects 0.000 description 1
- 239000004009 herbicide Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- RGSFGYAAUTVSQA-UHFFFAOYSA-N pentamethylene Natural products C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 1
- 230000000361 pesticidal effect Effects 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A kind of distilling apparatus is the utility model is related to, particularly a kind of pyrolkigneous liquid distilling apparatus.Distillation still uses jacket type structure, and chuck is connected with packed tower built with conduction oil, distillation still top, and packed tower is connected with condenser, and condenser is connected by reflux pump with active carbon filter, and active carbon filter is connected with acetum pyrolignosum rectificatum liquid storage tank.Compared with prior art, during being refined to pyrolkigneous liquid, without needing to add any compound, and indirect steam is not had into pyrolkigneous liquid, it is possible to increase pyrolkigneous liquid refines purity.
Description
Technical field
A kind of distilling apparatus is the utility model is related to, particularly a kind of pyrolkigneous liquid distilling apparatus.
Background technology
Pyrolkigneous liquid is obtained in dry distillation of wood equipment after the derived condensed separation of steam gas mixture with smoked smelly
The russet liquid of taste, it is a kind of based on acetic acid, the mixture containing many kinds of substance such as alcohol, phenol, ketone, aldehyde and its derivatives.
Because pyrolkigneous liquid has desinsection, sterilization, disinfection soil, eliminates that excrement is smelly, anti-corrosive fresh-keeping, promotes plant and edible mushroom life
The effect such as long, has obtained extensive use：Can be as fertilizer synergist, multi-effect pesticidal preparations, the insecticide of vinegar liquid extraction, life
Material resource herbicide etc..
Pyrolkigneous liquid is mainly organic by the alcohol such as water, methanol, formaldehyde, acetone, acetic acid, furfural, phenol, acid, phenol and Keto-aldehyde class
Thing forms.In organic matter, with the content highest of acid compounds, its form again because the difference of destructive distillation raw material type have it is very big
Difference.
After refined to pyrolkigneous liquid, sample separate using GC/MS qualitative, the main component verified includes：
93.97% water, 2.87% acetic acid, 0.41% propionic acid, 0.84% 1- hydroxyl -2- butanone, 0.08% 2- ethoxy propanes,
0.69% furfural, 0.09%2- cyclopentene -1- ketone, 0.05%3- picolines, 0.77% butyrolactone, 0.07% 3- hydroxyls -
2- butanone, 0.16% other compositions.Contain a large amount of tar, phenol, methanol, formaldehyde, 3,4- BaPs etc. in crude pyroligneous acid,
Need to further it be refined according to different purposes.
Several pyrolkigneous liquid process for purification：Settled process, the way of distillation, filtration method, distribution method, active carbon adsorption, organic solvent
Extraction, electrolysis, alkali heavy acid extracting and updating device method etc..Wherein settled process is the simplest method of acetum pyrolignosum rectificatum liquid, essence
Effect processed is good, and shortcoming is to take long enough；The way of distillation has air-distillation and is evaporated under reduced pressure two methods, to containing large quantity of moisture
Pyrolkigneous liquid can use in general non-pressure process, but in order to obtain required active pyrolkigneous liquid cut, it is preferable with being evaporated under reduced pressure.
Utility model content
The purpose of this utility model is to provide a kind of pyrolkigneous liquid distilling apparatus using distillation mode, and the device is distilling
During will not produce indirect steam and refine purity, the addition without any compound into pyrolkigneous liquid, improving pyrolkigneous liquid.
The utility model adopts the following technical scheme that：
A kind of pyrolkigneous liquid distilling apparatus, including distillation still, packed tower, reflux pump, condenser, acetum pyrolignosum rectificatum liquid storage tank, steam
Evaporate kettle and use jacket type structure, chuck is connected with packed tower built with conduction oil, distillation still top, and packed tower connects with condenser
Connect, condenser is connected by reflux pump with active carbon filter, and active carbon filter is connected with acetum pyrolignosum rectificatum liquid storage tank.
The utility model of above-mentioned technical proposal, during being refined to pyrolkigneous liquid, without needing to add any fill out
Add agent, and do not have indirect steam and enter in pyrolkigneous liquid, it is possible to increase pyrolkigneous liquid refines purity.
The utility model uses following optimal technical scheme：
Conduction oil is connected by pipeline with external world's circulation.
Packed tower is bi-directionally connected with distillation still.
Packed tower top pipeline is connected with condenser by pipeline.
Condenser lower end is connected by pipeline with two reflux pumps coupled parallel, and converging on two reflux pumps divides on pipeline
It is set to three pipelines：Wherein first pipeline is connected with the spray equipment in packed tower, second pipeline and active carbon filter
Connection, the 3rd pipeline are connected with condenser.
Active carbon filter is connected by pipeline with acetum pyrolignosum rectificatum liquid storage tank, and acetum pyrolignosum rectificatum liquid storage tank connects with preparing liquid bath
Connect.
Acetum pyrolignosum rectificatum liquid pump is provided with acetum pyrolignosum rectificatum liquid storage tank.
