CN204251495U - A kind of quartz crucible forming mould - Google Patents

A kind of quartz crucible forming mould Download PDF

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Publication number
CN204251495U
CN204251495U CN201420705792.8U CN201420705792U CN204251495U CN 204251495 U CN204251495 U CN 204251495U CN 201420705792 U CN201420705792 U CN 201420705792U CN 204251495 U CN204251495 U CN 204251495U
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CN
China
Prior art keywords
mould
metal alloy
outer mold
quartz crucible
universal stage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420705792.8U
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Chinese (zh)
Inventor
孙占喜
李涛
陈官元
姚刚
蔺崇召
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
XUCHANG TIANGE SILICON TECHNOLOGY Co Ltd
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XUCHANG TIANGE SILICON TECHNOLOGY Co Ltd
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Application filed by XUCHANG TIANGE SILICON TECHNOLOGY Co Ltd filed Critical XUCHANG TIANGE SILICON TECHNOLOGY Co Ltd
Priority to CN201420705792.8U priority Critical patent/CN204251495U/en
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Publication of CN204251495U publication Critical patent/CN204251495U/en
Expired - Fee Related legal-status Critical Current
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Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00Other methods of shaping glass
    • C03B19/09Other methods of shaping glass by fusing powdered glass in a shaping mould
    • C03B19/095Other methods of shaping glass by fusing powdered glass in a shaping mould by centrifuging, e.g. arc discharge in rotating mould
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

The utility model discloses a kind of quartz crucible forming mould, comprise metal alloy steel die, outer mold, porous alloy base, universal stage, turning axle, motor, the skin cover of described metal alloy steel die has outer mold, porous alloy base is equipped with in the bottom of described metal alloy steel die, described porous alloy base is placed on universal stage, turning axle is provided with below described universal stage, it is high that the utility model has intensity, long service life, efficiency utilization heat energy, reduce the advantage of power consumption, the utility model improves glass melting temperature, the metallic impurity in raw material can be removed fast, solve the drawback that starting material can only rely on import quartz sand, and improve intergranular degree of combining closely by high temperature melting, decrease number of bubbles, improve quality product, shorten the production cycle, improve production efficiency, fully save the energy, reduce production cost.

