CN107903929A - A kind of natural high-quality bamboo vinegar and preparation method thereof - Google Patents
A kind of natural high-quality bamboo vinegar and preparation method thereof Download PDFInfo
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- CN107903929A CN107903929A CN201711189530.5A CN201711189530A CN107903929A CN 107903929 A CN107903929 A CN 107903929A CN 201711189530 A CN201711189530 A CN 201711189530A CN 107903929 A CN107903929 A CN 107903929A
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- bamboo
- vinegar
- charcoal
- wood
- bamboo wood
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Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10C—WORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
- C10C5/00—Production of pyroligneous acid distillation of wood, dry distillation of organic waste
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10B—DESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
- C10B53/00—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form
- C10B53/02—Destructive distillation, specially adapted for particular solid raw materials or solid raw materials in special form of cellulose-containing material
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Abstract
The invention discloses a kind of natural high-quality bamboo vinegar and preparation method thereof, bamboo vinegar is the byproduct for firing bamboo charcoal, it is during being made charcoal with bamboo wood, collects volatile, water-soluble gas that bamboo wood produces in high temperature pyrolysis, and the liquid substance that this gas is cooled down at normal temperatures.Its composition is considerably complicated, and containing nearly 300 kinds of natural polymer organic compounds, main component is water, organic acid, alcohols, ketone, aldehydes, esters and micro alkaline components etc..Bamboo vinegar output of fluid is then with the different and different of the species of bamboo wood, the moisture content of bamboo wood and pyrolytic process, its component more with the difference of collection method, pyrolysis temperature, storage requirement etc. and difference.Bamboo-vinegar without refining spearation is 1.01~1.05kg/L generally in rufous or dark brown, density, there is the distinctive smoke aroma of bamboo vinegar.This method preparation method is easy to operate, relatively low without special installation, short preparation period, cost.
Description
Technical field
The invention belongs to pharmaceutical synthesis field, and in particular to a kind of natural high-quality bamboo vinegar and preparation method thereof.
Background technology
Bamboo vinegar is the product liquid that bamboo wood is pyrolyzed, it is a kind of considerably complicated liquid mixture of constituent,
Its main component is the materials such as water, organic acid, phenols, ketone, alcohols, its forming process is very complicated.Bamboo vinegar output of fluid then with
The species of bamboo wood, the moisture content of bamboo wood and pyrolytic process it is different and different, its component is more with collection method, pyrolysis temperature, storage
Deposit the different of condition etc. and constantly change.
Bamboo vinegar has many functions, its tissue to plant and animal has good permeability and absorbability, to domestic animal
Excrement and garbage stench also have eliminate effect.In terms of bamboo vinegar can also play the role of plant hormone, give
Crop adds micro bamboo vinegar, then can play and promote plant establishment, germination, growth, the effect for making the taste of fruit improve.
In short, it can be widely applied to each fields such as agricultural, medical treatment, health care.
Japan and Taiwan prove that bamboo vinegar has the fungies such as the ringworm of the foot, O157, Escherichia coli and aftosa, bird flu etc.
Good antibacterial and function of killing the virus, and develop the product that Gui is answered.Bamboo vinegar is to " three high ", gout and prostate, tumour etc.
The Hao Twin fruits of You compare.Meanwhile also it is applied to using the Thief zone thunderbolt effect of bamboo vinegar in pharmaceutical production.Japanese document is introduced such as
Under：
(1) hyperglycaemia.Wide graduate golden Mr. Wu Chaochun of rugged bioscience is tested with mouse, gives mouse alloaxantin,
Diabetes are sent out, complicated cataract.But raised with the acetum pyrolignosum rectificatum liquid for being diluted to 5%, give the diabetes obstacle after alloaxantin
Just it can't see.