Distillating method, adopt the following technical scheme that：
Distillating method, carry out as follows：
Conduction oil is entered by pipeline in the chuck of distillation still bottom, and conduction oil is returned by distillation still chuck top by pipeline
Stream；Crude pyroligneous acid is entered in distillation still kettle by pipeline, is entered after being heated by distillation still in packed tower, by being come out in packed tower
Pyrolkigneous liquid enter condenser in, after being condensed by condenser in by reflux pump enter active carbon filter in, by active carbon filtration
Out acetum pyrolignosum rectificatum liquid enters in acetum pyrolignosum rectificatum liquid storage tank in filter；Acetum pyrolignosum rectificatum liquid in acetum pyrolignosum rectificatum liquid storage tank, which enters, matches somebody with somebody
In liquid storage tank processed, corresponding preparations are prepared as needed.
The preferred scheme of distillating method is：
Acetum pyrolignosum rectificatum liquid in acetum pyrolignosum rectificatum liquid storage tank is squeezed into by acetum pyrolignosum rectificatum liquid pump to be prepared in storage tank.
A part of pyrolkigneous liquid come out by condenser is squeezed into packed tower by the effect of reflux pump via the first pipeline, separately
A part squeezes into condenser via the 3rd pipeline；Part III squeezes into active carbon filter through reflux pump by the second pipeline
In.
Need the crude pyroligneous acid of re-distillation to pass back into distillation still again to be distilled by what packed tower inner bottom part came out.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Embodiment
Below in conjunction with the accompanying drawings and the utility model is described in detail in embodiment：
A kind of pyrolkigneous liquid distilling apparatus, distillation still 1, packed tower 2, condenser 3, the first reflux pump 4, the second reflux pump 5, work
Property carbon filter 6, acetum pyrolignosum rectificatum liquid storage tank 7, acetum pyrolignosum rectificatum liquid pump 8, prepare liquid bath 9, the first pipeline 10, the second pipe kind 11, the
Three pipelines 12, spray equipment 13.
In the present embodiment, distillation still 1 uses jacket type structure, and the temperature in distillation still 1 can reach 160 DEG C, distillation still 1
Interior pressure is in 0.15Mpa or so, and for chuck built with conduction oil, the temperature of conduction oil can make the vapor (steam) temperature in distillation still 1
Reach 100 to 130 DEG C, crude pyroligneous acid can be made smoothly to evaporate.
Conduction oil is entered by pipeline in the lower end chuck layer of distillation still 1, and conduction oil is by pipeline from the top of distillation still 1
Flowed out in chuck, conduction oil passes through double-deck net filtration before entering in chuck.
Distillation still 1 is also automatically controlled by temperature controller A.T.C, liquid level etc. placed on it using control system.
The top of distillation still 1 is connected with packed tower 2, and pyrolkigneous liquid is played shunting action by packed tower 2；Pressure in packed tower 2
It is about 0.1Mpa or so, about 120 DEG C or so of temperature in packed tower, packed tower 2 is connected with condenser 3, and condenser 3 passes through
Reflux pump is connected with packed tower 2, reflux pump itself and active carbon filter 6 respectively, and active carbon filter 6 stores up with acetum pyrolignosum rectificatum liquid
Tank 7 connects.
Conduction oil is connected by pipeline with external world's circulation；Packed tower 2 and the diconnected of distillation still 1.The top pipeline of packed tower 2
It is connected with condenser 3 by pipeline.
The condensing temperature value of condenser 3 is about how many 30 DEG C, is cooled down by cooling water circulation.
The lower end of condenser 3 passes through pipeline and two reflux pumps coupled parallel：First reflux pump 4 and the second reflux pump 5 connect
Connect, converging on two reflux pumps splits into three pipelines on pipeline：Wherein the first pipeline 10 and the spray equipment in packed tower 2
12 connections, spray equipment 12 are located at the middle and upper part in packed tower 2, and spray equipment 12 in distillation still 1 by by entering in packed tower 2
Pyrolkigneous liquid is purified again, settles heavy substance therein, advantageously in the refined of pyrolkigneous liquid.Second pipeline 11 and activity
Carbon filter 6 is connected, and the 3rd pipeline 11 is connected with the bottom of condenser 3；Part pyrolkigneous liquid is returned condenser by the 3rd pipeline,
Primarily to avoiding the lift of reflux pump bigger, part pyrolkigneous liquid is set to be back in packed tower 2 or be directly entered activated carbon
Pressure in filter 6 is excessive and sets, and plays a part of shunting decompression.
The lift of reflux pump is 30 meters, and the scope of design of reflux pump is at 1 cube m/h, using centrifugal pump；Distillation still 1,
The parts that the associated pipes such as liquid level gauge and flowmeter must be equipped with are respectively provided with packed tower 2 and condenser 3.
Active carbon filter 6 is connected by pipeline with acetum pyrolignosum rectificatum liquid storage tank 7, and acetum pyrolignosum rectificatum liquid storage tank 8 is with preparing liquid bath 9
Connection.Acetum pyrolignosum rectificatum liquid pump 8 is provided with acetum pyrolignosum rectificatum liquid storage tank 7.
