CN206706052U - A kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil - Google Patents
A kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil Download PDFInfo
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- CN206706052U CN206706052U CN201720401683.0U CN201720401683U CN206706052U CN 206706052 U CN206706052 U CN 206706052U CN 201720401683 U CN201720401683 U CN 201720401683U CN 206706052 U CN206706052 U CN 206706052U
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Abstract
The utility model discloses the production line that a kind of low energy consumption high yield pulp1 obtains fir essential oil, production line includes boiler, steam superheating device, cuts open block and section and crushing and agitating device, destilling tower, cooling tower, oily-water seperating equipment；Also include equipment for separating liquid from solid, provided with stir with the Material collecting box for harvesting of spray equipment, set device of stirring in a distillation column；The outlet pipe of cooling tower connects with boiler；Spray equipment connects with oily-water seperating equipment；The leachate mouth of Material collecting box for harvesting connects with oily-water seperating equipment；The slag notch of Material collecting box for harvesting and the feeding mouth of equipment for separating liquid from solid connect；The liquid outlet of equipment for separating liquid from solid is connected with the entrance of oily-water seperating equipment, and slag notch is connected by being distributed conveyer belt around tower with the fuel inlet of boiler and steam superheating device；Using the production line, through powder processed, mixing, single flash, second distillation, cooling, spray stir, separation of solid and liquid, solid material drying, obtain fir essential oil after water-oil separating.Yield is high, energy consumption water consume is small.
Description
Technical field
The utility model belongs to the extractive technique field of fir essential oil, is related to a kind of low energy consumption high yield pulp1 and obtains fir essential oil
Production line.
Background technology
Contain substantial amounts of fir essential oil in China fir, its main component is cedrene, cedar wood alcohol etc., available for perfume industry
In.At present, the extraction processing of fir essential oil is mainly using solvent extraction method, cracking process, steam distillation.Using solvent extraction
The oil yield of method extraction fir essential oil is high compared with the oil yield of steam distillation, but needs substantial amounts of solvent, and subsequent treatment is complicated,
The problem of high energy consumption, dissolvent residual be present.Oil yield using cracking process extraction fir essential oil is higher, but it is a chemical mistake
Journey, obtained essential oil contain the materials such as substantial amounts of tar, phenol, aldehyde and ketone, have a strong impact on the quality of fir essential oil.Steam distillation
The fir essential oil quality of method extraction is best, clear, aroma of pure, is best suitable for being used for blending, and its extraction process is pure thing
Reason process, it is pollution-free, but oil yield is relatively low, it is typically only 1~2%, cedrene, the quality percentage of cedar wood alcohol contain in fir essential oil
Amount general be no greater than 20%.Several techniques compare, and steam distillation is the production technology of preferable environment-friendly type, but should also
This is optimized to improve yield and further reduce energy consumption.
Such as：Open (bulletin) number is CN105176690A, entitled " side of thing extraction fir essential oil to be remained using China fir three
A kind of method that thing extraction fir essential oil is remained using China fir three is disclosed in the patent application document technical scheme of method ", its is specific
Step is as follows：1. China fir three is remained into thing is processed into fir powder；2. fir powder is sent into the tempering tank of belt stirrer, to fir powder
Middle addition dietary alkali and Nacl are stirred mixing, and fir powder, dietary alkali, the weight of Nacl are：Fir powder 750
Part, 2.5~3.5 parts of dietary alkali, 1.8~2.2 parts of Nacl；3. the fir powder mixed is sent into destilling tower, to destilling tower
In to be passed through temperature be that 240~260 DEG C of vapor is distilled, distillation time is 9~11 hours；4. the mixing discharged after distillation
Gas is cooled down by pipeline into cooling tower, and cooling water temperature control obtains profit below 60 DEG C, after cooling and mixed
Close liquid；5. oil mixing with water liquid obtains fir essential oil after water-oil separating.Oil yield and the China fir of fir essential oil can be effectively improved
The content of cedar wood alcohol, cedrene in another name for oil.
Using the method for extracting fir essential oil of such technology it is of course possible to use, but its production line flow process is closed not enough
Reason, energy consumption is also relatively large, yield is high not enough, and using effect is preferable not enough.
Utility model content
For overcome the deficiencies in the prior art, the utility model provides a kind of flow and more optimized rationally, and energy consumption is relatively small,
The relatively higher low energy consumption high yield pulp1 of yield obtains the production line of fir essential oil, and using effect is more preferable.
