CN103055536A - Heat reflux extraction and concentration equipment - Google Patents
Heat reflux extraction and concentration equipment Download PDFInfo
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- CN103055536A CN103055536A CN2013100005123A CN201310000512A CN103055536A CN 103055536 A CN103055536 A CN 103055536A CN 2013100005123 A CN2013100005123 A CN 2013100005123A CN 201310000512 A CN201310000512 A CN 201310000512A CN 103055536 A CN103055536 A CN 103055536A
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- 238000000605 extraction Methods 0.000 title claims abstract description 60
- 238000010992 reflux Methods 0.000 title claims abstract description 41
- 239000002904 solvent Substances 0.000 claims abstract description 136
- 238000011084 recovery Methods 0.000 claims abstract description 24
- 238000001704 evaporation Methods 0.000 claims abstract description 16
- 238000009833 condensation Methods 0.000 claims abstract description 15
- 230000008020 evaporation Effects 0.000 claims abstract description 15
- 230000005494 condensation Effects 0.000 claims abstract 14
- 238000005259 measurement Methods 0.000 claims abstract 6
- 239000012141 concentrate Substances 0.000 claims description 5
- 239000000284 extract Substances 0.000 abstract description 12
- 238000000034 method Methods 0.000 abstract description 9
- 230000008569 process Effects 0.000 abstract description 6
- 230000007547 defect Effects 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 16
- 239000007788 liquid Substances 0.000 description 12
- 239000000463 material Substances 0.000 description 7
- 238000001514 detection method Methods 0.000 description 6
- 239000004480 active ingredient Substances 0.000 description 5
- 230000008901 benefit Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000012530 fluid Substances 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 238000005265 energy consumption Methods 0.000 description 3
- 230000036541 health Effects 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229930013930 alkaloid Natural products 0.000 description 2
- 150000003797 alkaloid derivatives Chemical class 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000110 cooling liquid Substances 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229930003935 flavonoid Natural products 0.000 description 2
- 235000017173 flavonoids Nutrition 0.000 description 2
- 150000002215 flavonoids Chemical class 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 235000008216 herbs Nutrition 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 235000007586 terpenes Nutrition 0.000 description 2
- 150000003505 terpenes Chemical class 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000010692 aromatic oil Substances 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 150000004053 quinones Chemical class 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
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- Extraction Or Liquid Replacement (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
本发明公布了一种热回流提取浓缩设备，包括提取罐、浓缩罐、蒸发冷凝回收溶剂贮罐、溶剂浓度在线测定装置、溶剂储罐和冷凝装置组成，所述的蒸发冷凝回收溶剂贮罐位于提取罐与冷凝装置之间，蒸发冷凝后回流的溶剂先收集于蒸发冷凝回收溶剂贮罐中，通过溶剂浓度在线测定装置和溶剂储罐调配溶剂浓度，使符合浓度要求的溶剂才排放至提取罐内提取。本发明保证提取过程中溶剂浓度稳定，提高了提取过程中工艺稳定性，克服了现有热回流提取浓缩设备由于蒸发回收的溶剂浓度不稳定而直接排放至提取罐中引起提取工艺不稳定的缺陷。
The invention discloses a heat reflux extraction and concentration equipment, which comprises an extraction tank, a concentration tank, a solvent storage tank for evaporation and condensation recovery, an online solvent concentration measurement device, a solvent storage tank and a condensation device. The evaporation and condensation recovery solvent storage tank is located at Between the extraction tank and the condensing device, the solvent returned after evaporation and condensation is first collected in the evaporation and condensation recovery solvent storage tank, and the solvent concentration is adjusted through the solvent concentration online measurement device and the solvent storage tank, so that the solvent that meets the concentration requirements is discharged to the extraction tank Extract within. The invention ensures the stability of the solvent concentration in the extraction process, improves the process stability in the extraction process, and overcomes the defect that the existing heat reflux extraction and concentration equipment is unstable in the extraction process due to the unstable concentration of the solvent recovered by evaporation and is directly discharged into the extraction tank .
