CN108264966A - A kind of fir essential oil production line and production method - Google Patents
A kind of fir essential oil production line and production method Download PDFInfo
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- CN108264966A CN108264966A CN201810306040.7A CN201810306040A CN108264966A CN 108264966 A CN108264966 A CN 108264966A CN 201810306040 A CN201810306040 A CN 201810306040A CN 108264966 A CN108264966 A CN 108264966A
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- water
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of fir essential oil production line and production methods, are related to the extractive technique field of fir essential oil.Including microwave steam pressure tank, cut open block assembly, slicing device, reducing mechanism, agitating device, dehydration device, cooling device, oily-water seperating equipment, water circle device；Block assembly, slicing device, reducing mechanism is cutd open to pass sequentially through corresponding conveying device with agitating device and connect；The gas outlet of microwave steam pressure tank is connected with the air inlet of cooling device；The condensate outlet of cooling device is connected with the entrance of oily-water seperating equipment；The feed inlet of dehydration device is connected with the material outlet of microwave steam pressure tank；The water outlet of dehydration device is connected with the entrance of oily-water seperating equipment.The present invention shortens the time of extraction fir essential oil by the steam pressure of microwave steam pressure tank progress fir powder, solves the problem of heating power broken wall inefficiency in existing distillation process, time consumption and energy consumption, effect is not ideal enough.
Description
Technical field
The invention belongs to the extractive technique field of fir essential oil, more particularly to a kind of fir essential oil production line and producer
Method.
Background technology
Containing a large amount of fir essential oil in China fir, main component is cedrene, cedar wood alcohol etc., available for perfume industry
In, at present, the extraction processing of fir essential oil is mainly using solvent extraction method, cracking process, steam distillation, using solvent extraction
The oil yield of method extraction fir essential oil is high compared with the oil yield of steam distillation, but needs a large amount of solvent, and subsequent processing is complicated,
There are problems that high energy consumption, dissolvent residual, the oil yield using cracking process extraction fir essential oil is higher, but it is a chemical mistake
Journey, obtained essential oil contain the substances such as a large amount of tar, phenol, aldehyde and ketone, seriously affect the quality of fir essential oil.Steam distillation
The fir essential oil quality of method extraction is best, clear, aroma of pure, is most suitable for for blending, and its extraction process is pure object
Reason process, it is pollution-free, but oil yield is relatively low, be typically only 1~2%, cedrene in fir essential oil, cedar wood alcohol quality percentage contain
Amount general be no greater than 20%, several techniques compare, and steam distillation is the production technology of preferred environment-friendly type, but should also
This optimizes to improve yield and further reduce energy consumption.
The method distilled using common hot steam is longer in time, and the machinery of participation and artificial amount are big, production week
Phase is long, and fir essential oil is primarily present intracellular with China fir, and cell wall structure complexity broken wall is more difficult, existing distillation process
In heating power broken wall inefficiency, time consumption and energy consumption, effect is not ideal enough.
Invention content
The purpose of the present invention is to provide a kind of fir essential oil production line and production methods, and China fir is carried out by microwave steam pressure tank
The steam pressure of wood powder shortens the time of extraction fir essential oil, solves the heating power broken wall inefficiency in existing distillation process, consumes
When consume energy, the problem of effect is not ideal enough.
In order to solve the above technical problems, the present invention is achieved by the following technical solutions：
The present invention is a kind of fir essential oil production line and production method, including microwave steam pressure tank, cuts open block assembly, slice dress
It puts, reducing mechanism, agitating device, dehydration device, cooling device, oily-water seperating equipment, water circle device；It is described cut open block assembly,
Slicing device, reducing mechanism and agitating device pass sequentially through corresponding conveying device and connect；The microwave steam pressure tank goes out
Gas port is connected with the air inlet of cooling device；The condensate outlet of the cooling device is connected with the entrance of oily-water seperating equipment；
The feed inlet of the dehydration device is connected with the material outlet of microwave steam pressure tank；The water outlet of the dehydration device and water-oil separating
The entrance connection of device；The discharge port of the dehydration device is connected with the material inlet of microwave steam pressure tank by conveyer belt；It is described
The water outlet of oily-water seperating equipment is connected with water circle device water inlet；The water circle device water outlet and microwave steam pressure tank into
The mouth of a river connects.