The utility model is that technical scheme is used by reaching above-mentioned technical purpose：A kind of low energy consumption high yield pulp1 obtains China fir
The production line of another name for oil, production line include boiler, steam superheating device, cut open block assembly, slicing device, reducing mechanism, stirring dress
Put, destilling tower, cooling tower, oily-water seperating equipment；The output jet chimney of boiler heated by steam superheating device after with distillation
The steam inlet connection of tower；Cut open block assembly, slicing device, reducing mechanism, agitating device and pass sequentially through corresponding conveying dress
Put connection；The output end of agitating device and the feeding mouth of destilling tower are connected by conveying device；The gas outlet of destilling tower and cooling
The air inlet connection of tower；The condensate outlet of cooling tower connects with the entrance of oily-water seperating equipment；Also include equipment for separating liquid from solid,
The Material collecting box for harvesting being connected with destilling tower slag notch by conveying device, the first set in a distillation column stir device, be located on Material collecting box for harvesting
The spray equipment of side, the second that is located in Material collecting box for harvesting are stirred device；The confession of cooling water outlet pipe and boiler after the heating of cooling tower
Water inlet connects；The water inlet of spray equipment connects with the delivery port of oily-water seperating equipment；Leachate outlet and the oil of Material collecting box for harvesting
The entrance connection of water separation device；The slag notch of Material collecting box for harvesting is connected by the feeding mouth of conveying device and equipment for separating liquid from solid；Gu
The liquid outlet of liquid separating apparatus connects with the entrance of oily-water seperating equipment；The slag notch of equipment for separating liquid from solid is defeated by being distributed around tower
Band and the fuel inlet of boiler and steam superheating device is sent to be connected；It is described around tower distribution conveyer belt be from equipment for separating liquid from solid
Slag notch is by arriving at the conveyer belt of the fuel inlet of boiler and steam superheating device after crooked route pile warp destilling tower outer wall.
Described equipment for separating liquid from solid is centrifugal separator.
Described equipment for separating liquid from solid is spiral squeezing type separator.
The utility model has the advantage of：
Due to production line also include equipment for separating liquid from solid, be connected with destilling tower slag notch by conveying device Material collecting box for harvesting,
If first in a distillation column is stirred, device, the spray equipment being located above Material collecting box for harvesting, the second that is located in Material collecting box for harvesting are stirred device；It is cold
But the cooling water outlet pipe after the heating of tower connects with the water feed inlet of boiler；The water inlet and oily-water seperating equipment of spray equipment
Delivery port connection；The leachate outlet of Material collecting box for harvesting connects with the entrance of oily-water seperating equipment；The slag notch of Material collecting box for harvesting passes through defeated
The feeding mouth of device and equipment for separating liquid from solid is sent to connect；The liquid outlet of equipment for separating liquid from solid and the entrance of oily-water seperating equipment connect
It is logical；The slag notch of equipment for separating liquid from solid is connected by being distributed conveyer belt around tower with the fuel inlet of boiler and steam superheating device；
It is described around tower distribution conveyer belt be the slag notch from equipment for separating liquid from solid by being arrived at after crooked route pile warp destilling tower outer wall
The conveyer belt of the fuel inlet of boiler and steam superheating device.
Therefore, production line is all rationally utilized water, middle liquid object, wooden slag, middle heat energy, among destilling tower
Upset can be stirred provided with first device of stirring, therefore distill can be more saturating, on the premise of distilling effect is ensured, distillation total time
Can significantly shortens, because the slag charge that is ejected after distillation can be stirred device by spray equipment and the second being located in Material collecting box for harvesting
Spray is stirred, then is further rationally utilized the slag charge containing active ingredient and middle leachate and separating liquid by separation of solid and liquid,
The conveying for the fuel inlet that slag charge arrives at boiler and steam superheating device after pile warp destilling tower outer wall is drying to be sent to do again and fires
Material, by various liquid, the optimization of solid material conveying flow and recycling, therefore yield improves, water consume energy consumption greatly reduces, and uses
Effect is more preferable.
Brief description of the drawings
The utility model is described in further detail with reference to the accompanying drawings and examples.Wherein：
Fig. 1 is the schematic diagram of production line of the present utility model.
