CN202666463U - Device for extracting rose essential oil, rose juice and rose glycosides circularly - Google Patents
Device for extracting rose essential oil, rose juice and rose glycosides circularly Download PDFInfo
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- CN202666463U CN202666463U CN 201220345122 CN201220345122U CN202666463U CN 202666463 U CN202666463 U CN 202666463U CN 201220345122 CN201220345122 CN 201220345122 CN 201220345122 U CN201220345122 U CN 201220345122U CN 202666463 U CN202666463 U CN 202666463U
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Abstract
The utility model provides a device for extracting rose essential oil, rose juice and rose glycosides circularly. The device is formed by connecting a feed hopper, a charging machine, a machine unit and a netted plate draining conveyor, wherein the machine unit is formed by connecting an ultrasonic counter-current extractor, a microwave low-temperature distillation machine and a recycling extractor; feed/discharge butterfly valves are arranged at the joint of the ultrasonic counter-current extractor and the microwave low-temperature distillation machine, the joint of the microwave low-temperature distillation machine and the recycling extractor and the head end and tail end of the machine unit respectively; a feed spiral conveyor is arranged in the machine unit and is connected with the feed/discharge butterfly valves; speed reduction motors are arranged at two ends of the feed spiral conveyor respectively; a discharge hole is formed in the tail part of the feed spiral conveyor and is connected with the netted plate draining conveyor; the speed reduction motors are arranged at the end of the netted plate draining conveyor; a discharge spiral conveyor is arranged in the netted plate draining conveyor; and waste residue outlets are formed in the tail part of the netted plate draining conveyor. By the device, rose can be extracted comprehensively and recycled, so that energy consumption is reduced, and the quality is improved.
Description
Technical field
The utility model belongs to the purification apparatus of rose, particularly a kind of extraction element for extraction Rosa Damascana, rose juice, rose glycosides.
Background technology
China's bitter water rose belongs to the rose family, upright shrub, and it grows in world-famous " township of Chinese rose " Yongdeng County, Gansu Province misery town, riverside, Zhuanglang, the upper reaches of the Yellow River, height above sea level 1650m north latitude 36o.This rose variety is in the world rare plateau rose variety, now has been subject to the duplicate protection of State General Administration for Quality Supervision's " original producton location mark " and State Administration for Industry ﹠ Commerce's " certificate of origin trade mark ".Contained 3/10000ths the Rosa Damascana expert that is correlated with is referred to as " liquid golden ", Rosa Damascana be widely used in pharmacy, health care, flavoring essence, highclass perfumes, flavouring essence for tobacco, etc. the field.Its value is embodied in the tiny absorption of human body of being convenient to of molecule, dispersing liver and promoting blood circulation, resuscitation with aromatics.Contained selenium element reaches 38.8 microgram/kilograms, has anti-cancer, anticancer, the effect that delays senility.Particularly be subject in recent years the domestic people that pay attention to taking care of health that like to be beautiful and favored, had a sudden rise in social status, rose to now 280,000 yuan/kg by 30,000 yuan/kg in 2000.And local Rosa Damascana extraction process also rests on the most original steam distillation method state at present, this process energy consumption is large, oil yield is low, maximum drawback is that the production technology that falls behind has only gathered 20% rose value, and do not carry out recycling to rose-juice, anthocyanidin, flavones, polysaccharide, organic nucleic acid equal size, and a large amount of slag and effluents behind the extraction Rosa Damascana are also recycled, unfortunately tangible.And serious pollution the upper reaches of the Yellow River riverside, Zhuanglang human livestock drinking water and the agricultural irrigation safety of a large amount of waste residues, waste liquid of getting rid of.Not too high to recycling raw material and the production cost of causing of rose, and make enterprise enter the passive situation of low repayment with high investment, the serious process that hinders the rose industry, make leading enterprise can not get tremendous development, plant interest thereby affect the flower-grower, industrial chain can not get extending, have a strong impact on local farmers and fiscal revenues, make " bitter water rose " this plateau wonderful work not in full bloom, gorgeous brilliant heartily, its resource is wasted.