Description
Technical field
The present invention relates to a kind of hot reflux and extract concentrator, belong to the concentrated technical field of Chinese medicine refluxing extraction.
Background technology
The contained complex chemical composition of Chinese medicine has carbohydrate, amino acid, protein, organic acid, alkaloid, flavonoids, quinones, terpene, glycoside, volatile oil, grease, wax, pigment, tannin, inorganic salts etc. usually.Every kind of Chinese medicine all contains thousands of kinds of chemical compositions, and in these compositions, some has obvious biological activity and plays the curative effect effect, often is called active ingredient, such as alkaloid, flavonoids, terpene, organic acid etc.Chinese medicine is developed to the products such as Chinese medicine, health products at first to be needed Chinese medicine is extracted.Extracting is exactly the process that the active ingredient in the Chinese medicine is dissolved out from plant tissue with suitable solvent.The technological parameters such as extracting method, extraction solvent and concentration thereof are most important to the acquisition of Effective Component of Chinese Medicine.Usually content is more little for active ingredient in the Chinese medicine, if the process parameter controls such as extracting method, extraction solvent and concentration thereof are improper, will make extracts active ingredients incomplete, even extract not out, has a strong impact on the curative effect of its product.
Existing hot reflux is extracted concentrator because the evaporation recovered solvent directly falls after rise to extractor, because the recovery solvent strength that obtains behind the evaporation-condensation is unstable, carrying out along with hot reflux circulation extraction, extraction solvent strength in the extractor can change and change Extraction technique, in fact changed the technological requirement that medicine, health products or extract are produced, do not met medicine, health products or extract the production of material GMP code requirement.
The patent that concentrator is extracted at present relevant hot reflux is mainly reflected in and saves the extraction solvent, saves extraction time, reduces aspects such as extracting concentrated energy resource consumption.
For example, disclose a kind of hot reflux in Chinese patent application number 201110026747.0 " the improved hot reflux extraction concentrators " and extract concentrator, formed by concentration tank, extractor, the pump housing and the circulation line that connects described concentration tank, extractor and the pump housing at least.Mainly be to take full advantage of the above cylindrical shell heat energy of liquid level, effectively increase evaporating surface, have the raising thickening efficiency, guarantee the concentrate quality evenly, shorten concentration time, reduce concentrated energy consumption, strengthen the froth breaking ability of concentration process, thoroughly solve the advantage such as barrel coking problem.
A kind of hot reflux extracting-concentration machine group of processing Chinese medicine is disclosed in Chinese patent application number 200810031387.1 " the hot reflux extracting-concentration machine groups ", it is characterized in that between the condenser condenses liquid outlet that has the hot reflux unit now and extractor condensate liquid refluxing opening, being connected with vacuum conversion tank, be connected with little condenser between demister outlet and the cooler cooling liquid inlet, the cooler cooling liquid outlet connects the oil water separator entrance point.After increasing vacuum conversion tank, audio inspissator vacuum-pumping is concentrated, converts the condensate liquid under the vacuum state condensate liquid of normal pressure to, is back to carry out normal pressure in the extractor and extract.Increase little condenser, will return in the extractor after the cooling of the steam in the extractor, realize extracting separately.But but not only alcohol extracting, but also water extraction, normal pressure extracts and negative pressure is concentrated carries out simultaneously, and extraction and concentration can use separately, also can use continuously, concentrates, the rate of filtration is fast, and energy conservation and consumption reduction effects is good.
A kind of multi-functional hot reflux extracting-concentration machine group is disclosed in Chinese patent application number 201210041987.2 " the multi-functional hot reflux extracting-concentration machine groups ", comprise extractor, concentration tank, alcohol recycling can and condensing unit, the gas vent at the gas vent at described extractor top and described concentration tank top respectively with described condensing unit treat the conducting of condensed gas inlet fluid, the liquid inlet fluid communication of the condensate outlet of described condensing unit and described alcohol recycling can, the medicine liquid outlet of described extractor bottom is by the liquid inlet fluid conducting at liquid conveyance conduit and described concentration tank top.Its advantage is: extract, concentrated and reclaim integrated work, can reach save time, the laborsaving and purpose of saving cost, and dna purity is high, cocnentration factor is large.