Further, it is as follows：
S001 makes fir powder, and China fir is ground into 40~60 purposes by cuing open block assembly, slicing device and reducing mechanism
Fir powder；
S002 carries out material mixing, adds in alkali into fir powder and salt is mixed, the weight proportion of three is：Fir powder
750 parts, 3.5~6 parts of 2.5~4 parts of alkali or urea or both 3~5.5 parts of mixture, 1.6~2.3 parts of salt；
S003 carries out Microwave Hybrid, and the material mixed in S002 is transported to microwave steam pressure tank, adds in 10%~30%
The water of mixed material volume, the temperature of water are controlled at 200 DEG C~230 DEG C, proceed by microwave heating；
S004 steam cools down：The steam that microwave heating generates in pipeline to cooling tower by being cooled down, cooling water
Temperature control is at 60 DEG C hereinafter, 1~2 hour microwave time, oily-water seperating equipment is pipelined to by condensate liquid；
S005 material dewaterings：5~15 minutes after microwave heating, the material in microwave steam pressure tank is passed through into conveyance conduit
It is transported to dehydration device to be dehydrated, the water that dehydration device generates is pipelined to oily-water seperating equipment；
S006 is recycled again：Dewatered China fir siccative is transported to microwave steam pressure tank by conveyer belt, is repeated
Waste material is taken out and collects storage by S002~S005；
S007 water-oil separatings：Oily-water seperating equipment detaches the oil mixing with water liquid that above step obtains, and isolates
Water Microwave Hybrid device be transported to by water circle device reuse, isolated oil is fir essential oil.
Further, it is as follows：
SS001 makes fir powder, and China fir is ground into 40~60 purposes by cuing open block assembly, slicing device and reducing mechanism
Fir powder；
SS002 carries out material mixing, adds in alkali into fir powder and salt is mixed, the weight proportion of three is：China fir
3.5~6 parts of 750 parts of powder, 2.5~4 parts of alkali or urea or both 3~5.5 parts of mixture, 1.6~2.3 parts of salt；
SS003 carries out Microwave Hybrid, and the material mixed in S002 is transported to microwave steam pressure tank, adds in 10%~30%
The water of mixed material volume, the temperature of water are controlled at 200 DEG C~230 DEG C, proceed by microwave heating；
SS004 steam cools down：The steam that microwave heating generates in pipeline to cooling tower by being cooled down, cooling water
Temperature control is at 60 DEG C hereinafter, 1~2 hour microwave time, oily-water seperating equipment is pipelined to by condensate liquid；
SS005 material dewaterings：5~15 minutes after microwave heating, the material in microwave steam pressure tank is passed through into delivery pipe
Road is transported to dehydration device and is dehydrated, and the water that dehydration device generates is pipelined to oily-water seperating equipment, and waste material is taken
Go out to collect storage；
SS006 water-oil separatings：Oily-water seperating equipment detaches the oil mixing with water liquid that above step obtains, and isolates
Water Microwave Hybrid device be transported to by water circle device reuse, isolated oil is fir essential oil.
The invention has the advantages that：
The present invention carries out microwave heating by microwave to fir powder and its mixture, and the cell for having fir essential oil is allowed to carry out
Inside surge heating, from internal sabotage eucaryotic cell structure, accelerates oil yield efficiency, is passed through a part of essential oil by the steam of generation cold
Solidifying mode is collected and water-oil separating obtains fir essential oil, then fir powder squeeze by dehydration device and is further destroyed carefully
Cell wall improves oil pump capacity, and the oil water mixture of abjection carries out water-oil separating and obtains fir essential oil, for the first time dewatered fir powder
Fir essential oil yield is can further improve again by microwave steam pressure tank, the whole flow process time is short efficient.
Certainly, it implements any of the products of the present invention and does not necessarily require achieving all the advantages described above at the same time.
Description of the drawings
In order to illustrate the technical solution of the embodiments of the present invention more clearly, embodiment will be described below required
Attached drawing is briefly described, it should be apparent that, the accompanying drawings in the following description is only some embodiments of the present invention, for ability
For the those of ordinary skill of domain, without creative efforts, it can also be obtained according to these attached drawings other attached
Figure.