Description

A kind of quartz crucible forming mould
Technical field
The utility model relates generally to the quartz crucible production equipment for drawn monocrystalline silicon, is specifically related to a kind of quartz crucible forming mould.
Background technology
Silicon single crystal is the main raw of conversion solar energy, electric energy.Crystalline silicon material (comprising polysilicon and silicon single crystal) is topmost photovoltaic material, and its share of market more than 90%, and is also still the mainstay material of solar cell in one quite long from now on period.High-purity silicon single crystal rod is the raw material of single crystal silicon solar cell, silicon purity requirement 99.999%.
Quartz crucible is the expendable vessel of drawn monocrystalline silicon, often produces a stove silicon single crystal and just to use up a quartz crucible.Quartz crucible is the crucial requisite of monocrystalline silicon production.Therefore the demand of silicon single crystal and the demand of quartz crucible are directly proportional.The whole nation needs crucible quantity 280-360 about ten thousand in silicon single crystal industry year.Current domestic yearly capacity is only 2,000,000, far can not meet the demand of domestic silicon single crystal industry.
At present, the production unit used during domestic quartz crucible manufacturing enterprise produces comes from the production unit introduced from Japan the beginning of the seventies in last century, and this technical equipment level of automation is not high, and in whole production process, more dependence manually realizes.
The core technology of producing quartz crucible is to found mould.Current mould of founding mainly adopts graphite jig and punching block mould, its ubiquitous problem mainly contain following some: 1. glass melting temperature is lower, is difficult to reject the metallic impurity in raw material; 2. need to install water jacket additional, mould resistance to elevated temperatures is poor; 3. die life is shorter, about each graphite jig can found 200 crucibles, and also can only reach about 600 with the punching block mould of pig iron casting; 4. starting material require higher, can not the lower domestic quartz sand of using character, can only the import quartz sand of Price-dependent costliness; 5. melting time is longer, and production efficiency is low; 6. energy consumption is too high, and electricity charge burden is heavier.
Along with the recovery of photovoltaic industry, based on material prepare container, quartz crucible must towards high-quality, less energy-consumption, major diameter, high crystal pulling success ratio future development, the fast development of photovoltaic industry to English crucible in major diameter, high purity, bubble is few, Impurity Distribution high uniformity, specification precision are high, the professional domains such as heat resistance is good are had higher requirement.Core technology again owing to preparing quartz crucible is to found mould, and therefore, the appearance of founding mould in the urgent need to a kind of new quartz crucible is filled a hole in the market.
Summary of the invention
The purpose of this utility model is the drawback solving prior art existence, provides the quartz crucible forming mould that a kind of intensity is high, long service life, power consumption are low, save energy, number of bubbles are few, with short production cycle, cost is low again.
For achieving the above object, the technical scheme that the utility model adopts is: a kind of quartz crucible forming mould, comprise metal alloy mould mould, outer mold, porous alloy base, universal stage, turning axle, the skin cover of described metal alloy mould has outer mold, porous alloy base is equipped with in the bottom of described metal alloy mould, described porous alloy base is placed on universal stage, is provided with turning axle below described universal stage.Wherein, a cavity is formed between described metal alloy mould and described outer mold, described universal stage is equipped with vacuum pipe, described vacuum pipe communicates with described cavity and passes the centre hole of outer mold and metal alloy mould, and described vacuum pipe accumulates a vacuum pipe in interior of rotating shaft and is connected with outside off-gas pump.
Described metal alloy mould is provided with multiple micro-pore.
Described outer mold eliminates the circulating chilled water device of original water jacket.
What described outer mold inside was filled is silica wool.
The beneficial effect that the utility model produces is: on the one hand, the utility model passes through the improvement of founding mold material, adopt tungsten Zinc alloy die, improve mould strength, mould can not be burst in high temperature melting process, reduce consumption and the thermal treatment energy consumption of mould, decrease energy dissipation, extend die life.On the other hand, the utility model is by the improvement of mold sandwich, solve the water jacket that traditional moulds outside need be provided as mould cooling, circulation cycle water in water jacket, circulating water pool and water circulating pump must be had, and to the cooling demoulding be carried out when product has founded the demoulding, this Mould operation is complicated, production cost is high, the consumption of moulding stock and the high problem of thermal treatment energy consumption.The utility model adopts insulation silica wool, and solving mold exterior need provide water jacket to lower the temperature, and causes the waste of thermal treatment energy consumption, the drawback that production cost is high, after improving, efficiently solve calorific loss, improves heat utilization rate.The utility model improves the vacuum tightness of mold system, reduces the striking voltage of electrode bar simultaneously.The lifting of pressure can make the combination between quartz sand particle more tight, greatly reduces the space reduced between particle and particle like this, thus reduces the probability that bubble occurs to a great extent, improve the drawing crystal forming rate of drawn monocrystalline silicon.In addition, the utility model also improves