Distillating method is carried out as follows：
Conduction oil is entered by pipeline in the chuck of the bottom of distillation still 1, and conduction oil is returned by the chuck top of distillation still 1 by pipeline
Stream；Crude pyroligneous acid is entered in the kettle of distillation still 1 by pipeline, is entered after being heated by distillation still 1 in packed tower 2, by packed tower 2
Pyrolkigneous liquid out enters in condenser 3, and a part of pyrolkigneous liquid come out by condenser 3 is by the effect of reflux pump via first
Pipeline 10 is squeezed into packed tower 2, and another part is squeezed into condenser 3 via the 3rd pipeline 12；Part III passes through through reflux pump
Second pipeline 11 is squeezed into active carbon filter 6.
Entered in after being condensed by condenser 3 by reflux pump in active carbon filter 6, by going out in activated carbon filtration filter 6
Carry out acetum pyrolignosum rectificatum liquid to enter in acetum pyrolignosum rectificatum liquid storage tank 7；Acetum pyrolignosum rectificatum liquid in acetum pyrolignosum rectificatum liquid storage tank 7, which enters, prepares liquid storage tank
In 9, corresponding preparations are prepared as needed.
Acetum pyrolignosum rectificatum liquid in acetum pyrolignosum rectificatum liquid storage tank 8 is squeezed into by acetum pyrolignosum rectificatum liquid pump 8 to be prepared in liquid storage tank 9.
Need the crude pyroligneous acid of re-distillation to pass back into again in distillation still 1 to be steamed by what the inner bottom part of packed tower 2 came out
Evaporate.
This vinegar liquid beaten inside packed tower 2 is pumped into addition to playing a part of heavy substance sedimentation by backflow, also participated in first
Enter into the liquid stream in packed tower 2 and delivered to again by pipeline in condenser 3, the wooden vinegar squeezed into by reflux pump inside condenser 3
Liquid participation first enters into the liquid stream in condenser and entered in reflux pump, is delivered to respectively by three different pipelines by reflux pump
In packed tower 2, condenser 3 and active carbon filter 6.
In the utility model, be not limited to enumerating for said structure and method, every agent structure using the present apparatus and
Compound is added without, the mode of indirect steam entrance is not produced, is accordingly to be regarded as within the scope of protection of the utility model.
Claims (7)
1. a kind of pyrolkigneous liquid distilling apparatus, including distillation still, packed tower, reflux pump, condenser, acetum pyrolignosum rectificatum liquid storage tank, it is special
Sign is：Distillation still uses jacket type structure, and chuck is connected with packed tower built with conduction oil above distillation still, packed tower with
Condenser is connected, and condenser is connected by reflux pump with active carbon filter, and active carbon filter connects with acetum pyrolignosum rectificatum liquid storage tank
Connect.
2. pyrolkigneous liquid distilling apparatus according to claim 1, it is characterised in that：Conduction oil is connected by pipeline and extraneous circulation
It is logical.
3. pyrolkigneous liquid distilling apparatus according to claim 1, it is characterised in that：Packed tower is bi-directionally connected with distillation still.
4. pyrolkigneous liquid distilling apparatus according to claim 1, it is characterised in that：Packed tower top pipeline passes through with condenser
Pipeline connects.
5. pyrolkigneous liquid distilling apparatus according to claim 1, it is characterised in that：Condenser lower end by pipeline and two simultaneously
The reflux pump of row connection connects, and converging on two reflux pumps splits into three pipelines on pipeline：Wherein first pipeline and filler
Spray equipment connection in tower, second pipeline are connected with active carbon filter, and the 3rd pipeline is connected with condenser.
6. pyrolkigneous liquid distilling apparatus according to claim 1, it is characterised in that：Active carbon filter is by pipeline with refining
Pyrolkigneous liquid storage tank is connected, and acetum pyrolignosum rectificatum liquid storage tank is connected with preparing liquid bath.
7. pyrolkigneous liquid distilling apparatus according to claim 1, it is characterised in that：It is provided with acetum pyrolignosum rectificatum liquid storage tank refined
Pyrolkigneous liquid pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720294918.0U CN206642390U (en) | 2017-03-24 | 2017-03-24 | Pyrolkigneous liquid distilling apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720294918.0U CN206642390U (en) | 2017-03-24 | 2017-03-24 | Pyrolkigneous liquid distilling apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206642390U true CN206642390U (en) | 2017-11-17 |
Family
ID=60279961
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720294918.0U Expired - Fee Related CN206642390U (en) | 2017-03-24 | 2017-03-24 | Pyrolkigneous liquid distilling apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206642390U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106823436A (en) * | 2017-03-24 | 2017-06-13 | 唐山赫潼生物质能源开发有限公司 | Pyrolkigneous liquid distilling apparatus and distillating method |
-
2017
- 2017-03-24 CN CN201720294918.0U patent/CN206642390U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106823436A (en) * | 2017-03-24 | 2017-06-13 | 唐山赫潼生物质能源开发有限公司 | Pyrolkigneous liquid distilling apparatus and distillating method |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171117 |
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| CF01 | Termination of patent right due to non-payment of annual fee |