Fig. 1 is a kind of fir essential oil production line of the present invention and the flow sheet of production method；
In attached drawing, parts list represented by the reference numerals are as follows：
1- microwave steam pressure tanks, 2- cut open block assembly, 3- slicing devices, 4- reducing mechanisms, 5- agitating devices, 6- dehydration devices,
7- cooling devices, 8- oily-water seperating equipments, 9- water circle devices.
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete
Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art are obtained all other without creative efforts
Embodiment shall fall within the protection scope of the present invention.
Refering to Figure 1, the present invention is a kind of fir essential oil production line and production method, including microwave steam pressure tank 1, cut open
Block assembly 2, slicing device 3, reducing mechanism 4, agitating device 5, dehydration device 6, cooling device 7, oily-water seperating equipment 8, water follow
Loop device 9；It cuts open block assembly 2, slicing device 3, reducing mechanism 4 and agitating device 5 four and passes sequentially through corresponding conveying device company
It connects；The gas outlet of microwave steam pressure tank 1 is connected with the air inlet of cooling device 7；The condensate outlet of cooling device 7 and water-oil separating
The entrance connection of device 8；The feed inlet of dehydration device 6 is connected with the material outlet of microwave steam pressure tank 1；The water outlet of dehydration device 6
Mouth is connected with the entrance of oily-water seperating equipment 8；The discharge port of dehydration device 6 passes through conveying with the material inlet of microwave steam pressure tank 1
Band is connected；The water outlet of oily-water seperating equipment 8 is connected with 9 water inlet of water circle device；9 water outlet of water circle device and microwave steam
Press the connection of 1 water inlet of tank.
Wherein as shown in Figure 1, being as follows：
S001 makes fir powder, and China fir is ground into 40~60 mesh by cuing open block assembly 2, slicing device 3 and reducing mechanism 4
Fir powder；
S002 carries out material mixing, adds in alkali into fir powder and salt is mixed, the weight proportion of three is：Fir powder
750 parts, 3.5~6 parts of 2.5~4 parts of alkali or urea or both 3~5.5 parts of mixture, 1.6~2.3 parts of salt；
S003 carries out Microwave Hybrid, and the material mixed in S002 is transported to microwave steam pressure tank 1, adds in 10%~30%
The water of mixed material volume, the temperature of water are controlled at 200 DEG C~230 DEG C, proceed by microwave heating；
S004 steam cools down：The steam that microwave heating generates in pipeline to cooling tower by being cooled down, cooling water
Temperature control is at 60 DEG C hereinafter, 1~2 hour microwave time, oily-water seperating equipment 8 is pipelined to by condensate liquid；
S005 material dewaterings：5~15 minutes after microwave heating, the material in microwave steam pressure tank 1 is passed through into delivery pipe
Road is transported to dehydration device 6 and is dehydrated, and the water that dehydration device 6 generates is pipelined to oily-water seperating equipment 8；
S006 is recycled again：Dewatered China fir siccative is transported to microwave steam pressure tank 1 by conveyer belt, is repeated
Waste material is taken out and collects storage by S002~S005；
S007 water-oil separatings：Oily-water seperating equipment 8 detaches the oil mixing with water liquid that above step obtains, and isolates
Water Microwave Hybrid device be transported to by water circle device 9 reuse, isolated oil is fir essential oil.
Wherein, it is as follows：
SS001 makes fir powder, and China fir is ground into 40~60 by cuing open block assembly 2, slicing device 3 and reducing mechanism 4
Purpose fir powder；
SS002 carries out material mixing, adds in alkali into fir powder and salt is mixed, the weight proportion of three is：China fir
3.5~6 parts of 750 parts of powder, 2.5~4 parts of alkali or urea or both 3~5.5 parts of mixture, 1.6~2.3 parts of salt；
SS003 carries out Microwave Hybrid, and the material mixed in S002 is transported to microwave steam pressure tank 1, add in 10%~
The water of 30% mixed material volume, the temperature of water are controlled at 200 DEG C~230 DEG C, proceed by microwave heating；
SS004 steam cools down：The steam that microwave heating generates in pipeline to cooling tower by being cooled down, cooling water
Temperature control is at 60 DEG C hereinafter, 1~2 hour microwave time, oily-water seperating equipment 8 is pipelined to by condensate liquid；
SS005 material dewaterings：5~15 minutes after microwave heating, the material in microwave steam pressure tank 1 is passed through into delivery pipe
Road is transported to dehydration device 6 and is dehydrated, and the water that dehydration device 6 generates is pipelined to oily-water seperating equipment 8, by waste material
It takes out and collects storage；
SS006 water-oil separatings：Oily-water seperating equipment 8 detaches the oil mixing with water liquid that above step obtains, separation
The water gone out is transported to Microwave Hybrid device by water circle device 9 and reuses, and isolated oil is fir essential oil.
