CN206355640U - A kind of hydrodistillation device with oil water separator - Google Patents
A kind of hydrodistillation device with oil water separator Download PDFInfo
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- CN206355640U CN206355640U CN201720022350.7U CN201720022350U CN206355640U CN 206355640 U CN206355640 U CN 206355640U CN 201720022350 U CN201720022350 U CN 201720022350U CN 206355640 U CN206355640 U CN 206355640U
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- hydrodistillation
- oil
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- water separator
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Abstract
The utility model discloses a kind of hydrodistillation device with oil water separator, including：Extractor (9), its outer layer has heater (10), its upper port exports the bottom that (8) connect condenser pipe (1) by retort gas, and its lower port connects steam generator (12) upper port by steam outlet (11)；Oil water separator (5), its upper port connects condenser pipe (1) lower port by condensing fluid outlet (3), its middle and upper part connects the top of the steam generator (12) by moisture outlet (4), and bottom has oil to export (6).Device of the present utility model is simple, can continuously run, efficiency high can apply to laboratory and industrialized production.
Description
Technical field
The utility model belongs to chemical apparatuses technical field, and in particular to a kind of hydrodistillation dress with oil water separator
Put.
Background technology
Extracting effective ingredient of volatile component such as Chinese medicine of plant etc. has many methods, such as supercritical methanol technology.This method
Advantage be to carry out at low temperature, do not destroy volatile component.But the equipment of this method is complicated, extraction cost is higher.Have
The volatile component of a little plants is more stable and water insoluble, can use hydrodistillation, but there is presently no can be continuously and steady
Fixed this device.
Utility model content
The utility model provides a kind of hydrodistillation device with oil water separator, and device of the present utility model can be used
Hydrodistillation is with the volatile component of some plants, and efficiency high, device are simple, and extract purity is high.
A kind of hydrodistillation device with oil water separator of the present utility model, including：
Extractor 9, its outer layer has heater 10, and its upper port is connected under condenser pipe 1 by retort gas outlet 8
Portion, its lower port connects the upper port of steam generator 12 by steam outlet 11；
Oil water separator 5, its upper port connects the lower port of condenser pipe 1 by condensing fluid outlet 3, and its middle part passes through moisture
The top of the connection of outlet 4 steam generator 12, bottom has oil to export 6.
Preferably, the outer layer heater 10 of the extractor 9 is steam heating interlayer.
Preferably, the outer layer of condenser pipe 1 is condensation water interlayer, and condensed water water inlet 2, top are arranged at condensation water interlayer bottom
There is condensed water delivery port 7.
Preferably, the volume of the extractor 9 is 50~100L.
Extraction element step of the present utility model is：Plant is put into extractor, with the water in steam generator
Steam extraction plant, the condensed water water inlet of plant condenser pipe is passed through cold water, and the steam heating interlayer of extractor is passed through water steaming
Vapour.After the condensed pipework condensation of volatile oil component through hydrodistillation, water vapour becomes aqueous water, enters together with volatile oil component
Enter oil water separator, after being separated through oil water separator, moisture reenters steam generator through moisture outlet, and moisture is obtained
Recycle；1~3h of extraction time, after extraction terminates, releasing oil component from the oil outlet of oil water separator bottom is
The higher plant extracts of purity.
The advantage of the utility model device：
1st, device of the present utility model is simple, can continuously run, efficiency high, can apply to laboratory and industrial metaplasia
Production.
2nd, the outer layer of device extractor of the present utility model is furnished with steam heating interlayer, can control in the tank of extractor
Temperature is more than 100 DEG C, so as to ensure that the water vapour of steam generator generation keeps steam condition after entering extractor, no
Water can be condensed into, extraction effect is more preferable.
3rd, after the condensed pipework condensation of volatile oil component through hydrodistillation, water vapour becomes aqueous water, with volatile oil into
Divide and enter oil water separator together, after being separated through oil water separator, moisture reenters steam generator through moisture outlet,
Moisture is recycled；Volatile oil component is exported from oil to flow out, so as to obtain the higher volatile component of plant of purity.
4th, the volatile component of plant normal temperature lower density that device of the present utility model can be extracted is more than the plant component of water,
Such as extract the chemical composition in tobacco, the chemical composition in radix glycyrrhizae.