(2) hypertension.Drink the bamboo vinegar distilled water after a bottle cap dilution every morning.Although there is individual difference, 2- numbers
After month, blood pressure can decline really.Bamboo vinegar can prevent the decomposition synthesized and promote fat of fat.In addition to excessively salty
The intake divided is also effective.Due to bamboo vinegar diuresis effect, unnecessary salinity just can be from internal discharge.
(3) hyperlipidemia.Artery sclerosis is the disease of the blood flow obstructions in artery.Cholesterol in artery is with middle thunderbolt fat
Fat is accumulated, and is protruded as tumour, due to wastes such as fatty peracid compounds, is caused blood vessel aging.That is endarterial blood
Pipe flow obstacle, as long as cleaning blood vessel, makes blood flow smooth all right.The acid of bamboo vinegar just plays the role of this big fill.
(4) gout.Same experiment, which also demonstrates wood vinegar, the reason for suppressing gout-uric acid poison Ting Twin fruits, concurrently
Table.Same experiment, also confirms and delivers the origin cause of formation of the wood vinegar to gout of knowing clearly --- the malicious thunderbolt of uric acid has inhibitory action.Bamboo
Vinegar will play the part of important role in the modernization of Chinese medicine.
The product of above-mentioned 4 types, the country there is no report.
The production method of bamboo vinegar has 3 kinds:One kind is the direct firing process of earth kiln, and equipment cost is low, to bamboo charcoal, bamboo after improvement
The quality and the rate of recovery of vinegar liquid all increase；It is retort pyrolysismethod in second, point fixed destructive distillation and moving bed are continuously done
Two classes are evaporated, the exhaust gas that some type of furnaces and technique produce can be used as fuel, and bamboo vinegar quality and yield are better than the former；The third is
With special equipment the preparation method, the type of furnace is small, and links accurately can be controlled.
The content of the invention
The purpose of the present invention is to solve each manufacturer's raw material sources of tradition, production equipment, technology etc. no
Together, product quality is uneven, and some also infiltrates the wood vinegar component such as wood tar, into a kind of mixed type bamboo vinegar, shadow
Ring its application field.In order to improve and stablize the quality of bamboo vinegar, it is ensured that it is safe to use, expand application field, this research from
Bamboo vinegar raw materials for production, production equipment, collection process, storage method and process for purification etc. are explored, and make every effort to acquisition one
The production of kind high-purity bamboo vinegar and processing technology.
The present invention provides a kind of natural high-quality bamboo vinegar and preparation method thereof, takes 5~6 tons of fresh feed through preliminary
The bamboo vinegar of isolated 1 ton of bamboo charcoal and 300~600kg, general bamboo vinegar are divided into three classes according to temperature is collected：Less than 90 DEG C
For low temperature bamboo vinegar, the medium temperature bamboo vinegar for being between 90~120 DEG C, is high temperature bamboo vinegar higher than 120 DEG C.The first bamboo vinegar obtained
Liquid is brown, and after standing, upper strata is clarification bamboo vinegar, and lower sediment be bamboo tar, then clarified solution substep is refined.Initial gross separation
Frequently with settled process, organic solvent extractionprocess, common bamboo charcoal is further refined, Activated Carbon Adsorption Separation, reuses distillation, rectifying
Technique purifies.
As preferred means, preparation method comprises the following steps：1) the crooked termination precision pulling that will be formed when felling bamboo
Bench saw is clipped, and using port as positioning surface, raw bamboo is cut into fixed length thick bamboo tube, is broken thick bamboo tube with broken bamboo machine, then will be cut with slicer
It is 1-4mm into thickness, width is the bamboo chip of 10-25mm, while removes that bamboo is blue or green and tabasheer, bamboo green grass or young crops thickness are processed in 1-3mm
The bamboo scraps that process produces；2) bamboo charcoal is dry, bamboo wood carbonizes in advance, bamboo wood carbonized, bamboo charcoal are calcined and five stages of cooling；3) using quiet
Put method, organic solvent extractionprocess carries out initial gross separation to bamboo-vinegar；4) simple distillation：Mixture to be separated is loaded into distillation
In kettle, heating and part are evaporated.The steam released by distillation still is imported in condenser, due to cooling effect steam within the condenser
It is changed into liquid, the distillate of generation flows into collector.5) rectification and purification：Utilize the steam generated in distillation equipment and previously steaming
The steam gone out, partial condensation obtain phegma, and smoke is removed with resin adsorption, that is, obtain natural high-quality refined bamboo vinegar production
Product.
