CN103638690A - Boiling and extracting device and method for honeysuckle - Google Patents
Boiling and extracting device and method for honeysuckle Download PDFInfo
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- CN103638690A CN103638690A CN201310619624.7A CN201310619624A CN103638690A CN 103638690 A CN103638690 A CN 103638690A CN 201310619624 A CN201310619624 A CN 201310619624A CN 103638690 A CN103638690 A CN 103638690A
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Abstract
The invention relates to a boiling and extracting device and method for honeysuckle. The boiling and extracting device and method have the advantages that a boiling tank is connected with a condenser in series; by adopting a process method of compatibility of boiling and distilling, honeysuckle materials enter a net plate in the boiling tank, then water is added in the boiling tank to enable the distance between the water level and the net plate to be 5-10cm, steam is introduced into water of the boiling tank, and the honeysuckle is in a critical state in infiltration; in the boiling process, a feed liquid of effective components of the honeysuckle with the coexistence of a gaseous state and a liquid state flows out from a liquid discharging pipe to rowed pipes in the condenser, the flowing speed is 5-8L/min, then the feed liquid is cooled to be below 40 DEG C by normal-temperature water outside the pipes, the whole feed liquid is transformed into the liquid and is collected by a liquid outlet; the normal-temperature water outside the rowed pipes is replaced to hot water; the circulating hot water with the temperature rising to 70-80 DEG C is conveyed to the boiling tank as solvent hot water; the steps are repeatedly carried out, the high efficiency and the energy-saving effect are achieved; not only can effective components such as chlorogenic acid and flavonoid of the honeysuckle be extracted to a greater extent, but also the effective components such as honeysuckle oil contained in volatile gas can be completely recovered.
Description
Technical field
The invention belongs to Chinese medicine and extract manufacture field, particularly relate to a kind of honeysuckle and boil steaming extraction element and method.
Background technology
Honeysuckle is caprifoliaceae plant dry flower or the first flower of opening of band of honeysuckle, herb all can be used as medicine, bud contains volatility honeysuckle aromatic oil, inositol, saponin(e, chlorogenic acid, the compounds such as flavonoids, cinnamic acid, nerol, jasmine arrives aldehyde etc., in stem, contain biological salty, he is rhinoceros element etc. in leaf, to contain lonicerin, wherein, chlorogenic acid is the main pharmacodynamics active component of honeysuckle, also have the compounds such as flavonoids, other volatility honeysuckle wet goods active ingredient also has medical value, also be one of traditional Chinese medicine material, have clearing heat and detoxicating, wind-heat dissipating, the effect of hepatic cholagogic, the swollen sore for the treatment of of carbuncle, larynx numbness, anemopyretic colds etc. all have good curative effect, chlorogenic acid is to digestive system, hematological system and reproductive system all have pharmacological action, there is anti-inflammation widely, cholagogic, the effect that white blood cell count is increased in hemostasis.At present, from honeysuckle extracting method and from honeysuckle the method for chlorogenic acid extracting, mainly contain water extraction, water extract-alcohol precipitation, rare alcohol extracting etc., as Chinese patent CN201010124495.0 discloses " a kind of method that adopts combined-enzyme method to extract Chlorogenic Acid of Flos Lonicerae " proposition, adopt the combined-enzyme method new technology chlorogenic acid extracting of cellulase and pectase.
Chinese patent CN201210308017.4 discloses " a kind of from honeysuckle-leaf chlorogenic acid extracting and Hyperoside method " and has proposed a kind of utilize crystallization and recrystallization method large-scale production chlorogenic acid and Hyperoside from fresh honeysuckle-leaf.
Chinese patent 201110292709.X discloses a kind of method of chlorogenic acid extracting in honeysuckle that " from honeysuckle rapidly and efficiently the method for chlorogenic acid extracting " discloses rapid extraction and be not destroyed in the biologically active of leaching process Content of Chlorogenic Acid and chemical constitution.
Chinese patent CN01144170.4 discloses " method for extraction and purification of Chlorogenic Acid of Flos Lonicerae " and has adopted Diluted Alcohol to carry out secondary back extraction to honeysuckle, concentrated extract, again with the preliminary edulcoration purification of flocculence, finally adopts Amberlyst process or acid ethyl acetate extraction purification refine.