A kind of Chinese-medicinal thermal-refluxing extraction is disclosed in Chinese patent application number 200510027654.4 " Chinese-medicinal thermal-refluxing extractions ", it is characterized in that in lower the uncapping of described extractor, being provided with again the removable stainless steel filter plate with larger aperture and order number of one deck, the extractor liquid outlet is connected with the feed pump input through duplex strainer, the feed pump output divides two-way, one the tunnel is connected with heater, and another road back of pipeline head piece returns with extractor filter plate top tangent connection of tank chamber.Its purpose is smooth, stable in order to design a kind of fluid, is difficult for producing the stifled Chinese-medicinal thermal-refluxing extraction of gas.Compared with prior art, it has be difficult for to stop up, and the extraction of applicable different qualities material is concentrated, and medicinal liquid flow can effectively be controlled, the advantages such as filter screen easily fills, readily removable, easy cleaning.
Disclose a kind of reverse dual reflux in Chinese patent application number 03112719.3 " the traditional Chinese medicine extraction thickener " and extracted thickener, make extraction, concentrated, receiving cream loops simultaneously, also can carry out aromatic oil reclaims, alcohol reclaims, it is to be provided with motor-driven helical blade stirrer axle in extractor, be communicated with the bottom of liquid tube connector with extractor bottom and concentration systems, steam connection tube at extractor top and evaporimeter top is connected with another and is connected to the indirect steam condenser, coiled pipe cooler, the pipeline of oil water separator, under the extractor end socket, be provided with solidifying water aggregation shower, two cover concentration systems are arranged, draining condenser and indirect steam condenser, coiled pipe cooler, oil water separator, the both sides that antithesis is arranged at extractor namely by unidirectional concentrated addition be symmetric double to concentrated, medicine is carried the rate height, the concentrate time is short, energy consumption is low, occupied ground is few, investment is light.
A kind of Chinese-medicinal thermal-refluxing extraction group is disclosed in Chinese patent application number 200510027655.9 " the Chinese-medicinal thermal-refluxing extraction groups ", it is characterized in that the oil water separator delivery outlet is connected with a heating device input port, the heating device delivery outlet is connected with extractor.Its purpose is in order to design a kind of Chinese-medicinal thermal-refluxing extraction group that temperature stabilization, energy-saving effect are showing of extracting.Compared with prior art, it has condensate temperature and promotes and can automatically control, and extraction rate is stable, and the condenser condenses ability such as can normally bring into play at the advantage.
Disclose a kind of traditional Chinese herbs by thermal reflux in Chinese patent application number 200410058127.5 " traditional Chinese herbs by thermal reflux extracts, concentrates unit " and extracted, concentrated unit, this unit is characterized in that mainly the end of described hot reflux condenser (1) is provided with vacuum tank (14), and be connected with vavuum pump at vacuum tank, described vacuum tank is communicated with described vacuum switch (4), have the difference in height that can overcome the poor suction of vacuum between vacuum tank and the extractor between described vacuum tank and the extractor, all pipelines when vavuum pump is worked on this unit all are in connected state.Unit of the present invention is when opening vavuum pump, whole unit is under the vacuum state to be moved, after cooling off through hot reflux condenser, the indirect steam that produces turns back to extractor replenishing as solvent, the temperature of extractor is controlled at low-temperature condition, make solvent repeatedly move in medicinal material surface with infiltrate into medicinal material inside, improve solvent to friction wash-out power and the solubility of medicinal material, increase the soluble substance in the medicinal material and solvent strength is poor and extended capability, improved the rate of extract of Chinese medicine, guaranteed that the active ingredient of medicinal material is not evaporated loss.