At present, the technique of extraction Rosa Damascana has: water-boiling method, CO
2Supercritical extract, solvent extraction;
Water-boiling method: namely utilizing 100 ℃ of boiling water that fresh rose flower is carried out boiling in 4 hours, producing gas and carry out condensation, extracting a small amount of Rosa Damascana and can't carry out recycling to colored juice a large amount of in the rose, anthocyanidin, flavones, polysaccharide, nucleic acid.
CO
2Supercritical extract: namely utilize CO
2Under supercriticality rose is carried out separating and extracting, obtain 40/10000ths rose medicinal extract, remarkable benefit is than water-boiling method.But, owing under supercriticality, produce, just be equivalent to the powerful time bomb operation in the crown, and because super-pressure production, so container is very little, so production cost is high than water-boiling method, undoubtedly in making the matter worse, and also can't put to good use rose is recycling.
The solvent extraction present situation: adopting No. 4 solvents is benzinum, caryophyllane equal solvent, although CO roughly the same
2The supercritical extract production technology also can be produced 40/10000ths rose medicinal extract, distills with alcohol immersion again, makes ethanol break away from the concentrated rear rose absolute that produces of medicinal extract.This production technology, technology be mature and feasible, and compares with supercritical extract, and the blast coefficient reduces, but also belongs to inflammable and explosive, and working condition requires very high.Accidental once-through operation error can be bred disaster, and makes enterprise suffer deathblow.In addition, owing to the easiest leakage of solvent, volatilization, thus take to produce under the closed state, can't be recycling to rose.Up to now without any very thorough to solvent and feed separation of a kind of technique, solvent remains in the material all the time, and product purpose is had a greatly reduced quality, and is restricted, and can't enter food ranks and medicine and healthcare field.
Conclusion draws; (1) although the water-boiling method production technology is simple, and equipment investment is little, convenient operation, natural, the green performance of product is strong, the use safety applications is extensive, but owing under the condition of high temperature, produce, so oil yield is low, poor quality, power consumption is high, can't be recycling to rose, should not carry out.(2) CO
2Although having significantly improvement to be better than water-boiling method than the poach way of distillation, supercritical extract can obtain 40/10000ths rose medicinal extract, energy consumption decreases, but this technological equipment investment is high, the production safety coefficient requires high, in addition because the restriction of being produced container, make it production cost and be higher than the poach way of distillation and should not promote.(3) solvent extraction, this technique also can obtain 40/10000ths rose medicinal extract, are better than water-boiling method and CO
2Overcritical production technology.Than CO
2Supercritical extract small investment convenient operation, production safety is than CO
2Supercritical extraction process is much lower, but also belongs to inflammable and explosive, and safety precaution requires very high technique, and penetrating solvent can't thoroughly be separated in the material, is unsuitable for food service industry, and the pharmacy healthcare field is so should not promote.And subsequent technique is also complicated, concentrates with the ethanol secondary separation to draw rose absolute and can't obtain the pure natural Rosa Damascana.CO
2The rose medicinal extract subsequent technique of supercritical extract is also complicated, utilizes the macromolecule distillation equipment to carry out secondary separation, draw rose absolute and also can't obtain the pure natural Rosa Damascana, and the after-cost is higher.
The utility model content
The purpose of this utility model provides a kind of efficient, energy-conservation, low-cost, recycling, oil extraction plant of being suitable for Rosa Damascana that industrialization, serialization produce, rose juice, rose glycosides, and the oil yield that exists with the method that solves existing extraction Rosa Damascana is low, cost is high, problem that can't be recycling to rose.