In described patent and patent application or prior art, technology round extracting chlorogenci acid from honeysuckle main component, research honeysuckle main component chlorogenic acid extract yield, and the limitation of extraction process, and some other active ingredient has been left in the basket, to the abundant extraction and application of effective ingredient of honeysuckle, as volatility honeysuckle wet goods active ingredient also has medical value, , there is the process for extracting of some other active ingredient obviously to have drawback, the one, the active ingredient of honeysuckle can not obtain release and the utilization of larger limit, and the infiltration adopting is distilled while extracting processing method, also only limit to extract main component chlorogenic acid etc., the 2nd, in the infiltration distillation adopting, extract processing technology, other active ingredient beyond extraction main component chlorogenic acid etc., but be difficult to form production capacity.
Therefore, research displaces outside effective ingredient of honeysuckle chlorogenic acid and flavonoids etc., reclaims the contained active ingredient of volatilization gas, improves honeysuckle the making full use of of active ingredient in leaching process, and improving production capacity is the problem that need to research and solve.
Summary of the invention
Object of the present invention is exactly the not problem of the abundant extraction and application of efficiency of active ingredient in order to solve honeysuckle, provide a kind of effective ingredient of honeysuckle to obtain the release of larger limit and the honeysuckle of utilization extraction steaming extraction element and method, the technique of honeysuckle water-boiling method and way of distillation compatibility, can larger limit extract outside effective ingredient of honeysuckle chlorogenic acid and flavonoids etc., can all reclaim again the contained composition volatility honeysuckle wet goods active ingredient of volatilization gas.
Another object of the present invention is to provide a kind of honeysuckle and boils the process of steaming extraction use circulating hot water, by boiling steaming pot serial connection condenser, the effective ingredient of honeysuckle feed liquid of boiling steaming extraction through boiling steaming pot is high temperature, by cooling by normal-temperature water in condenser, normal-temperature water is replaced as hot water and is sent to again and boils steaming pot and make solvent hot water, for boiling steaming pot honeysuckle, boil steaming use, so iterative cycles, reaches and extracts complete, energy-efficient object.
The technical solution adopted in the present invention is: a kind of honeysuckle is boiled steaming extraction element, it is characterized in that: the hermetically sealed steaming pot of boiling is provided with feed inlet and outlet, steam inlet, boil steaming pot top access solvent hot-water line, and be furnished with drain pipe and sewage draining exit, boil and in steaming pot, be provided with web plate; Described drain pipe access condenser, condenser is provided with normal-temperature water import, liquid outlet, and condenser top is connected to hot-water line.
Honeysuckle is boiled a steaming extracting method, and concrete steps are as follows:
1) the poach stage, by dropping into and boil in steaming pot after honeysuckle screening, cleaning, is laid on web plate and compacting, shuts feed inlet and outlet; Then add water to boiling in steaming pot, making the water surface and web plate spacing is 5-10cm, opens steam and passes into and boil in steaming pot water, boils water in steaming pot in fluidized state, makes the critical condition of honeysuckle in infiltrating;
Honeysuckle raw material 30-40kg, boils steaming time 2-3 hour, boils in steaming process, the honeysuckle effective ingredient feed liquid that gaseous, liquid coexists flows out to condenser from drain pipe, flow velocity 5-8L/ minute, honeysuckle raw material is with Flos Lonicerae extractive solution yield than 1:45-50, and dirt is discharged from sewage draining exit;
3) cooling stage, the honeysuckle effective ingredient feed liquid that gas-liquid coexists by discharge nozzle to the tubulation in condenser, by the outer normal-temperature water of pipe, being cooled to 40 ℃ is all converted into below liquid and collects from liquid outlet, normal-temperature water outside tubulation is replaced as hot water, water temperature is increased to the circulating hot water of 70-80 ℃ and is delivered to again and boiled steaming pot and make solvent hot water by hot-water line, and the honeysuckle of extraction is collected liquid and comprises chlorogenic acid and honeysuckle wet goods effective ingredient.