In the present specification, schematic expression of the above terms may not refer to the same embodiment or example.And
And particular features, structures, materials, or characteristics described can be in any one or more embodiments or example with suitable
Mode combine.
Present invention disclosed above preferred embodiment is only intended to help to illustrate the present invention.There is no detailed for preferred embodiment
All details are described, are not limited the invention to the specific embodiments described.Obviously, according to the content of this specification,
It can make many modifications and variations.This specification is chosen and specifically describes these embodiments, is in order to preferably explain the present invention
Principle and practical application, so as to which skilled artisan be enable to be best understood by and utilize the present invention.The present invention is only
It is limited by claims and its four corner and equivalent.
Claims (3)
1. a kind of fir essential oil production line, it is characterised in that：Including microwave steam pressure tank (1), cut open block assembly (2), slicing device
(3), reducing mechanism (4), agitating device (5), dehydration device (6), cooling device (7), oily-water seperating equipment (8), water cycle dress
It puts (9)；It is described cut open block assembly (2), slicing device (3), reducing mechanism (4) and agitating device (5) four pass sequentially through it is corresponding
Conveying device connects；The gas outlet of the microwave steam pressure tank (1) is connected with the air inlet of cooling device (7)；The cooling device
(7) condensate outlet is connected with the entrance of oily-water seperating equipment (8)；The feed inlet of the dehydration device (6) and microwave steam pressure
The material outlet of tank (1) is connected；The water outlet of the dehydration device (6) is connected with the entrance of oily-water seperating equipment (8)；It is described de-
The discharge port of water installations (6) is connected with the material inlet of microwave steam pressure tank (1) by conveyer belt；The oily-water seperating equipment (8)
Water outlet connected with water circle device (9) water inlet；Water circle device (9) water outlet is intake with microwave steam pressure tank (1)
Mouth connection.
2. a kind of fir essential oil production method according to claim 1, which is characterized in that be as follows：
S001 makes fir powder, and China fir is ground into 40~60 by cuing open block assembly (2), slicing device (3) and reducing mechanism (4)
Purpose fir powder；
S002 carries out material mixing, adds in alkali into fir powder and salt is mixed, the weight proportion of three is：Fir powder 750
3.5~6 parts of part, 2.5~4 parts of alkali or urea or both 3~5.5 parts of mixture, 1.6~2.3 parts of salt；
S003 carries out Microwave Hybrid, and the material mixed in S002 is transported to microwave steam pressure tank (1), it is mixed to add in 10%~30%
The water of volume of material is closed, the temperature of water is controlled at 200 DEG C~230 DEG C, proceeds by microwave heating；
S004 steam cools down：The steam that microwave heating generates in pipeline to cooling tower by being cooled down, cooling water temperature
Control is at 60 DEG C hereinafter, 1~2 hour microwave time, oily-water seperating equipment (8) is pipelined to by condensate liquid；
S005 material dewaterings：5~15 minutes after microwave heating, the material in microwave steam pressure tank (1) is passed through into conveyance conduit
It is transported to dehydration device (6) to be dehydrated, the water that dehydration device (6) generates is pipelined to oily-water seperating equipment (8)；
S006 is recycled again：Dewatered China fir siccative is transported to microwave steam pressure tank (1) by conveyer belt, repeats S002
Waste material is taken out and collects storage by~S005；
S007 water-oil separatings：Oily-water seperating equipment (8) detaches the oil mixing with water liquid that above step obtains, and isolates
Water is transported to Microwave Hybrid device by water circle device (9) and reuses, and isolated oil is fir essential oil.
