CN206081744U - Draw reaction unit of onion crust flavone - Google Patents

Draw reaction unit of onion crust flavone Download PDF

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Publication number
CN206081744U
CN206081744U CN201621132811.8U CN201621132811U CN206081744U CN 206081744 U CN206081744 U CN 206081744U CN 201621132811 U CN201621132811 U CN 201621132811U CN 206081744 U CN206081744 U CN 206081744U
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China
Prior art keywords
valve
reative cell
control module
drying system
connection
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621132811.8U
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Chinese (zh)
Inventor
王存堂
王伟
孙天颖
余世锋
李海玉
李建立
张译心
付亮
张文婷
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Qiqihar University
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Qiqihar University
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Priority to CN201621132811.8U priority Critical patent/CN206081744U/en
Application granted granted Critical
Publication of CN206081744U publication Critical patent/CN206081744U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Extraction Or Liquid Replacement (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

The utility model discloses a draw reaction unit of onion crust flavone, including feeder hopper, organic solvent jar, microwave generator, microwave controller, reacting chamber, electric cabinet, forcing transmission pump, membrane separation post, pressure and flow control module, evaporation drying system and evaporation control module, be provided with microwave generator in the reacting chamber. Be equipped with the feeder hopper in one side upper end of reacting chamber, the opposite side upper end is equipped with the organic solvent jar, and the reacting chamber lower extreme is equipped with the discharge valve, discharge valve other end connection pressure delivery pump, forcing transmission pump junctional membrane separator column. Pressure is passed through to membrane separation post one end and the flow control module is connected with the electric cabinet, and the other end passes through the feed liquor valve and is connected with evaporation drying system, evaporation drying system connects the electric cabinet through evaporation control module, and the other end passes through the pipeline between steam control valve bond feed valve and the reacting chamber, the blow -off valve is connected to evaporation drying system lower extreme. This method has flow weak point, low, simple and convenient, the efficient advantage of equipment of energy consumption.