For achieving the above object, the utility model is by the following technical solutions:
A kind of cycling extraction Rosa Damascana, rose juice, the extraction element of rose glycosides, by feed hopper, feeder, body, web plate drains conveyer and is formed by connecting, described body is by ultrasonic wave counter-current extraction machine, microwave low temperature distillation machine, recycling extractor is connected in sequence, the junction of described ultrasonic wave counter-current extraction machine and microwave low temperature distillation machine, the junction of microwave low temperature distillation machine and recycling extractor is respectively equipped with an input and output material dish valve, the head end of described body and tail end are respectively equipped with an input and output material dish valve, be provided with feeding spiral conveyer in the described body, described feeding spiral conveyer links to each other with each input and output material dish valve, the two ends of described feeding spiral conveyer are respectively equipped with a reducing motor, the feeding spiral conveyer afterbody is provided with discharging opening, described discharging opening drains conveyer with web plate and links to each other, the end that described web plate drains conveyer is provided with a reducing motor, web plate drains and is provided with discharging spiral conveyor in the conveyer, and the afterbody that described web plate drains conveyer is provided with the waste residue outlet.
The bottom of described body is provided with exhaust-valve, described internal body and web plate drain the conveyer bottom and are equipped with overanxious web plate, described feeding spiral conveyer and discharging spiral conveyor all are provided with shaft, described shaft is provided with stirring vane, be provided with ultrasonic unit in the described ultrasonic wave counter-current extraction machine, ultrasonic wave counter-current extraction chain-drive section top is provided with the rose-juice outlet, and ultrasonic wave counter-current extraction drive end unit top is provided with the pure water entrance; Be provided with microwave heating equipment in the described microwave low temperature distillation machine, the top of microwave low temperature distillation machine is provided with saturated retort gas outlet, and the afterbody top of microwave low temperature distillation machine is provided with the fuliu water inlet; The apical head of described recycling extractor is provided with mixture export, and the afterbody top of recycling extractor is provided with the waste liquid entrance, and the bottom that the tail end bottom of described body and described web plate drain conveyer respectively is provided with a waste liquid outlet.
The top of described body is provided with the photoscope device.
Be respectively equipped with a fluid level control device in described ultrasonic wave counter-current extraction machine, microwave low temperature distillation machine, the recycling extractor.
Described each input and output material dish valve place is provided with a heat insulation dividing plate of body.
The shell of described body is provided with inspection manhole.
The utility model has the advantages that: 1, outstanding energy-conservation, recycling, ultrasonic wave extracts, microwave heating low-temperature extraction, waste residue and liquid are recycled, technique is simple, convenient operation, production cost is low, extraction efficiency is high, and is safe and reliable, reduces power consumption, comprehensive utilization, energy-conserving and environment-protective, industry-leading.2, this device makes whole production process realize full serialization and industrial scale production, has solved full serialization and industrial scale and has processed the technical barrier of discarded object recycling behind the attar of rose and the difficult problem of rose-juice and the recycling isolation technics of extraction.3, drain conveyer by ultrasonic extracting machine microwave heating low-temperature extracter and web plate, the extraction equipment that the parts such as the recycling extractor of waste residue and liquid form, easy and simple to handle after the material dosing automatic control, Separation of Solid and Liquid is complete, in succession obtain 1.6% anthocyanidin, 4/10000ths Rosa Damascana, 30% flower glycosides, 60% rose flavored juice.The products obtained therefrom basic controlling is in critical field.4, this device not only adapts to the comprehensive extraction and application to rose, also be applicable to STEVIA REBAUDIANA, lavender, peppermint, etc. the comprehensive extraction of natural plants.Waste residue after comprehensive cyclic utilization is extracted can make the flower protein feed or organic fertilizer etc. is made in fermentation.
The utility model can be recycling to the comprehensive extraction of rose, reduces energy consumption, promotes quality, and solved the pollution of slag and effluent to environment, recycled simultaneously limited resource, has very high economic benefit and social value.