Summary of the invention
The present invention seeks to provides a kind of hot reflux to extract concentrator for the defective that prior art exists.
The present invention adopts following technical scheme for achieving the above object:
Concentrator is extracted in hot reflux of the present invention, comprise that extractor, concentration tank, evaporative condenser reclaim solvent tanker, solvent strength on-line determination device, solvent tank and condensing unit and form, described evaporative condenser reclaims solvent tanker between extractor and condensing unit, the solvent that refluxes behind the evaporative condenser is collected in first evaporative condenser and reclaims in the solvent tanker, by solvent strength on-line determination device and solvent tank allotment solvent strength, it is concentrated by concentration tank after the extraction that the solvent that meets concentration requirement just is disposed in the extractor.
Described evaporative condenser reclaims on the solvent tanker solvent strength on-line determination device is installed.
Solvent strength on-line determination device is installed on the described solvent tank.
Described solvent strength on-line determination device reclaims solvent strength in the solvent tanker for detection of evaporative condenser, when the recovery solvent strength is lower than the solvent strength of extraction process requirement, makes the recovery solvent strength reach extraction process by solvent tank interpolation high concentration solvent and require just to be disposed in the extractor.
Described solvent strength on-line determination device reclaims solvent strength in the solvent tanker for detection of evaporative condenser, when the recovery solvent strength meets the solvent strength of extraction process requirement, directly will reclaim solvent discharge to extractor.
Described solvent strength on-line determination device reclaims solvent strength in the solvent tanker for detection of evaporative condenser, when the recovery solvent strength is higher than the solvent strength of extraction process requirement, makes the recovery solvent strength reach extraction process by solvent tank interpolation low concentration solvent and require just to be disposed in the extractor.
Hot reflux of the present invention is extracted concentrator evaporative condenser recovery solvent is carried out concentration determination, regulating the recovery solvent strength by the solvent tank system just is disposed in the extractor after meeting technological requirement, guarantee that solvent strength is stable in the leaching process, improved technology stability in the leaching process, overcome that concentrator is extracted in existing hot reflux because evaporation recovered solvent concentration is unstable and directly be disposed to and cause the unsettled defective of extraction process in the extractor.
Description of drawings
Fig. 1: structural representation of the present invention.
The specific embodiment
As shown in Figure 1, concentrator is extracted in hot reflux of the present invention, comprise that extractor 1, concentration tank 2, evaporative condenser reclaim solvent tanker 3, solvent strength on-line determination device 4, solvent tank 5 and condensing unit and form 6, described evaporative condenser reclaims solvent tanker 3 between extractor 1 and condensing unit 6, the solvent that refluxes behind the evaporative condenser is collected in first evaporative condenser and reclaims in the solvent tanker 3, by solvent strength on-line determination device 4 and solvent tank 5 allotment solvent strengths, it is concentrated by concentration tank 2 afterwards to make the solvent that meets concentration requirement just be disposed to extractor 1 interior extraction.
Described evaporative condenser reclaims on the solvent tanker 3 solvent strength on-line determination device 4 is installed.
Solvent strength on-line determination device 4 is installed on the described solvent tank 5.
Described solvent strength on-line determination device 4 reclaims solvent strength in the solvent tanker 3 for detection of evaporative condenser, when the recovery solvent strength is lower than the solvent strength of extraction process requirement, makes the recovery solvent strength reach extraction process by solvent tank 5 interpolation high concentration solvents and require just to be disposed in the extractor.
Described solvent strength on-line determination device 4 reclaims solvent strength in the solvent tanker 3 for detection of evaporative condenser, when the recovery solvent strength meets the solvent strength of extraction process requirement, directly will reclaim solvent discharge to extractor.