As further preferred means, the concrete technology of the step 2) is：
Bamboo wood is dried：The red-hot flue gas produced using fuel combustion carries out fumigation drying, generally needs one week or so time.This
When, the temperature in charcoal kiln is generally less than 150 DEG C, mainly removes the moisture in bamboo wood, makes the geomery of bamboo wood be not easy to change
Become.If the drying of bamboo wood is separately carried out, it is necessary to separately build bamboo wood smoke kiln with the process made charcoal.
Bamboo wood carbonizes in advance：At this moment 150 DEG C~270 DEG C of the temperature in charcoal kiln, bamboo wood by thermally decompose it is obvious, start to produce
Raw acetic acid and tar.
Bamboo wood carbonized：Very fast thermal decomposition occurs at this moment 270 DEG C~360 DEG C of the temperature in charcoal kiln, bamboo wood, produces a large amount of
Catabolite, be the natural polymer product such as acetic acid, tar Main Stage.Within this stage, since bamboo wood is very fast
Thermal decomposition, release substantial amounts of heat.
Bamboo charcoal is calcined：At this moment more than 360 DEG C of the temperature in charcoal kiln.In this stage, with the lasting progress of high temperature, residual
The exclusion that the material that can be volatilized in bamboo charcoal obtains, but produce gas-condensate liquid --- bamboo vinegar is seldom.
Embodiment
Embodiment 1
A kind of natural high-quality bamboo vinegar and preparation method thereof, comprises the following steps：
1) the crooked termination formed when felling bamboo is clipped with precision pulling bench saw, using port as positioning surface, raw bamboo is cut into
Fixed length thick bamboo tube, is broken thick bamboo tube with broken bamboo machine, then it is 1-4mm that will be cut into thickness with slicer, and width is the bamboo chip of 10-25mm, together
When remove that bamboo is blue or green and tabasheer, bamboo green grass or young crops thickness obtain the bamboo scraps of process generation in 1-3mm；
2) bamboo charcoal is dry, bamboo wood carbonizes in advance, bamboo wood carbonized, bamboo charcoal are calcined and five stages of cooling；
Bamboo wood is dried：The red-hot flue gas produced using fuel combustion carries out fumigation drying, generally needs one week or so time.This
When, the temperature in charcoal kiln is generally less than 150 DEG C, mainly removes the moisture in bamboo wood, makes the geomery of bamboo wood be not easy to change
Become.If the drying of bamboo wood is separately carried out, it is necessary to separately build bamboo wood smoke kiln with the process made charcoal.
Bamboo wood carbonizes in advance：At this moment 150 DEG C of the temperature in charcoal kiln, bamboo wood by thermally decompose it is obvious, start produce acetic acid
And tar.
Bamboo wood carbonized：Very fast thermal decomposition occurs at this moment 270 DEG C of the temperature in charcoal kiln, bamboo wood, produces substantial amounts of decompose
Product, is the Main Stage of the natural polymer product such as acetic acid, tar.Within this stage, due to bamboo wood very fast heat point
Solution, releases substantial amounts of heat.
Bamboo charcoal is calcined：At this moment more than 360 DEG C of the temperature in charcoal kiln.In this stage, with the lasting progress of high temperature, residual
The exclusion that the material that can be volatilized in bamboo charcoal obtains, but produce gas-condensate liquid --- bamboo vinegar is seldom.