Technique scheme of the present invention, has the following advantages:
1, the present invention adopts honeysuckle to boil steaming extracting method, boil steaming pot serial connection condenser, when collecting Flos Lonicerae extractive solution, hot dipping is carried to escaping gas and all give cooling recovery, add water to boiling in steaming pot, and pass into steam to boiling in steaming pot water, boil in steaming process, the effective ingredient of honeysuckle feed liquid that gaseous, liquid coexists by drain pipe to condenser, with boiling, steam technique and extracted whole active ingredient feed liquids that honeysuckle comprises liquid and gaseous state, normal-temperature water in condenser is cooled to below 40 ℃, the effective ingredient of honeysuckle feed liquid that gaseous, liquid coexists all converts liquid to, comprise and extract honeysuckle main component chlorogenic acid, also reclaimed the contained lonicera oil of other active ingredient escaping gas of honeysuckle simultaneously, improve making full use of of effective ingredient of honeysuckle.
2, the present invention adopts honeysuckle to boil steaming process for extracting, below boiling in steaming pot, web plate is set, honeysuckle is laid in and boils also compacting on web plate in steaming pot, by built-in diffusing net above extraction steaming pot, add water to boiling in steaming pot, making the water surface and web plate spacing is 5-10cm, opening steam passes into and boils in steaming pot water, boil water in steaming pot in fluidized state, make the critical condition of honeysuckle in infiltrating, honeysuckle is boiled steam to extract more to divide fully.
3, the present invention is boiled and is steamed extraction element to boil steaming pot be hermetically sealed by honeysuckle, boil below steaming pot liquid outlet is set, and directly deliver in condenser by discharge nozzle, the honeysuckle effective ingredient feed liquid that realization collection gas, liquid coexist, and by the cooling whole active ingredient liquid of honeysuckle of collecting of condenser, by the technique of honeysuckle water-boiling method and way of distillation compatibility, improve chlorogenic acid extract yield, realize honeysuckle material effective component and all make full use of.
4, the present invention is connected in series with condenser owing to boiling steaming pot on adopting process equipment, employing is boiled honeysuckle in steaming pot and is boiled the method that steaming pot is used circulating hot water, making full use of through boiling the effective ingredient of honeysuckle feed liquid discharging of steaming extraction is high temperature, by cooling by normal-temperature water in condenser, and normal-temperature water is replaced as hot water, is sent to and boils steaming pot and make solvent hot water, for boiling steaming pot honeysuckle, boil steam to use hot water be provided, iterative cycles like this, reach extract complete, energy-efficient.
Accompanying drawing explanation
Fig. 1 is that a kind of honeysuckle of the present invention is boiled steaming extraction element structural representation.
Fig. 2 is that a kind of honeysuckle of the present invention is boiled steaming extracting method process flow diagram.
Boil steaming pot 1, feed inlet and outlet 2, steam inlet 3, hot-water line 4, drain pipe 5, sewage draining exit 6, web plate 7, condenser 8, normal-temperature water import 9, liquid outlet 10.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is described in more detail.
As shown in Figure 1, 2, a kind of honeysuckle is boiled steaming extraction element, adopts water-boiling method and way of distillation compatible technology, when collecting Flos Lonicerae extractive solution, hot dipping is carried to gaseous volatilization composition and all gives cooling recovery; On apparatus and process, will boil steaming pot 1 and condenser 8 series connection, and heat energy be transformed mutually and reach energy-conservation.
Boil steaming pot and be designed to hermetically sealedly, the hermetically sealed steaming pot 1 of boiling is provided with feed inlet and outlet 2, steam inlet 3, boils steaming pot 1 top access solvent hot-water line 4, and is furnished with drain pipe 5 and sewage draining exit 6, boils and in steaming pot 1, is provided with web plate 7; Drain pipe 5 access condensers 8, leave normal-temperature water import 9, liquid outlet 10 on condenser 8, condenser 8 tops are connected to hot-water line 4.