Below in conjunction with accompanying drawing the utility model is described further.
Description of drawings
Fig. 1 is the structural representation of the A-B of first section of the present utility model;
Fig. 2 is the structural representation of second portion B-C section of the present utility model;
Fig. 3 is the structural representation of third part C-D section of the present utility model;
Fig. 4 is the structural representation of the 4th part D-E section of the present utility model.
Among the figure, the 1-body, the 2-feeding spiral conveyer, 3-input and output material dish valve, the heat insulation dividing plate of 4-body, 5-ultrasonic wave counter-current extraction machine, 6-microwave low temperature distillation machine, the recycling extractor of 7-, the 8-tail, the 9-web plate drains conveyer, the 10-feeder, the 11-feed hopper, the 12-discharging opening, the 13-ultrasonic unit, the 14-microwave heating equipment, the 15-shaft, the 16-stirring vane, the outlet of 17-rose-juice, 18-pure water entrance, the 19-exhaust-valve, the saturated retort gas outlet of 20-, 21-fuliu water inlet, the 22-mixture export, 23-photoscope device, the 24-fluid level control device, the 26-reducing motor, the 27-inspection manhole, the overanxious web plate of 28-, 32-waste liquid entrance, the 33-waste liquid outlet, the outlet of 34-waste residue, the 36-discharging spiral conveyor.
The specific embodiment
The utility model is main equipment, whole is connected to form by the AB section among Fig. 1, BC section, CD section among Fig. 3 and the DE section among Fig. 4 among Fig. 2.
Such as 1, Fig. 2, shown in Fig. 3 and Fig. 4 figure, the utility model cycling extraction Rosa Damascana, rose juice, the extraction element of rose glycosides, by feed hopper 11, feeder 10, body 1, web plate drains conveyer 9 and is formed by connecting, body 1 is by ultrasonic wave counter-current extraction machine 5, microwave low temperature distillation machine 6, recycling extractor 7 is connected in sequence, the junction of ultrasonic wave counter-current extraction machine 5 and microwave low temperature distillation machine 6, the junction of microwave low temperature distillation machine 6 and recycling extractor 7 is respectively equipped with an input and output material dish valve 3, the head end of body 1 and tail end are respectively equipped with an input and output material dish valve 3, be provided with feeding spiral conveyer 2 in the body 1, feeding spiral conveyer 2 links to each other with each input and output material dish valve 3, the two ends of feeding spiral conveyer 2 are respectively equipped with a reducing motor 26, feeding spiral conveyer 2 afterbodys are provided with discharging opening 12, discharging opening 12 drains conveyer 9 with web plate and links to each other, the end that web plate drains conveyer 9 is provided with a reducing motor 26, web plate drains and is provided with discharging spiral conveyor 36 in the conveyer 9, and the afterbody that web plate drains conveyer 9 is provided with waste residue outlet 34.
The bottom of body 1 is provided with exhaust-valve 19, and body 1 inside and web plate drain conveyer 9 bottoms and be equipped with overanxious web plate 28, are equipped with shaft 15 on feeding spiral conveyer 2 and the discharging spiral conveyor 36, and shaft 15 is provided with stirring vane 16; Be provided with ultrasonic unit 13 in the ultrasonic wave counter-current extraction machine 5, ultrasonic wave counter-current extraction machine 5 apical heads are provided with rose-juice outlet 17, and ultrasonic wave counter-current extraction machine 5 afterbody tops are provided with pure water entrance 18; Be provided with microwave heating equipment 14 in the described microwave low temperature distillation machine 6, the top of microwave low temperature distillation machine 6 is provided with saturated retort gas outlet 20, and the afterbody top of microwave low temperature distillation machine 6 is provided with fuliu water inlet 21; The apical head of recycling extractor 7 is provided with mixture export 22, and the afterbody top of recycling extractor 7 is provided with waste liquid entrance 32; The bottom that the tail end bottom of body 1 and web plate drain conveyer 9 respectively is provided with a waste liquid outlet 33.