3) initial gross separation is carried out to bamboo-vinegar using settled process, organic solvent extractionprocess；
4) simple distillation：Mixture to be separated is loaded in distillation still, heating and part are evaporated.Released by distillation still
Steam is imported in condenser, and since cooling effect steam is changed into liquid within the condenser, the distillate of generation flows into collector；
5) rectification and purification：Using the steam generated in distillation equipment and the steam previously steamed, partial condensation is flowed back
Liquid, removes smoke with resin adsorption, that is, obtains natural high-quality refined bamboo vinegar product.
Embodiment 2
A kind of natural high-quality bamboo vinegar and preparation method thereof, comprises the following steps：
1) the crooked termination formed when felling bamboo is clipped with precision pulling bench saw, using port as positioning surface, raw bamboo is cut into
Fixed length thick bamboo tube, is broken thick bamboo tube with broken bamboo machine, then it is 1-4mm that will be cut into thickness with slicer, and width is the bamboo chip of 10-25mm, together
When remove that bamboo is blue or green and tabasheer, bamboo green grass or young crops thickness obtain the bamboo scraps of process generation in 1-3mm；
2) bamboo charcoal is dry, bamboo wood carbonizes in advance, bamboo wood carbonized, bamboo charcoal are calcined and five stages of cooling；
Bamboo wood is dried：The red-hot flue gas produced using fuel combustion carries out fumigation drying, generally needs one week or so time.This
When, the temperature in charcoal kiln is generally less than 150 DEG C, mainly removes the moisture in bamboo wood, makes the geomery of bamboo wood be not easy to change
Become.If the drying of bamboo wood is separately carried out, it is necessary to separately build bamboo wood smoke kiln with the process made charcoal.
Bamboo wood carbonizes in advance：At this moment 150 DEG C of the temperature in charcoal kiln, bamboo wood by thermally decompose it is obvious, start produce acetic acid
And tar.
Bamboo wood carbonized：Very fast thermal decomposition occurs at this moment 300 DEG C of the temperature in charcoal kiln, bamboo wood, produces substantial amounts of decompose
Product, is the Main Stage of the natural polymer product such as acetic acid, tar.Within this stage, due to bamboo wood very fast heat point
Solution, releases substantial amounts of heat.
Bamboo charcoal is calcined：At this moment more than 360 DEG C of the temperature in charcoal kiln.In this stage, with the lasting progress of high temperature, residual
The exclusion that the material that can be volatilized in bamboo charcoal obtains, but produce gas-condensate liquid --- bamboo vinegar is seldom.
3) initial gross separation is carried out to bamboo-vinegar using settled process, organic solvent extractionprocess；
4) simple distillation：Mixture to be separated is loaded in distillation still, heating and part are evaporated.Released by distillation still
Steam is imported in condenser, and since cooling effect steam is changed into liquid within the condenser, the distillate of generation flows into collector；
5) rectification and purification：Using the steam generated in distillation equipment and the steam previously steamed, partial condensation is flowed back
Liquid, removes smoke with resin adsorption, that is, obtains natural high-quality refined bamboo vinegar product.
Embodiment 3
A kind of natural high-quality bamboo vinegar and preparation method thereof, comprises the following steps：
1) the crooked termination formed when felling bamboo is clipped with precision pulling bench saw, using port as positioning surface, raw bamboo is cut into
Fixed length thick bamboo tube, is broken thick bamboo tube with broken bamboo machine, then it is 1-4mm that will be cut into thickness with slicer, and width is the bamboo chip of 10-25mm, together
When remove that bamboo is blue or green and tabasheer, bamboo green grass or young crops thickness obtain the bamboo scraps of process generation in 1-3mm；
2) bamboo charcoal is dry, bamboo wood carbonizes in advance, bamboo wood carbonized, bamboo charcoal are calcined and five stages of cooling；
Bamboo wood is dried：The red-hot flue gas produced using fuel combustion carries out fumigation drying, generally needs one week or so time.This
When, the temperature in charcoal kiln is generally less than 150 DEG C, mainly removes the moisture in bamboo wood, makes the geomery of bamboo wood be not easy to change
Become.If the drying of bamboo wood is separately carried out, it is necessary to separately build bamboo wood smoke kiln with the process made charcoal.
