CN108929783A - A kind of production line of san-mou oil - Google Patents

A kind of production line of san-mou oil Download PDF

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Publication number
CN108929783A
CN108929783A CN201810895178.5A CN201810895178A CN108929783A CN 108929783 A CN108929783 A CN 108929783A CN 201810895178 A CN201810895178 A CN 201810895178A CN 108929783 A CN108929783 A CN 108929783A
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CN
China
Prior art keywords
san
water
mou
oil
mou oil
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810895178.5A
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Chinese (zh)
Inventor
魏惠芳
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Fujian Longling Plant Oil Development Co Ltd
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Fujian Longling Plant Oil Development Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Fujian Longling Plant Oil Development Co Ltd filed Critical Fujian Longling Plant Oil Development Co Ltd
Priority to CN201810895178.5A priority Critical patent/CN108929783A/en
Publication of CN108929783A publication Critical patent/CN108929783A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/025Recovery by solvent extraction
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Processing Of Solid Wastes (AREA)

Abstract

The present invention relates to a kind of extraction process units of san-mou oil, and in particular to a kind of production line of san-mou oil, including grinding device, biomass boiler, san-mou oil extraction element, oily-water seperating equipment and san-mou oil collection device;San-mou oil extraction element offers feed inlet, gas outlet, discharge port and air inlet;Biomass boiler includes drum and wet scrubber;Wet scrubber includes water inlet;Grinding device is connect with feed inlet, and the waste material of discharge port discharge is as biomass fuel for burning;Drum is connect with air inlet, and gas outlet is connect with oily-water seperating equipment;Oily-water seperating equipment includes oil outlet and water outlet, and oil outlet is connect with san-mou oil collection device, the water inlet connection of water outlet and wet scrubber;By the present invention in that with biomass boiler, can by after the extraction of san-mou oil extraction element remaining waste material be used for the burning of biomass boiler;By using waste water as the water in dust removal of wet scrubber, the consumption of water resource is reduced.