Described solvent strength on-line determination device 4 reclaims solvent strength in the solvent tanker 3 for detection of evaporative condenser, when the recovery solvent strength is higher than the solvent strength of extraction process requirement, makes the recovery solvent strength reach extraction process by solvent tank interpolation low concentration solvent and require just to be disposed in the extractor.
The above only is the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment the present invention is had been described in detail, for a person skilled in the art, it still can be made amendment to the technical scheme that aforementioned each embodiment puts down in writing, and perhaps part technical characterictic wherein is equal to replacement.Within the spirit and principles in the present invention all, any modification of doing, be equal to replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (6)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310000512.3A CN103055536B (en) | 2013-01-03 | 2013-01-03 | A kind of circumfluence distillation concentrator |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310000512.3A CN103055536B (en) | 2013-01-03 | 2013-01-03 | A kind of circumfluence distillation concentrator |
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| Publication Number | Publication Date |
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| CN103055536A true CN103055536A (en) | 2013-04-24 |
| CN103055536B CN103055536B (en) | 2016-08-03 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310000512.3A Expired - Fee Related CN103055536B (en) | 2013-01-03 | 2013-01-03 | A kind of circumfluence distillation concentrator |
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| Country | Link |
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| CN (1) | CN103055536B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105477900A (en) * | 2015-12-11 | 2016-04-13 | 苏州泽达兴邦医药科技有限公司 | Quality stability control method for traditional Chinese medicine hot reflux extraction concentration process |
| CN107320999A (en) * | 2017-08-02 | 2017-11-07 | 浙江森博机械科技有限公司 | A kind of Chinese Herbal Extract Can and extracting method |
| CN109320565A (en) * | 2018-11-14 | 2019-02-12 | 云南博泽林化工有限公司 | Deimpurity method is gone during a kind of medical tannic acid of extraction |
| CN109781468A (en) * | 2017-11-13 | 2019-05-21 | 恒天纤维集团有限公司 | A method of dense solvent sample detection point is evaporated by setting and accurately detects evaporation exit concentration |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1597038A (en) * | 2004-08-16 | 2005-03-23 | 邱云彪 | Traditional Chinese medicine thermal reflux extraction, concentration machine set |
| CN101306255A (en) * | 2008-05-21 | 2008-11-19 | 衡阳市金山中药设备制造有限公司 | Hot reflux extracting-concentration machine set |
| CN201415068Y (en) * | 2009-06-16 | 2010-03-03 | 江苏七〇七天然制药有限公司 | Device for extracting and concentrating effective ingredient of traditional Chinese medicine |
-
2013
- 2013-01-03 CN CN201310000512.3A patent/CN103055536B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1597038A (en) * | 2004-08-16 | 2005-03-23 | 邱云彪 | Traditional Chinese medicine thermal reflux extraction, concentration machine set |
| CN101306255A (en) * | 2008-05-21 | 2008-11-19 | 衡阳市金山中药设备制造有限公司 | Hot reflux extracting-concentration machine set |
| CN201415068Y (en) * | 2009-06-16 | 2010-03-03 | 江苏七〇七天然制药有限公司 | Device for extracting and concentrating effective ingredient of traditional Chinese medicine |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105477900A (en) * | 2015-12-11 | 2016-04-13 | 苏州泽达兴邦医药科技有限公司 | Quality stability control method for traditional Chinese medicine hot reflux extraction concentration process |
| CN107320999A (en) * | 2017-08-02 | 2017-11-07 | 浙江森博机械科技有限公司 | A kind of Chinese Herbal Extract Can and extracting method |
| CN109781468A (en) * | 2017-11-13 | 2019-05-21 | 恒天纤维集团有限公司 | A method of dense solvent sample detection point is evaporated by setting and accurately detects evaporation exit concentration |
| CN109320565A (en) * | 2018-11-14 | 2019-02-12 | 云南博泽林化工有限公司 | Deimpurity method is gone during a kind of medical tannic acid of extraction |
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| Publication number | Publication date |
|---|---|
| CN103055536B (en) | 2016-08-03 |
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