Bamboo wood carbonizes in advance：At this moment 150 DEG C of the temperature in charcoal kiln, bamboo wood by thermally decompose it is obvious, start produce acetic acid
And tar.
Bamboo wood carbonized：Very fast thermal decomposition occurs at this moment 360 DEG C of the temperature in charcoal kiln, bamboo wood, produces substantial amounts of decompose
Product, is the Main Stage of the natural polymer product such as acetic acid, tar.Within this stage, due to bamboo wood very fast heat point
Solution, releases substantial amounts of heat.
Bamboo charcoal is calcined：At this moment more than 360 DEG C of the temperature in charcoal kiln.In this stage, with the lasting progress of high temperature, residual
The exclusion that the material that can be volatilized in bamboo charcoal obtains, but produce gas-condensate liquid --- bamboo vinegar is seldom.
3) initial gross separation is carried out to bamboo-vinegar using settled process, organic solvent extractionprocess；
4) simple distillation：Mixture to be separated is loaded in distillation still, heating and part are evaporated.Released by distillation still
Steam is imported in condenser, and since cooling effect steam is changed into liquid within the condenser, the distillate of generation flows into collector；
5) rectification and purification：Using the steam generated in distillation equipment and the steam previously steamed, partial condensation is flowed back
Liquid, removes smoke with resin adsorption, that is, obtains natural high-quality refined bamboo vinegar product.
The present invention is using settled process, organic solvent extractionprocess initial gross separation bamboo-vinegar, with bamboo charcoal, activated carbon adsorption point
From, reuse distillation, rectification process purification, be further refining to obtain natural high-quality refined bamboo vinegar.The preparation method operates
Simply, it is relatively low without special installation, short preparation period, cost.
Description the invention is not restricted to more than to embodiment, the content that those skilled in the art disclose according to the present invention,
The creative work improvement and modification that be carried out need not be passed through on the basis of the present invention, all should protection scope of the present invention it
It is interior.
Claims (3)
1. a kind of natural high-quality bamboo vinegar and preparation method thereof, it is characterised in that take 5~6 tons of fresh feed through initial gross separation
1 ton of bamboo charcoal and the bamboo vinegar of 300~600kg are obtained, general bamboo vinegar is divided into three classes according to temperature is collected：It is low less than 90 DEG C
Warm bamboo vinegar, the medium temperature bamboo vinegar for being between 90~120 DEG C, is high temperature bamboo vinegar higher than 120 DEG C.First bamboo vinegar is
Brown, after standing, upper strata is clarification bamboo vinegar, and lower sediment be bamboo tar, then clarified solution substep is refined.Initial gross separation is often adopted
With settled process, organic solvent extractionprocess, common bamboo charcoal is further refined, Activated Carbon Adsorption Separation, reuses distillation, rectification process
Purification.
A kind of 2. natural high-quality bamboo vinegar according to claim 1 and preparation method thereof, it is characterised in that preparation method
Comprise the following steps：1) the crooked termination formed when felling bamboo is clipped with precision pulling bench saw, using port as positioning surface, by raw bamboo
Fixed length thick bamboo tube is cut into, is broken thick bamboo tube with broken bamboo machine, then it is 1-4mm that will be cut into thickness with slicer, width is the bamboo of 10-25mm
Piece, while bamboo green grass or young crops and tabasheer are removed, bamboo green grass or young crops thickness obtains the bamboo scraps of process generation in 1-3mm；2) bamboo charcoal drying, bamboo
Material carbonizes in advance, bamboo wood carbonized, bamboo charcoal are calcined and five stages of cooling；3) it is former to bamboo vinegar using settled process, organic solvent extractionprocess
Liquid carries out initial gross separation；4) simple distillation：Mixture to be separated is loaded in distillation still, heating and part are evaporated；By distilling
The steam that kettle is released is imported in condenser, since cooling effect steam is changed into liquid, the distillation liquid stream of generation within the condenser
Enter collector.5) rectification and purification：Using the steam generated in distillation equipment and the steam previously steamed, partial condensation is flowed back
Liquid, removes smoke with resin adsorption, that is, obtains natural high-quality refined bamboo vinegar product.