Honeysuckle is boiled steaming extracting method, the poach stage, by dropping into and boil in steaming pot after honeysuckle screening, cleaning, be laid on web plate and compacting, and shut feed inlet and outlet; Then add water to boiling in steaming pot, then add running water to the height of technological requirement, guarantee that water and web plate spacing are at 5-10cm, by visor, grasp water surface elevation, opening steam passes into and boils in steaming pot water, boil water in steaming pot in fluidized state, make the critical condition of honeysuckle in infiltrating, boil in steaming and can not have honeysuckle to seethe phenomenon; Honeysuckle raw material 30-40kg, boil steaming time 2-3 hour, boil in steaming process, the honeysuckle effective ingredient feed liquid that gaseous, liquid coexists flows out to condenser from drain pipe, the flow velocity that collection honeysuckle effective ingredient feed liquid flows out from drain pipe should be controlled at 5-8L/ minute and be advisable, honeysuckle raw material is with Flos Lonicerae extractive solution yield than 1:45-50, and dirt is discharged from sewage draining exit.
Cooling stage, the honeysuckle effective ingredient feed liquid that gas-liquid coexists by discharge nozzle to the tubulation in condenser, cooling from the beginning by the tubulation in condenser by normal temperature, the gas-liquid of boiling steaming pot generation effective ingredient of honeysuckle of connecting steam is coexisted, by liquid outlet conveyance conduit warp let-off condenser, by the outer normal-temperature water of pipe, being cooled to 40 ℃ is all converted into below liquid and collects from liquid outlet, be about to gas-liquid and all change into honeysuckle liquid, normal-temperature water outside tubulation is replaced as hot water, water temperature is increased to the circulating hot water of 70-80 ℃ and is delivered to again and boiled steaming pot and make solvent hot water by hot-water line, so cycling and use, and the honeysuckle of extracting collection liquid comprises chlorogenic acid and honeysuckle wet goods effective ingredient.
Above-described embodiment is used for illustrating the present invention, is not limitation of the invention.
Claims (2)
1. honeysuckle is boiled a steaming extraction element, it is characterized in that: the hermetically sealed steaming pot 1 of boiling is provided with feed inlet and outlet 2, steam inlet 3, boils steaming pot 1 top access solvent hot-water line 4, and is furnished with drain pipe 5 and sewage draining exit 6, boils and in steaming pot 1, is provided with web plate 7; Described drain pipe 5 access condensers 8, condenser 8 is provided with normal-temperature water import 9, liquid outlet 10, and condenser 8 tops are connected to hot-water line 4.
2. a kind of honeysuckle according to claim 1 is boiled steaming extracting method, it is characterized in that: concrete steps are as follows:
1) the poach stage, by dropping into and boil in steaming pot after honeysuckle screening, cleaning, is laid on web plate and compacting, shuts feed inlet and outlet; Then add water to boiling in steaming pot, making the water surface and web plate spacing is 5-10cm, opens steam and passes into and boil in steaming pot water, boils water in steaming pot in fluidized state, makes the critical condition of honeysuckle in infiltrating;
Honeysuckle raw material 30-40kg, boils steaming time 2-3 hour, boils in steaming process, the honeysuckle effective ingredient feed liquid that gaseous, liquid coexists flows out to condenser from drain pipe, flow velocity 5-8L/ minute, honeysuckle raw material is with Flos Lonicerae extractive solution yield than 1:45-50, and dirt is discharged from sewage draining exit;