Description

A kind of reaction unit for extracting onion crust flavones
Technical field
The utility model is related to a kind of reaction unit, more particularly to a kind of reaction unit for extracting onion crust flavones, category In technical field of food science.
Background technology
Flavones content extremely enriches in onion crust, and flavone compound has anti-oxidant, anti-inflammatory, anticancer, antibacterial, drop blood The effect such as pressure, has a wide range of applications in medicine and food.However, onion edible and process peel off outer layer squama Skin, can produce 2%-3% onion-skin discarded objects, if not being used, will cause the significant wastage of resource.At present, it is relevant both at home and abroad The extracting method of flavones mainly has:Organic solvent extraction, ion catch electron microscopy, ultrasonic wave added extraction, supercritical fluid extraction Etc. method, but organic solvent extraction efficiency is low, ion catch electron microscopy inferior separating effect, ultrasonic wave added method are wayward, super face Boundary's extraction high expensive, these methods are unfavorable for extracting flavonoids and industrialized production in onion crust.
In order to solve an onion crust flavones production difficult problem, through experimental study for many years, applicants have invented outside a kind of onion The production technology of Beijing opera ketone:Microwave―assisted extraction, microwave―assisted extraction compared with conventional method, with efficiency high, flow process Short, energy consumption is low, process is simple, the advantage of environmentally safe, and microwave―assisted extraction is a kind of novel green extracting method, is had Beneficial to improve production efficiency and industrialized production.
The content of the invention
In order to solve the deficiencies in the prior art, the utility model provides a kind of reaction dress of extraction onion crust flavones Put, the device includes microwave treatment reative cell and UF membrane post two parts, be capable of achieving microwave treatment and UF membrane continuous prodution, Improve production efficiency.
The utility model solves the technical scheme that its technical problem adopted:A kind of reaction for extracting onion crust flavones Device, is by feed hopper, inlet valve, adiabatic case lid, organic solvent tank, organic solvent control valve, microwave generator, microwave control Instrument processed, reative cell, electric cabinet, casing, discharge valve, pressure feed pump, UF membrane post, pressure and flow-control module, liquid feed valve, Eduction valve, evaporation drying system, blow-off valve, steam control valve and evaporation control module composition, reative cell is a rectangular box, by Adiabatic case lid, casing connection composition.Reaction interior is provided with microwave generator, and microwave generator is connected and consolidates with microwave controller It is scheduled on casing and is connected with electric cabinet.Feed hopper is provided with the side upper end of reative cell, feed hopper passes through inlet valve, feed pipe Line is connected with reative cell.Organic solvent tank is provided with the opposite side upper end of reative cell, organic solvent tank is by organic solvent control The connection of valve, pipeline and reative cell.Discharge valve is connected by pipeline with reative cell, discharge valve other end connection pressure feed pump, pressure Power delivery pump junctional membrane splitter.UF membrane post one end is connected by pressure and flow-control module with electric cabinet, and the other end leads to Cross liquid feed valve to be connected with evaporation drying system;Evaporation drying system connects electric cabinet by evaporation control module, and the other end passes through Steam control valve connects the pipeline between inlet valve and reative cell;Evaporation drying system lower end connects blow-off valve.In UF membrane post Lower end be additionally provided with eduction valve.
Described casing is made of stainless steel.
The beneficial effects of the utility model are:Using multistage microwave amplifier onion crust flavones compared with conventional method, have Flow process is short, energy consumption is low, simple equipments, efficiency high, environmentally safe, is that a kind of environmentally friendly onion crust flavones produces work Skill.This reaction unit energy precise control microwave power, microwave time, flavones preparation efficiency is high, security is good, pollution-free, can be wide The general research for being applied to extracting flavonoids production field, is that chromocor compound researcher carries out researching and developing indispensable device.
Description of the drawings
The utility model is described further with reference to the accompanying drawings and detailed description.
Fig. 1 is structural representation of the present utility model.
Label in figure:
1st, feed hopper, 2, inlet valve, 3, adiabatic case lid, 4, organic solvent tank, 5, organic solvent control valve, 6, microwave occurs Device, 7, microwave controller, 8, reative cell, 9, electric cabinet, 10, casing, 11, discharge valve, 12, pressure feed pump, 13, UF membrane Post, 14, pressure and flow-control module, 15, liquid feed valve, 16, eduction valve, 17, evaporation drying system, 18, blow-off valve, 19, steam Vapour controls valve, and 20, evaporation control module.
Specific embodiment
Fig. 1 is referred to, a kind of reaction unit of extraction onion crust flavones, is by feed hopper 1, inlet valve 2, insulated cabinet Lid 3, organic solvent tank 4, organic solvent control valve 5, microwave generator 6, microwave controller 7, reative cell 8, electric cabinet 9, case Body 10, discharge valve 11, pressure feed pump 12, UF membrane post 13, pressure and flow-control module 14, liquid feed valve 15, eduction valve 16, Evaporation drying system 17, blow-off valve 18, steam control valve 19 and evaporation control module 20 are constituted, and reative cell 8 is a rectangular box, It is made up of adiabatic case lid 3, the connection of casing 10.Microwave generator 6, microwave generator 6 and microwave controller are provided with reative cell 8 7 are connected and are fixed on casing 10 and are connected with electric cabinet 9.Feed hopper 1 is provided with the side upper end of reative cell 8, feed hopper 1 leads to Cross inlet valve 2, feeding line and reative cell 8 connects.Organic solvent tank 4, organic solvent are provided with the opposite side upper end of reative cell 8 Tank 4 controls valve 5, pipeline by organic solvent and reative cell 8 connects.Discharge valve 11 is connected by pipeline with reative cell 8, discharge valve 11 other ends connect pressure feed pump 12, the junctional membrane splitter 13 of pressure feed pump 12.The one end of UF membrane post 13 by pressure and Flow-control module 14 is connected with electric cabinet 9, and the other end is connected by liquid feed valve 15 with evaporation drying system 17;Evaporation drying system System 17 connects electric cabinet 9 by evaporation control module 20, and the other end connects inlet valve 2 and reative cell 8 by steam control valve 19 Between pipeline;The lower end of evaporation drying system 17 connects blow-off valve 18.Eduction valve 16 is additionally provided with the lower end of UF membrane post 13.
Pressure and the control pressure of flow-control module 14 and flow, steam control valve 19 and the control of evaporation control module 20 have Machine solvent is circulated.
Using method:First onion crust is put into into feed hopper 1, opens inlet valve 2, onion crust is put in reative cell 8. Separately weigh a certain amount of organic solvent and be put into organic solvent tank 4, open organic solvent control valve 5, organic solvent is put into into reative cell 8, close adiabatic case lid 3.Microwave power, microwave time are arranged by microwave controller 7, starts microwave treatment journey in electric cabinet 9 Sequence, microwave treatment is arranged and started, and after microwave treatment certain hour, opens discharge valve 11, and the material after process is defeated by pressure The input UF membrane of pump 12 post 13 is sent, UF membrane pressure, flow is arranged by pressure and flow-control module 14, by evaporation control Module 20 controls cyclic process, restarts UF membrane program in electric cabinet 9, and UF membrane is arranged and started, and membrane separating process starts, and locates Reason a period of time, opening liquid feed valve 15 makes extract enter evaporation drying system 17 by pipeline, opens steam control valve 19, opens Dynamic evaporation control module 20, evaporative drying process starts, and organic vapor enters reative cell 8, evaporation drying one by pipeline Fix time, open blow-off valve 18, obtain flavones product.
Organic solvent can select ethanol.