A kind of 3. natural high-quality bamboo vinegar according to claim 2 and preparation method thereof, it is characterised in that the step
2) concrete technology is：
Bamboo wood is dried：The red-hot flue gas produced using fuel combustion carries out fumigation drying, generally needs one week or so time.At this moment,
Temperature in charcoal kiln is generally less than 150 DEG C, mainly removes the moisture in bamboo wood, the geomery of bamboo wood is not allowed malleable.
If the drying of bamboo wood is separately carried out, it is necessary to separately build bamboo wood smoke kiln with the process made charcoal；
Bamboo wood carbonizes in advance：At this moment 150 DEG C~270 DEG C of the temperature in charcoal kiln, bamboo wood by thermally decompose it is obvious, start produce vinegar
Acid and tar；
Bamboo wood carbonized：Very fast thermal decomposition occurs at this moment 270 DEG C~360 DEG C of the temperature in charcoal kiln, bamboo wood, produces substantial amounts of point
Product is solved, is the Main Stage of the natural polymer product such as acetic acid, tar.Within this stage, due to the very fast heat of bamboo wood
Decompose, release substantial amounts of heat；
Bamboo charcoal is calcined：At this moment more than 360 DEG C of the temperature in charcoal kiln.In this stage, with the lasting progress of high temperature, bamboo is remained in
The exclusion that the material that can be volatilized in charcoal obtains, but produce gas-condensate liquid --- bamboo vinegar is seldom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711189530.5A CN107903929A (en) | 2017-11-24 | 2017-11-24 | A kind of natural high-quality bamboo vinegar and preparation method thereof |
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| CN201711189530.5A CN107903929A (en) | 2017-11-24 | 2017-11-24 | A kind of natural high-quality bamboo vinegar and preparation method thereof |
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ID=61847641
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115006579A (en) * | 2021-03-04 | 2022-09-06 | 江苏华骏绿帆环境科技有限公司 | Plant deodorant liquid for urban public toilets and preparation method thereof |
| CN115125024A (en) * | 2021-03-24 | 2022-09-30 | 江苏华骏绿帆环境科技有限公司 | Refining and purifying method of natural bamboo vinegar stock solution |
| CN115368923A (en) * | 2022-08-23 | 2022-11-22 | 铜鼓县伟升实业有限公司 | Process and device for extracting fresh bamboo juice by dry distillation method of fresh bamboo |
-
2017
- 2017-11-24 CN CN201711189530.5A patent/CN107903929A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115006579A (en) * | 2021-03-04 | 2022-09-06 | 江苏华骏绿帆环境科技有限公司 | Plant deodorant liquid for urban public toilets and preparation method thereof |
| CN115125024A (en) * | 2021-03-24 | 2022-09-30 | 江苏华骏绿帆环境科技有限公司 | Refining and purifying method of natural bamboo vinegar stock solution |
| CN115368923A (en) * | 2022-08-23 | 2022-11-22 | 铜鼓县伟升实业有限公司 | Process and device for extracting fresh bamboo juice by dry distillation method of fresh bamboo |
| CN115368923B (en) * | 2022-08-23 | 2023-08-11 | 铜鼓县伟升实业有限公司 | Process and device for extracting fresh bamboo juice by fresh bamboo carbonization method |
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