Description

A kind of production line of san-mou oil
Technical field
The present invention relates to a kind of extraction process units of san-mou oil, and in particular to a kind of production line of san-mou oil.
Background technique
China fir is the most important reproducting tree species of south China.China fir tree body is tall and big, and texture is straight, and structure is careful, and material is light Soft, handling ease is not stuck up and is not split, and corrosion resistant insect prevention, wearability is strong, and has aromatic odor, therefore is widely used in building, bridge Beam, vessel, electric pole, furniture etc..Chinese fir root-bark and processing waste are not utilized well at present, or are stayed in mountain forest and left It rots, or as low value-added utilizations such as burnings, causes the serious waste of resource.
Largely statistics indicate that, a large amount of fir essential oil is contained in China fir, and Chinese fir root-bark is essential oil content in whole Chinese fir Highest position.The main component of fir essential oil is cedar wood alcohol, eneα-cedar, β-cedrene, thujopsene, australene and α-pine Oleyl alcohol etc., all very close cedar wood oil from the point of view of primary chemical composition and fragrance, so can be used to substitute Cypress ethereal oil completely For perfume industry.Cedar wood oil has strong woody-musky-ambergris fragrance, is mainly used for talcum powder, muffin, kermes Equal cosmetics class cosmetics and soaps could be applicable in supplying illusion type essence.Cedar wood oil is one of big essential oil in the world ten, market Be in great demand.Since the growth cycle of cypress is very long, can just become a useful person within about 60 years, so cypress scarcity of resources is caused, from And the development of China's cedar wood oil industry is seriously affected.China fir has the characteristics that fast-growth, leaves after trees felling big Amount tree root resource can be used for the production of fir essential oil, and substitute cedar wood oil in perfume industry.
It can be used directly as fragrance by the isolated obtained cedrol of san-mou oil, cedrene, deep processing synthesis can also be carried out The fragrance of high added value.The synthetic perfume of cypress series mainly has: cedrol methyl ether, vertofix coeur, cedryl acetate, epoxy Cedrane, cedralone and cypress olefine aldehydr etc., are all widely used in flavors and fragrances industry.
The extraction of san-mou oil mainly uses steam distillation, solvent extraction and cracking process at present.It is extracted using steam method Fir essential oil aroma of pure, substantially conform to blending requirement, but yield is very low;The fir essential oil yield of extract by solvents is steamed compared with water The problem of gas is high, but needs a large amount of solvent, and subsequent processing is complicated, and it is high that there are energy consumptions, dissolvent residual;Cracking process extracts yield Height, can simultaneously obtain the products such as wood vinegar, charcoal, wood tar and fuel gas, but empyreumatic oil contain a large amount of tar, phenol, The substances such as aldehyde and ketone, seriously affect the quality of san-mou oil.Thick empyreumatic oil has to pass through burnt deodorization processing of dispelling, and can just substantially meet tune Perfume requires.
Although the yield of extraction by steam distillation san-mou oil is come low than solvent extraction method, its cost is comparatively It is cheap, and it is not necessarily to the treatment process of subsequent complexity, thus most domestic producer is extracted using steam distillation at present San-mou oil.Existing san-mou oil production equipment generates vapor generally by water vapor generation device, and vapor is led to Enter to being stacked in the reactor tank of China fir or China fir tree root, by carrying out continuous heating to reactor tank, so as to allow vapor not It is disconnected to penetrate into China fir or China fir tree root, to take away san-mou oil.
The waste material and san-mou oil generated due to the China fir raw material of distillation process can generate waste water after being separated from water and need additionally Processing, therefore we need a kind of production line that can be recycled waste material and waste water.
Summary of the invention
The technical problems to be solved by the present invention are: providing a kind of China fir that can be recycled waste material and waste water Oily production line.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention are as follows: a kind of production line of san-mou oil is provided, is wrapped Include grinding device, conveying device, biomass boiler, san-mou oil extraction element, oily-water seperating equipment and san-mou oil collection device;
Feed inlet and gas outlet are offered at the top of the san-mou oil extraction element, offer discharge port and air inlet on bottom Mouthful;
The biomass boiler includes the drum and wet scrubber that vapor occurs;The wet scrubber includes water inlet Mouthful;
The grinding device is connect by conveying device with feed inlet, and the waste material of the discharge port discharge can be used as biomass Burning of the fuel for biomass boiler uses;The drum is connect with air inlet, and the gas outlet and oily-water seperating equipment connect It connects;
The oily-water seperating equipment includes oil outlet and water outlet, and the oil outlet is connect with san-mou oil collection device, institute The water inlet for stating water outlet and wet scrubber connects.
Further, in the production line of above-mentioned san-mou oil, the production line of the san-mou oil further includes crushing device, described Crushing device is connect by conveying device with grinding device.
Further, in the production line of above-mentioned san-mou oil, the san-mou oil extraction element is alembic, the alembic The feed inlet at top and gas outlet are provided with valve at the material mouth and air inlet of bottom.
Further, in the production line of above-mentioned san-mou oil, heating layer is disposed on the outer surface of the alembic And thermal insulation layer.