3. a kind of fir essential oil production method according to claim 2, which is characterized in that be as follows：
SS001 makes fir powder, it is ground into 40 by cuing open block assembly (2), slicing device (3) and reducing mechanism (4) by China fir~
The fir powder of 60 mesh；
SS002 carries out material mixing, adds in alkali into fir powder and salt is mixed, the weight proportion of three is：Fir powder 750
3.5~6 parts of part, 2.5~4 parts of alkali or urea or both 3~5.5 parts of mixture, 1.6~2.3 parts of salt；
SS003 carries out Microwave Hybrid, and the material mixed in S002 is transported to microwave steam pressure tank (1), adds in 10%~30%
The water of mixed material volume, the temperature of water are controlled at 200 DEG C~230 DEG C, proceed by microwave heating；
SS004 steam cools down：The steam that microwave heating generates in pipeline to cooling tower by being cooled down, cooling water temperature
Control is at 60 DEG C hereinafter, 1~2 hour microwave time, oily-water seperating equipment (8) is pipelined to by condensate liquid；
SS005 material dewaterings：5~15 minutes after microwave heating, the material in microwave steam pressure tank (1) is passed through into conveyance conduit
It is transported to dehydration device (6) to be dehydrated, the water that dehydration device (6) generates is pipelined to oily-water seperating equipment (8), will
Waste material, which takes out, collects storage；
SS006 water-oil separatings：Oily-water seperating equipment (8) detaches the oil mixing with water liquid that above step obtains, and isolates
Water Microwave Hybrid device be transported to by water circle device (9) reuse, isolated oil is fir essential oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810306040.7A CN108264966A (en) | 2018-04-08 | 2018-04-08 | A kind of fir essential oil production line and production method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810306040.7A CN108264966A (en) | 2018-04-08 | 2018-04-08 | A kind of fir essential oil production line and production method |
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| CN108264966A true CN108264966A (en) | 2018-07-10 |
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ID=62777481
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810306040.7A Pending CN108264966A (en) | 2018-04-08 | 2018-04-08 | A kind of fir essential oil production line and production method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108929783A (en) * | 2018-08-08 | 2018-12-04 | 福建龙凌植物油开发有限公司 | A kind of production line of san-mou oil |
| CN115261137A (en) * | 2022-06-21 | 2022-11-01 | 刘宏智 | Method for preparing agilawood material and method for preparing essential oil and agilawood vinegar from agilawood material |
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| CN103897806A (en) * | 2014-04-03 | 2014-07-02 | 广东添乐化妆品有限公司 | Microwave assisted extraction method of lemon essential oil |
| CN203999556U (en) * | 2014-06-17 | 2014-12-10 | 南京飞马食品有限公司 | Microwave-assisted essential oil extracting device |
| CN106883932A (en) * | 2017-04-17 | 2017-06-23 | 福建鑫绿林产品开发有限公司 | A kind of low energy consumption high yield pulp1 obtains the production method and production line of fir essential oil |
| CN106947602A (en) * | 2017-05-03 | 2017-07-14 | 福建鑫绿林产品开发有限公司 | The high yield pulp1 production method and production line of a kind of fir essential oil |
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2018
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103897806A (en) * | 2014-04-03 | 2014-07-02 | 广东添乐化妆品有限公司 | Microwave assisted extraction method of lemon essential oil |
| CN203999556U (en) * | 2014-06-17 | 2014-12-10 | 南京飞马食品有限公司 | Microwave-assisted essential oil extracting device |
| CN106883932A (en) * | 2017-04-17 | 2017-06-23 | 福建鑫绿林产品开发有限公司 | A kind of low energy consumption high yield pulp1 obtains the production method and production line of fir essential oil |
| CN106947602A (en) * | 2017-05-03 | 2017-07-14 | 福建鑫绿林产品开发有限公司 | The high yield pulp1 production method and production line of a kind of fir essential oil |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108929783A (en) * | 2018-08-08 | 2018-12-04 | 福建龙凌植物油开发有限公司 | A kind of production line of san-mou oil |
| CN115261137A (en) * | 2022-06-21 | 2022-11-01 | 刘宏智 | Method for preparing agilawood material and method for preparing essential oil and agilawood vinegar from agilawood material |
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