Claims (2)

1. it is a kind of extract onion crust flavones reaction unit, it is characterised in that:Including feed hopper(1), organic solvent tank(4)、 Microwave generator(6), microwave controller(7), reative cell(8), electric cabinet(9), casing(10), pressure feed pump(12), film point From post(13), pressure and flow-control module(14), evaporation drying system(17)And evaporation control module(20), reative cell(8) For a rectangular box, by adiabatic case lid(3), casing(10)Connection composition;Reative cell(8)Inside it is provided with microwave generator(6), it is micro- Wave producer(6)With microwave controller(7)It is connected and is fixed on casing(10)Upper and and electric cabinet(9)Connection;In reative cell(8) Side upper end be provided with feed hopper(1), feed hopper(1)By inlet valve(2), feeding line and reative cell(8)Connection;In reaction Room(8)Opposite side upper end be provided with organic solvent tank(4), organic solvent tank(4)Valve is controlled by organic solvent(5), pipeline with Reative cell(8)Connection;Discharge valve(11)By pipeline and reative cell(8)It is connected, discharge valve(11)Other end connection pressure conveying Pump(12), pressure feed pump(12)Junctional membrane splitter(13);UF membrane post(13)One end is by pressure and flow-control module (14)With electric cabinet(9)Connection, the other end passes through liquid feed valve(15)With evaporation drying system(17)Connection;Evaporation drying system (17)By evaporation control module(20)Connection electric cabinet(9), the other end is by steam control valve(19)Connection inlet valve(2)With Reative cell(8)Between pipeline;Evaporation drying system(17)Lower end connects blow-off valve(18).
2. it is according to claim 1 it is a kind of extract onion crust flavones reaction unit, it is characterised in that:In UF membrane post (13)Lower end be additionally provided with eduction valve(16).
CN201621132811.8U 2016-10-19 2016-10-19 Draw reaction unit of onion crust flavone Expired - Fee Related CN206081744U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621132811.8U CN206081744U (en) 2016-10-19 2016-10-19 Draw reaction unit of onion crust flavone

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621132811.8U CN206081744U (en) 2016-10-19 2016-10-19 Draw reaction unit of onion crust flavone

Publications (1)

Publication Number Publication Date
CN206081744U true CN206081744U (en) 2017-04-12

Family

ID=59976261

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201621132811.8U Expired - Fee Related CN206081744U (en) 2016-10-19 2016-10-19 Draw reaction unit of onion crust flavone

Country Status (1)

Country Link
CN (1) CN206081744U (en)

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170412

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