Further, in the production line of above-mentioned san-mou oil, pass through pipeline between the gas outlet and oily-water seperating equipment Connection, is additionally provided with cooling instrument between gas outlet and oily-water seperating equipment;The pipeline that spirals passes through cooling instrument.
Further, in the production line of above-mentioned san-mou oil, the cooling instrument further includes coolant liquid, and the coolant liquid is Water.
Further, in the production line of above-mentioned san-mou oil, the production line of the san-mou oil further includes water recovery device, institute Stating water recovery device includes sink and filter device, and the sink is used to accept the liquid of wet scrubber generation;The filtering Device is for the liquid in filtering trough;The filter device is connect with the drum of cooling instrument, biomass boiler.
The beneficial effects of the present invention are: by using biomass boiler, can will be extracted by san-mou oil extraction element Afterwards remaining waste material be used for biomass boiler burning, and the woody part of fir powder be also it is powdered, can greatly be promoted Combustion efficiency is effectively reduced the consumption of the energy, reduces the discharge of carbon dioxide, sulfur dioxide and oxynitrides, changes Environment has been apt to it, has saved fuel cost, has realized energy-saving and emission-reduction;Reduce simultaneously waste generation and processing waste it is required additional Cost;By being used waste water as the water in dust removal of wet scrubber, Sewage treatment can be utilized, reduce disappearing for water resource Consumption, while save the cost.
Detailed description of the invention
Fig. 1 is a kind of structure diagram of san-mou oil production line of the specific embodiment of the invention;
Label declaration: 1, crushing device;2, grinding device;3, biomass boiler;4, san-mou oil extraction element;5, cooling Instrument;6, oily-water seperating equipment;7, san-mou oil collection device.
Specific embodiment
To explain the technical content, the achieved purpose and the effect of the present invention in detail, below in conjunction with embodiment and cooperate attached Figure is explained.
The most critical design of the present invention is: can will be mentioned by san-mou oil extraction element by using biomass boiler Take burning of the rear remaining waste material for biomass boiler;It, can by being used waste water as the water in dust removal of wet scrubber Sewage treatment is utilized, the consumption of water resource is reduced.
Please refer to Fig. 1, a kind of production line of san-mou oil, including grinding device 2, conveying device, biomass boiler 3, China fir Oil extract device 4, oily-water seperating equipment 6 and san-mou oil collection device 7;
The top of the san-mou oil extraction element 4 offers feed inlet and gas outlet, offered on bottom discharge port and into Port;
The biomass boiler 3 includes the drum and wet scrubber that vapor occurs;The wet scrubber include into The mouth of a river;
The grinding device 2 is connect by conveying device with feed inlet, and the waste material of the discharge port discharge can be used as biology Burning of the matter fuel for biomass boiler 3 uses;The drum is connect with air inlet, the gas outlet and oily-water seperating equipment 6 connections;
The oily-water seperating equipment 6 includes oil outlet and water outlet, and the oil outlet is connect with san-mou oil collection device 7, The connection of the water inlet of the water outlet and wet scrubber.
As can be seen from the above description, production process of the invention are as follows: the China fir raw material meets China fir by the formation of grinding device 2 The fir powder that wood oil extraction element 4 uses, the fir powder enter san-mou oil extraction element 4 by feed inlet by conveying device In, the vapor that biomass boiler 3 generates is passed through by air inlet, the vapor in fir powder san-mou oil and wooden progress Separation distills and generates the hot steam containing san-mou oil;The hot steam by gas outlet enter in oily-water seperating equipment 6 into Row water-oil separating, and wooden, the burning that can be collected by discharge port and can be used as biomass fuel for biomass boiler 3 It uses;By in oily-water seperating equipment 6 carry out water-oil separating at fir essential oil and waste water, the fir essential oil by oil outlet into Enter into san-mou oil collection device 7, waste water is entered in the water inlet of wet scrubber by water outlet, is used for biomass boiler 3 dedusting.
As can be seen from the above description, the beneficial effects of the present invention are: by using biomass boiler 3, China fir can will be passed through Remaining waste material is used for the burning of biomass boiler 3 after wood oil extraction element 4 extracts, and the woody part of fir powder is also powder Shape can greatly promote combustion efficiency, be effectively reduced the consumption of the energy, reduce carbon dioxide, sulfur dioxide and nitrogen The discharge of oxygen compound improves environment, saves fuel cost, realizes energy-saving and emission-reduction;Generation and the place of waste are reduced simultaneously Manage the required extra cost of waste;It, can be by Sewage treatment benefit by being used waste water as the water in dust removal of wet scrubber With reducing the consumption of water resource, while save the cost.
Further, the production line of the san-mou oil further includes crushing device 1, and the crushing device 1 passes through conveying device It is connect with grinding device 2.
As can be seen from the above description, China fir raw material can be carried out to preliminary stripping and slicing or broken, subtracted by crushing device 1 The facility load of self raising flour crushing device 2.
Further, the san-mou oil extraction element 4 is alembic, feed inlet and gas outlet at the top of the alembic, Valve is provided at the material mouth and air inlet of bottom.
As can be seen from the above description, can be realized the sealing of alembic, thus more convenient control alembic by valve Interior reaction.