Each input and output material dish valve 3 place is provided with a heat insulation dividing plate 4 of body.
The shell of body 1 is provided with inspection manhole 27.
The top of body 1 is provided with photoscope device 23.
Be respectively equipped with a fluid level control device 24 in ultrasonic wave counter-current extraction machine 5, microwave low temperature distillation machine 6, the recycling extractor 7.
Operation principle of the present utility model is as follows:
Fresh rose flower is sent into feed hopper by the raw material elevator, send into ultrasonic wave counter-current extraction machine after sending into feeding spiral conveyer and pure water mixes by charging dish valve.In charging, feeding spiral conveyer replaces agitating device to stir simultaneously, make mixing of materials even, reach liquid level rear feeding dish valve autoshutdown, agitating device stirs simultaneously, at this moment, ultrasonic wave plays a role, and pure water injects by pressure and makes it produce counter flow action, the rapid lixiviate rose of helping ultrasonic wave juice, and send into concentrated workshop through discharging opening fast and carry out concentrating and separating, obtain the products such as anthocyanidin.Observe by photoscope device and fluid level control device, rose-juice is extracted the rear microwave low temperature distillation machine that enters rapidly, utilize rapidly the microwave certain power to add the auxiliary low temperature distillation of carrying out of a small amount of steam, saturated vapor is sent into condenser to be cooled off, enter oil water separator and get attar of rose, again the distillate after the water-oil separating is sent into microwave low temperature distillation machine again and carried out fuliu.Observe by photoscope device and fluid level control device, the rose slag that extracts behind the attar of rose is sent into recycling extractor by conveying worm, and adverse current stirs sedimentation fast, soaks when reaching liquid level, send into rapidly concentrated workshop, add ethanol and carry out the concentrated rose glycosides that obtains of lixiviate.Send into slag and effluent by feeding spiral conveyer after waste residue separated and drain machine and drain conveyer with web plate more last mixed waste liquor is separated, send into recycling extractor through circulating pump and carry out second extraction.
Above-described embodiment is preferred embodiment of the present invention; but the utility model mode is not restricted to the described embodiments; other any do not deviate from change, the modification of making under spirit of the present invention and the technology or substitutes, and all should be equivalent replacement, all is contained within the protection domain of the present utility model.
Claims (6)
1. cycling extraction Rosa Damascana, rose juice, the extraction element of rose glycosides, it is characterized in that: it is by feed hopper (11), feeder (10), body (1), web plate drains conveyer (9) and is formed by connecting, described body (1) is by ultrasonic wave counter-current extraction machine (5), microwave low temperature distillation machine (6), recycling extractor (7) is connected in sequence, the junction of described ultrasonic wave counter-current extraction machine (5) and microwave low temperature distillation machine (6), the junction of microwave low temperature distillation machine (6) and recycling extractor (7) is respectively equipped with an input and output material dish valve (3), the head end of described body (1) and tail end are respectively equipped with an input and output material dish valve (3), be provided with feeding spiral conveyer (2) in the described body (1), described feeding spiral conveyer (2) links to each other with each input and output material dish valve (3), the two ends of described feeding spiral conveyer (2) are respectively equipped with a reducing motor (26), feeding spiral conveyer (2) afterbody is provided with discharging opening (12), described discharging opening (12) drains conveyer (9) with web plate and links to each other, the end that described web plate drains conveyer (9) is provided with a reducing motor (26), web plate drains and is provided with discharging spiral conveyor (36) in the conveyer (9), and the afterbody that described web plate drains conveyer (9) is provided with waste residue outlet (34).