Brief description of the drawings
Fig. 1 is a kind of hydrodistillation schematic device with oil water separator of the present utility model
Reference is：1- condenser pipes, 2- condensed water water inlets, 3- condensation fluid outlets, 4- moisture outlets, 5- profits point
From device, the outlet of 6- oils, 7- condensed water delivery ports, the outlet of 8- retort gas, 9- extractors, 10- heaters, 11- water vapours
Outlet, 12- steam generators.
Embodiment
Embodiment 1：Extract the extraction of the volatile chemical component in offal
Offal 10kg is put into 100L extractors, 1L 5wt% aqueous citric acid solution (effect is added：Contain in tobacco leaf
The alkaline matters such as a large amount of volatile nicotine, if be extracted, can influence the quality of volatile oil, citric acid and alkaline matter
With reference to, become ionic compound, it is not volatile, and density is more than water), then carried with the water vapour in steam generator
Take.The condensed water water inlet of condenser pipe is passed through cold water, and the steam heating interlayer of extractor is passed through water vapour, through hydrodistillation
The condensed pipework condensation of volatile oil component after, water vapour becomes aqueous water, together with volatile oil component enter oil water separator, warp
After oil water separator separation, moisture reenters steam generator through moisture outlet, and moisture is recycled；During extraction
Between 1~3h, after extraction terminates, it is that the higher tobacco of purity carries to release oil component from the outlet of the oil of oil water separator bottom
Take thing.
Embodiment 2：The extraction of volatile chemical component in radix glycyrrhizae powder
Radix glycyrrhizae powder 5kg is put into 50L extractors, then with the hydrodistillation in steam generator, condensation
The condensed water water inlet of pipe is passed through cold water, and the steam heating interlayer of extractor is passed through water vapour, the volatilization through hydrodistillation
After the condensed pipework condensation of oil component, water vapour becomes aqueous water, and oil water separator is entered together with volatile oil component, through profit point
After device separation, moisture reenters steam generator through moisture outlet, and moisture is recycled；Extraction time 1~
3h, after extraction terminates, it is the higher licorice of purity to release oil component from the oil outlet of oil water separator bottom.
Claims (4)
1. a kind of hydrodistillation device with oil water separator, it is characterised in that including：
Extractor (9), its outer layer has heater (10), and its upper port exports (8) by retort gas and connects condenser pipe (1)
Bottom, its lower port connects steam generator (12) upper port by steam outlet (11)；
Oil water separator (5), its upper port connects condenser pipe (1) lower port by condensing fluid outlet (3), and its middle and upper part passes through
Moisture outlet (4) connects the top of the steam generator (12), and bottom has oil to export (6).
2. hydrodistillation device according to claim 1, it is characterised in that the outer layer heating dress of the extractor (9)
(10) are put for steam heating interlayer.
3. hydrodistillation device according to claim 1, it is characterised in that condenser pipe (1) outer layer is condensed water
Interlayer, condensation water interlayer bottom has condensed water water inlet (2), top to have condensed water delivery port (7).
4. hydrodistillation device according to claim 1, it is characterised in that the volume of the extractor (9) is 50~
100L。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720022350.7U CN206355640U (en) | 2017-01-07 | 2017-01-07 | A kind of hydrodistillation device with oil water separator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720022350.7U CN206355640U (en) | 2017-01-07 | 2017-01-07 | A kind of hydrodistillation device with oil water separator |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206355640U true CN206355640U (en) | 2017-07-28 |
Family
ID=59380270
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720022350.7U Active CN206355640U (en) | 2017-01-07 | 2017-01-07 | A kind of hydrodistillation device with oil water separator |
Country Status (1)
| Country | Link |
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| CN (1) | CN206355640U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108034500A (en) * | 2017-12-29 | 2018-05-15 | 苏州勃朗科技股份有限公司 | A kind of family expenses plants essential oil fragrance extraction element |
-
2017
- 2017-01-07 CN CN201720022350.7U patent/CN206355640U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108034500A (en) * | 2017-12-29 | 2018-05-15 | 苏州勃朗科技股份有限公司 | A kind of family expenses plants essential oil fragrance extraction element |
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