Further, heating layer and thermal insulation layer are disposed on the outer surface of the alembic.
As can be seen from the above description, the behaviour of the processes such as heating or heat-insulation preheating can be carried out to alembic by heating layer Make, by thermal insulation layer, avoids the heat losses in heating layer or alembic, cause distilling effect poor.
Further, it is connected between the gas outlet and oily-water seperating equipment 6 by pipeline, gas outlet and water-oil separating fill It sets and is additionally provided with cooling instrument 5 between 6;The pipeline that spirals passes through cooling instrument 5.
As can be seen from the above description, spiraling by pipeline across cooling instrument 5, it is capable of increasing the contact surface of pipeline and cooling instrument 5 Product, promoted cooling effect, thus make the hot steam in pipeline be cooled into containing distillate enter oily-water seperating equipment 6 In, it is more convenient water-oil separating.
Further, the cooling instrument 5 further includes coolant liquid, and the coolant liquid is water.
As can be seen from the above description, since the cost of water is low, it is convenient and pollution-free to obtain by using water as coolant liquid.
Further, the production line of the san-mou oil further includes water recovery device, the water recovery device include sink and Filter device, the sink are used to accept the liquid of wet scrubber generation;The filter device is for the liquid in filtering trough Body;The filter device is connect with the drum of cooling instrument 5, biomass boiler 3.
As can be seen from the above description, by water recovery device, liquid that can be aqueous caused by the production line by san-mou oil Body carries out recycling filtering, to form circulation, can be realized maximally utilizing for water resource, further decreases disappearing for water resource Consumption, while making cost cheaper.
Embodiment one
A kind of production line of san-mou oil, including crushing device, grinding device, conveying device, biomass boiler, san-mou oil mention Take device, cooling instrument, oily-water seperating equipment and san-mou oil collection device;
The san-mou oil extraction element is alembic, offers feed inlet and gas outlet, bottom at the top of the alembic On offer discharge port and air inlet, the feed inlet at top and gas outlet, be provided with valve at the material mouth and air inlet of bottom; Heating layer and thermal insulation layer are disposed on the outer surface of the alembic.
The biomass boiler includes the drum and wet scrubber that vapor occurs;The wet scrubber includes water inlet Mouthful;
The crushing device is connect by conveying device with grinding device, and the grinding device passes through conveying device and charging Mouth connection, the waste material of the discharge port discharge can be used as burning of the biomass fuel for biomass boiler and use;The drum It is connect with air inlet, the gas outlet is connect with oily-water seperating equipment;
The oily-water seperating equipment includes oil outlet and water outlet, and the oil outlet is connect with san-mou oil collection device, institute The water inlet for stating water outlet and wet scrubber connects.
It is connected between the gas outlet and oily-water seperating equipment by pipeline, the pipeline that spirals passes through cooling instrument.
The cooling instrument further includes coolant liquid, and the coolant liquid is water.
The production line of the san-mou oil further includes water recovery device, and the water recovery device includes sink and filter device, The sink is used to accept the liquid of wet scrubber generation;The filter device is for the liquid in filtering trough;The mistake Filter device is connect with the drum of cooling instrument, biomass boiler.
In conclusion a kind of production line of san-mou oil provided by the invention can will be passed through by using biomass boiler Remaining waste material is used for the burning of biomass boiler after san-mou oil extraction element extracts, and the woody part of fir powder is also powder Shape can greatly promote combustion efficiency, be effectively reduced the consumption of the energy, reduce carbon dioxide, sulfur dioxide and nitrogen The discharge of oxygen compound improves environment, saves fuel cost, realizes energy-saving and emission-reduction;Generation and the place of waste are reduced simultaneously Manage the required extra cost of waste;It, can be by Sewage treatment benefit by being used waste water as the water in dust removal of wet scrubber With reducing the consumption of water resource, while save the cost.
By crushing device, China fir raw material can be carried out to preliminary stripping and slicing or broken, lower the equipment of grinding device Burden.
By valve, the sealing of alembic can be realized, thus the reaction in more convenient control alembic.
By heating layer, the operation that the processes such as heating or heat-insulation preheating can be carried out to alembic is kept away by thermal insulation layer Exempt from the heat losses in heating layer or alembic, causes distilling effect poor.
It is spiraled by pipeline across cooling instrument, is capable of increasing the contact area of pipeline and cooling instrument, promotes cooling effect, from And make the hot steam in pipeline be cooled into containing distillate enter in oily-water seperating equipment, be more convenient water-oil separating.
By using water as coolant liquid, since the cost of water is low, it is convenient and pollution-free to obtain.
By water recovery device, liquid that can be aqueous caused by the production line by san-mou oil carries out recycling filtering, To form circulation, it can be realized maximally utilizing for water resource, further decrease the consumption of water resource, while making cost more Add cheap.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair Equivalents made by bright specification and accompanying drawing content are applied directly or indirectly in relevant technical field, similarly include In scope of patent protection of the invention.