Marker number in accompanying drawing is described as follows：Boiler 1, steam superheating device 2, slicing device 3, reducing mechanism 4, cut open block
Device 5, destilling tower 6, agitating device 7, device 9 of stirring around tower distribution conveyer belt 8, first, cooling tower 10, spray equipment 11, gather materials
Case 12, second are stirred device 13, equipment for separating liquid from solid 14, oily-water seperating equipment 15
Embodiment
Embodiment of the present utility model, as shown in figure 1, a kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil, it is raw
Producing line include boiler 1, steam superheating device 2, cut open block assembly 5, slicing device 3, reducing mechanism 4, agitating device 7, destilling tower 6,
Cooling tower 10, oily-water seperating equipment 15；Boiler 1 output jet chimney by steam superheating device 2 heat after with destilling tower 6
Steam inlet connects；Cut open block assembly 5, slicing device 3, reducing mechanism 4, agitating device 7 four and pass sequentially through corresponding conveying dress
Put connection；The output end of agitating device 7 is connected with the feeding mouth of destilling tower 6 by conveying device；The gas outlet of destilling tower 6 with it is cold
But the air inlet connection of tower 10；The condensate outlet of cooling tower 10 connects with the entrance of oily-water seperating equipment 15；Also include solid-liquid
Separator 14, the Material collecting box for harvesting 12 being connected with the slag notch of destilling tower 6 by conveying device, the first that is located in destilling tower 6 are stirred dress
Put 9, the spray equipment 11 for being located at the top of Material collecting box for harvesting 12, the second being located in Material collecting box for harvesting 12 are stirred device 13；The heating of cooling tower 10
Cooling water outlet pipe afterwards connects with the water feed inlet of boiler 1；The water inlet of spray equipment 11 goes out with oily-water seperating equipment 15
The mouth of a river connects；The leachate outlet of Material collecting box for harvesting 12 connects with the entrance of oily-water seperating equipment 15；The slag notch of Material collecting box for harvesting 12 passes through
Conveying device is connected with the feeding mouth of equipment for separating liquid from solid 14；The liquid outlet of equipment for separating liquid from solid 14 and oily-water seperating equipment 15
Entrance connects；The slag notch of equipment for separating liquid from solid 14 passes through the combustion around tower distribution conveyer belt 8 and boiler 1 and steam superheating device 2
Expect entrance connection；It is described around tower distribution conveyer belt 8 be to be steamed from the slag notch of equipment for separating liquid from solid 14 by crooked route pile warp
Evaporate the conveyer belt for the fuel inlet that boiler 1 and steam superheating device 2 are arrived at after the outer wall of tower 6.
Described equipment for separating liquid from solid 14 is centrifugal separator.
Described equipment for separating liquid from solid 14 is spiral squeezing type separator.
When being produced using described production line, comprise the following steps that：
A, powder processed, by cuing open block assembly 5, slicing device 3, reducing mechanism 4, China fir raw material is ground into 80~120 purposes
Fir powder；
B, mix, add dietary alkali into fir powder and Nacl agitating device 7 is stirred mixing, the weight of three
Part matches：750 parts of fir powder, 2.5~3.5 parts of dietary alkali, 1.8~2.2 parts of Nacl；
C, single flash, will the fir powder that mixed be sent into destilling tower 6 in, be passed through into destilling tower 6 temperature for 240 DEG C~
260 DEG C of superheated steam carries out single flash, and the single flash time is 4~6 hours；
D, second distillation, by the first being located in destilling tower 6 stir device 9 by destilling tower 6 material stirring overturn 2-3
Second distillation is and then carried out after minute 2~3 hours；
E, cool down, the mixed gas discharged after being distilled during single flash and second distillation passes through pipeline to cooling
Cooled down in tower 10, cooling water temperature should be controlled below 60 DEG C, the cooling water conveying to be heated up in cooling tower 10 after heat exchange
Water inlet to boiler 1 as boiler 1, condensed oil mixing with water liquid is sent into oily-water seperating equipment 15 in cooling tower 10；
F, spray is stirred, and solid material is gone out into tower after the completion of second distillation is sent into Material collecting box for harvesting 12, equal by spray equipment 11
The even separation water for trickling through water pipe and being introduced from oily-water seperating equipment 15, the parts by weight control of every 750 parts of fir powders institute shower water
15~20 parts are made as, moderately should be stirred during spray with second device 13 of stirring so as to spray evenly；
G, separation of solid and liquid, separation of solid and liquid is carried out with equipment for separating liquid from solid 14 after the completion of spray, the oil mixing with water isolated point
Chaotropic body is sent into oily-water seperating equipment 15；
H, solid material is dried, and the solid material after the completion of separation of solid and liquid passes through is distributed the outer wall of 8 pile warp destilling tower of conveyer belt 6 around tower
Boiler 1 is transported to again after the drying of periphery and steam superheating device 2 is used as fuel；
The oil that oil mixing with water liquid obtains after water-oil separating is China fir essence by F, water-oil separating, oily-water seperating equipment 15
Oil.