2. the extraction element of cycling extraction Rosa Damascana as claimed in claim 1, rose juice, rose glycosides, it is characterized in that: the bottom of described body (1) is provided with exhaust-valve (19), described body (1) inside and web plate drain conveyer (9) bottom and are equipped with overanxious web plate (28), described feeding spiral conveyer (2) and discharging spiral conveyor (36) all are provided with shaft (15), and described shaft (15) is provided with stirring vane (16); Be provided with ultrasonic unit (13) in the described ultrasonic wave counter-current extraction machine (5), ultrasonic wave counter-current extraction machine (5) apical head is provided with rose-juice outlet (17), and ultrasonic wave counter-current extraction machine (5) afterbody top is provided with pure water entrance (18); Be provided with microwave heating equipment (14) in the described microwave low temperature distillation machine (6), the top of microwave low temperature distillation machine (6) is provided with saturated retort gas outlet (20), and the afterbody top of microwave low temperature distillation machine (6) is provided with fuliu water inlet (21); The apical head of described recycling extractor (7) is provided with mixture export (22), the afterbody top of recycling extractor (7) is provided with waste liquid entrance (32), and the bottom that the tail end bottom of described body (1) and described web plate drain conveyer (9) respectively is provided with a waste liquid outlet (33).
3. the extraction element of cycling extraction Rosa Damascana as claimed in claim 1 or 2, rose juice, rose glycosides, it is characterized in that: the top of described body (1) is provided with photoscope device (23).
4. the extraction element of cycling extraction Rosa Damascana as claimed in claim 3, rose juice, rose glycosides is characterized in that: be respectively equipped with a fluid level control device (24) in described ultrasonic wave counter-current extraction machine (5), microwave low temperature distillation machine (6), the recycling extractor (7).
5. the extraction element of cycling extraction Rosa Damascana as claimed in claim 4, rose juice, rose glycosides, it is characterized in that: described each input and output material dish valve (3) locates to be provided with a heat insulation dividing plate of body (4).
6. the extraction element of cycling extraction Rosa Damascana as claimed in claim 5, rose juice, rose glycosides, it is characterized in that: the shell of described body (1) is provided with inspection manhole (27).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220345122 CN202666463U (en) | 2012-07-17 | 2012-07-17 | Device for extracting rose essential oil, rose juice and rose glycosides circularly |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220345122 CN202666463U (en) | 2012-07-17 | 2012-07-17 | Device for extracting rose essential oil, rose juice and rose glycosides circularly |
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| Publication Number | Publication Date |
|---|---|
| CN202666463U true CN202666463U (en) | 2013-01-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220345122 Expired - Fee Related CN202666463U (en) | 2012-07-17 | 2012-07-17 | Device for extracting rose essential oil, rose juice and rose glycosides circularly |
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| CN (1) | CN202666463U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105524717A (en) * | 2015-12-21 | 2016-04-27 | 衡阳智源农业科技有限公司 | Novel rose oil extraction machine |
| CN109576057A (en) * | 2018-12-07 | 2019-04-05 | 湖北好雨时节生物科技有限公司 | Effective component high-efficiency device for extracting and extracting method in a kind of roseleaf |
| CN109749852A (en) * | 2019-03-13 | 2019-05-14 | 甘肃瑰隆生物科技有限公司 | The conveying charging process of rose in a kind of Rosa Damascana extraction process |
-
2012
- 2012-07-17 CN CN 201220345122 patent/CN202666463U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105524717A (en) * | 2015-12-21 | 2016-04-27 | 衡阳智源农业科技有限公司 | Novel rose oil extraction machine |
| CN109576057A (en) * | 2018-12-07 | 2019-04-05 | 湖北好雨时节生物科技有限公司 | Effective component high-efficiency device for extracting and extracting method in a kind of roseleaf |
| CN109749852A (en) * | 2019-03-13 | 2019-05-14 | 甘肃瑰隆生物科技有限公司 | The conveying charging process of rose in a kind of Rosa Damascana extraction process |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130116 Termination date: 20180717 |
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| CF01 | Termination of patent right due to non-payment of annual fee |