3) cooling stage, the honeysuckle effective ingredient feed liquid that gas-liquid coexists by discharge nozzle to the tubulation in condenser, by the outer normal-temperature water of pipe, being cooled to 40 ℃ is all converted into below liquid and collects from liquid outlet, normal-temperature water outside tubulation is replaced as hot water, water temperature is increased to the circulating hot water of 70-80 ℃ and is delivered to again and boiled steaming pot and make solvent hot water by hot-water line, and the honeysuckle of extraction is collected liquid and comprises chlorogenic acid and honeysuckle wet goods effective ingredient.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310619624.7A CN103638690A (en) | 2013-11-29 | 2013-11-29 | Boiling and extracting device and method for honeysuckle |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310619624.7A CN103638690A (en) | 2013-11-29 | 2013-11-29 | Boiling and extracting device and method for honeysuckle |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104288204A (en) * | 2014-05-27 | 2015-01-21 | 河南科技大学 | Method for extracting chlorogenic acid from honeysuckle flower |
| CN107950845A (en) * | 2017-11-16 | 2018-04-24 | 湖北瀚思生物科技有限公司 | Honeysuckle functional beverage and its production method |
| CN108066382A (en) * | 2017-11-10 | 2018-05-25 | 湖北瀚思生物科技有限公司 | A kind of gold and silver alantol functional beverage and its production method |
| CN108543327A (en) * | 2018-03-29 | 2018-09-18 | 江西中医药大学 | A kind of volatile oil intelligent extraction collects separation equipment and technique |
| CN110157544A (en) * | 2019-05-20 | 2019-08-23 | 山东省分析测试中心 | A kind of total preparation facilities and method of the distilled liquid of honeysuckle and water extract of flos lonicerae |
| CN111054093A (en) * | 2019-12-25 | 2020-04-24 | 哈尔滨学院 | Three-way ultrasonic steam reaction generating device and chlorogenic acid extraction method |
| CN116889584A (en) * | 2023-08-28 | 2023-10-17 | 真奥金银花药业有限公司 | Continuous extraction process of honeysuckle |
| CN117303402A (en) * | 2023-11-30 | 2023-12-29 | 山东飞源东泰高分子材料有限公司 | Ammonium bifluoride refining purification device |
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| WO2002072743A1 (en) * | 2001-03-13 | 2002-09-19 | Council Of Scientific And Industrial Research | A simple portable mini distillation apparatus for the production of essential oils and hydrosols |
| CN201415068Y (en) * | 2009-06-16 | 2010-03-03 | 江苏七〇七天然制药有限公司 | Device for extracting and concentrating effective ingredient of traditional Chinese medicine |
| CN202671521U (en) * | 2012-06-30 | 2013-01-16 | 安徽皖峰蜂业集团有限公司 | Honeysuckle distillation extraction device |
| CN203620285U (en) * | 2013-11-29 | 2014-06-04 | 湖北瀚思生物科技有限公司 | Honeysuckle flower decoction extraction device |
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2013
- 2013-11-29 CN CN201310619624.7A patent/CN103638690A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2002072743A1 (en) * | 2001-03-13 | 2002-09-19 | Council Of Scientific And Industrial Research | A simple portable mini distillation apparatus for the production of essential oils and hydrosols |
| CN201415068Y (en) * | 2009-06-16 | 2010-03-03 | 江苏七〇七天然制药有限公司 | Device for extracting and concentrating effective ingredient of traditional Chinese medicine |
| CN202671521U (en) * | 2012-06-30 | 2013-01-16 | 安徽皖峰蜂业集团有限公司 | Honeysuckle distillation extraction device |
| CN203620285U (en) * | 2013-11-29 | 2014-06-04 | 湖北瀚思生物科技有限公司 | Honeysuckle flower decoction extraction device |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104288204A (en) * | 2014-05-27 | 2015-01-21 | 河南科技大学 | Method for extracting chlorogenic acid from honeysuckle flower |
| CN108066382A (en) * | 2017-11-10 | 2018-05-25 | 湖北瀚思生物科技有限公司 | A kind of gold and silver alantol functional beverage and its production method |
| CN107950845A (en) * | 2017-11-16 | 2018-04-24 | 湖北瀚思生物科技有限公司 | Honeysuckle functional beverage and its production method |
| CN108543327A (en) * | 2018-03-29 | 2018-09-18 | 江西中医药大学 | A kind of volatile oil intelligent extraction collects separation equipment and technique |
| CN110157544A (en) * | 2019-05-20 | 2019-08-23 | 山东省分析测试中心 | A kind of total preparation facilities and method of the distilled liquid of honeysuckle and water extract of flos lonicerae |
| CN111054093A (en) * | 2019-12-25 | 2020-04-24 | 哈尔滨学院 | Three-way ultrasonic steam reaction generating device and chlorogenic acid extraction method |
| CN116889584A (en) * | 2023-08-28 | 2023-10-17 | 真奥金银花药业有限公司 | Continuous extraction process of honeysuckle |
| CN117303402A (en) * | 2023-11-30 | 2023-12-29 | 山东飞源东泰高分子材料有限公司 | Ammonium bifluoride refining purification device |
| CN117303402B (en) * | 2023-11-30 | 2024-01-30 | 山东飞源东泰高分子材料有限公司 | Ammonium bifluoride refining purification device |
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Application publication date: 20140319 |