Claims (3)
1. a kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil, production line include boiler, steam superheating device, cut open it is packaged
Put, slicing device, reducing mechanism, agitating device, destilling tower, cooling tower, oily-water seperating equipment；The output jet chimney of boiler leads to
Connected after crossing steam superheating device heating with the steam inlet of destilling tower；Cut open block assembly, slicing device, reducing mechanism, stirring dress
Put four and pass sequentially through corresponding conveying device connection；The output end of agitating device and the feeding mouth of destilling tower pass through conveying device
Connection；The gas outlet of destilling tower connects with the air inlet of cooling tower；The condensate outlet of cooling tower and entering for oily-water seperating equipment
Mouth connection；It is characterized in that：Also include equipment for separating liquid from solid, be connected with destilling tower slag notch by conveying device Material collecting box for harvesting,
If first in a distillation column is stirred, device, the spray equipment being located above Material collecting box for harvesting, the second that is located in Material collecting box for harvesting are stirred device；It is cold
But the cooling water outlet pipe after the heating of tower connects with the water feed inlet of boiler；The water inlet and oily-water seperating equipment of spray equipment
Delivery port connection；The leachate outlet of Material collecting box for harvesting connects with the entrance of oily-water seperating equipment；The slag notch of Material collecting box for harvesting passes through defeated
The feeding mouth of device and equipment for separating liquid from solid is sent to connect；The liquid outlet of equipment for separating liquid from solid and the entrance of oily-water seperating equipment connect
It is logical；The slag notch of equipment for separating liquid from solid is connected by being distributed conveyer belt around tower with the fuel inlet of boiler and steam superheating device；
It is described around tower distribution conveyer belt be the slag notch from equipment for separating liquid from solid by being arrived at after crooked route pile warp destilling tower outer wall
The conveyer belt of the fuel inlet of boiler and steam superheating device.
2. a kind of low energy consumption high yield pulp1 according to claim 1 obtains the production line of fir essential oil, it is characterised in that：It is described
Equipment for separating liquid from solid be centrifugal separator.
3. a kind of low energy consumption high yield pulp1 according to claim 1 obtains the production line of fir essential oil, it is characterised in that：It is described
Equipment for separating liquid from solid be spiral squeezing type separator.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720401683.0U CN206706052U (en) | 2017-04-17 | 2017-04-17 | A kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720401683.0U CN206706052U (en) | 2017-04-17 | 2017-04-17 | A kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil |
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| Publication Number | Publication Date |
|---|---|
| CN206706052U true CN206706052U (en) | 2017-12-05 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720401683.0U Expired - Fee Related CN206706052U (en) | 2017-04-17 | 2017-04-17 | A kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil |
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| Country | Link |
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| CN (1) | CN206706052U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883932A (en) * | 2017-04-17 | 2017-06-23 | 福建鑫绿林产品开发有限公司 | A kind of low energy consumption high yield pulp1 obtains the production method and production line of fir essential oil |
| CN108467786A (en) * | 2018-04-16 | 2018-08-31 | 福建鑫绿林产品开发有限公司 | A kind of fir essential oil production system and its production method |
| CN108929783A (en) * | 2018-08-08 | 2018-12-04 | 福建龙凌植物油开发有限公司 | A kind of production line of san-mou oil |
-
2017
- 2017-04-17 CN CN201720401683.0U patent/CN206706052U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106883932A (en) * | 2017-04-17 | 2017-06-23 | 福建鑫绿林产品开发有限公司 | A kind of low energy consumption high yield pulp1 obtains the production method and production line of fir essential oil |
| CN106883932B (en) * | 2017-04-17 | 2023-03-10 | 福建鑫绿林产品开发有限公司 | Production method and production line for obtaining cedar essential oil with low energy consumption and high yield |
| CN108467786A (en) * | 2018-04-16 | 2018-08-31 | 福建鑫绿林产品开发有限公司 | A kind of fir essential oil production system and its production method |
| CN108929783A (en) * | 2018-08-08 | 2018-12-04 | 福建龙凌植物油开发有限公司 | A kind of production line of san-mou oil |
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| GR01 | Patent grant | ||
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171205 Termination date: 20210417 |
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| CF01 | Termination of patent right due to non-payment of annual fee |