Claims (7)

1. a kind of production line of san-mou oil, which is characterized in that mentioned including grinding device, conveying device, biomass boiler, san-mou oil Take device, oily-water seperating equipment and san-mou oil collection device;
Feed inlet and gas outlet are offered at the top of the san-mou oil extraction element, offer discharge port and air inlet on bottom;
The biomass boiler includes the drum and wet scrubber that vapor occurs;The wet scrubber includes water inlet;
The grinding device is connect by conveying device with feed inlet, and the waste material of the discharge port discharge can be used as biomass fuel Burning for biomass boiler uses;The drum is connect with air inlet, and the gas outlet is connect with oily-water seperating equipment;
The oily-water seperating equipment includes oil outlet and water outlet, and the oil outlet is connect with san-mou oil collection device, it is described go out The connection of the water inlet of the mouth of a river and wet scrubber.
2. the production line of san-mou oil according to claim 1, which is characterized in that the production line of the san-mou oil further includes brokenly Crushing device, the crushing device are connect by conveying device with grinding device.
3. the production line of san-mou oil according to claim 1, which is characterized in that the san-mou oil extraction element is distillation Tank, feed inlet and gas outlet at the top of the alembic are provided with valve at the material mouth and air inlet of bottom.
4. the production line of san-mou oil according to claim 3, which is characterized in that successively set on the outer surface of the alembic It is equipped with heating layer and thermal insulation layer.
5. the production line of san-mou oil according to claim 1, which is characterized in that the gas outlet and oily-water seperating equipment it Between by pipeline connect, cooling instrument is additionally provided between gas outlet and oily-water seperating equipment;The pipeline that spirals passes through cooling instrument.
6. the production line of san-mou oil according to claim 5, which is characterized in that the cooling instrument further includes coolant liquid, institute Stating coolant liquid is water.
7. the production line of san-mou oil according to claim 6, which is characterized in that the production line of the san-mou oil further includes water Recyclable device, the water recovery device include sink and filter device, and the sink is used to accept the liquid of wet scrubber generation Body;The filter device is for the liquid in filtering trough;The drum of the filter device and cooling instrument, biomass boiler connects It connects.
CN201810895178.5A 2018-08-08 2018-08-08 A kind of production line of san-mou oil Pending CN108929783A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106883932A (en) * 2017-04-17 2017-06-23 福建鑫绿林产品开发有限公司 A kind of low energy consumption high yield pulp1 obtains the production method and production line of fir essential oil
CN206706052U (en) * 2017-04-17 2017-12-05 福建鑫绿林产品开发有限公司 A kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil
CN108264966A (en) * 2018-04-08 2018-07-10 福建鑫绿林产品开发有限公司 A kind of fir essential oil production line and production method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106883932A (en) * 2017-04-17 2017-06-23 福建鑫绿林产品开发有限公司 A kind of low energy consumption high yield pulp1 obtains the production method and production line of fir essential oil
CN206706052U (en) * 2017-04-17 2017-12-05 福建鑫绿林产品开发有限公司 A kind of low energy consumption high yield pulp1 obtains the production line of fir essential oil
CN108264966A (en) * 2018-04-08 2018-07-10 福建鑫绿林产品开发有限公司 A kind of fir essential oil production line and production method

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Application publication date: 20181204