glass melting temperature, can to remove on the one hand in domestic quartz sand raw material the metallic impurity such as lithium, aluminium, potassium, sodium fast, and solving raw material can only the drawback of dependence on import quartz sand, significantly reduces production cost.On the other hand, after in mould, temperature improves, the liquefied that product quartz crucible inner surface presents is more thorough, reduce the viscosity of liquid quartz, the bubble of liquid quartz inside, crucible internal skin is discharged fast, reach and remove bubble fast, the outer quartz sand particle of quartz crucible is combined closely, improve the intensity of product quartz crucible, improve quality product simultaneously, shorten the production cycle, save melting time, single finished product melting time is made to reduce to 9 minutes, improve production efficiency, utilization rate of raw materials brings up to more than 85%, reduce production cost, really reach energy-saving and cost-reducing object.
Accompanying drawing explanation
Fig. 1 is longitudinal profile schematic diagram of the present utility model.
Fig. 2 is stravismus schematic diagram of the present utility model.
Fig. 3 is schematic top plan view of the present utility model.
In figure: 1 is metal alloy mould, 2 is outer mold, and 3 is porous alloy base, and 4 is universal stage, and 5 is turning axle.
Embodiment
Below in conjunction with accompanying drawing, the utility model is described further.
Embodiment 1
As shown in Figure 1, Figure 2 and Figure 3, a kind of quartz crucible forming mould, comprise metal alloy mould 1, outer mold 2, porous alloy base 3, universal stage 4, turning axle 5, the skin cover of described metal alloy inner mold 1 has outer mold 2, porous alloy base 3 is equipped with in the bottom of described metal alloy mould 1, described porous alloy base puts 3 on universal stage 4, and described universal stage 4 is provided with turning axle 5 below.Wherein, a cavity is formed between described metal alloy mould 1 and described outer mold 2, described universal stage is equipped with vacuum pipe, described vacuum pipe communicates with described cavity and passes the centre hole of outer mold 2 and metal alloy mould 1, and described vacuum pipe accumulates a vacuum pipe and is connected with outside off-gas pump in the inside of turning axle 5.
What inner mold of the present utility model adopted is tungsten, molybdenum, Zinc alloy die, improves mould strength, mould can not be burst in high temperature melting process, reduce consumption and the thermal treatment energy consumption of mould, decrease energy dissipation, extend die life.The utility model improves the vacuum tightness of mold system, reduces the striking voltage of electrode bar simultaneously.The lifting of pressure can make the combination between quartz sand particle more tight, greatly reduces the space reduced between particle and particle like this, thus reduces the probability that bubble occurs to a great extent, improve the drawing crystal forming rate of drawn monocrystalline silicon.In addition, the utility model also improves glass melting temperature, to remove on the one hand fast in domestic quartz sand raw material the metallic impurity such as lithium, aluminium, potassium, sodium, and solving raw material can only the drawback of dependence on import quartz sand, significantly reduces production cost.On the other hand, after in mould, temperature improves, the liquefied that product quartz crucible inner surface presents is more thorough, reduce the viscosity of liquid quartz, the bubble of liquid quartz inside, crucible internal skin is discharged fast, reach and remove bubble fast, the outer quartz sand particle of quartz crucible is combined closely, improve the intensity of product quartz crucible, improve quality product simultaneously, shorten the production cycle, save melting time, single finished product melting time is made to reduce to 9 minutes, improve production efficiency, utilization rate of raw materials brings up to more than 85%, reduce production cost, really reach energy-saving and cost-reducing object.
To sum up, the utility model has the advantage that intensity is high, long service life, power consumption are low, save energy, number of bubbles are few, with short production cycle, production cost is low.
Embodiment 2
As shown in Figure 1, Figure 2 and Figure 3, a kind of quartz crucible forming mould, comprise metal alloy mould 1, outer mold 2, porous alloy base 3, universal stage 4, turning axle 5, the skin cover of described metal alloy inner mold 1 has outer mold 2, porous alloy base 3 is equipped with in the bottom of described metal alloy mould 1, described porous alloy base puts 3 on universal stage 4, and described universal stage 4 is provided with turning axle 5 below.Wherein, a cavity is formed between described metal alloy mould 1 and described outer mold 2, described universal stage is equipped with vacuum pipe, described vacuum pipe communicates with described cavity and passes the centre hole of outer mold 2 and metal alloy mould 1, and described vacuum pipe accumulates a vacuum pipe and is connected with outside off-gas pump in the inside of turning axle 5.
Described metal alloy mould is provided with multiple micro-pore.
Described outer mold eliminates the circulating chilled water device of original water jacket.
What described outer mold inside was filled is silica wool.
What inner mold of the present utility model adopted is tungsten, molybdenum, Zinc alloy die, improves mould strength, mould can not be burst in high temperature melting process, reduce consumption and the thermal treatment energy consumption of mould, decrease energy dissipation, extend die life.Outer mold of the present utility model eliminates the circulating chilled water device of original water jacket, inner filling is incubated silica wool, solving mold exterior need provide water jacket to lower the temperature, cause the waste of thermal treatment energy consumption, the drawback that production cost is high, after improving, efficiently solve calorific loss, improve heat utilization rate.The utility model improves the vacuum tightness of mold system, reduces the striking voltage of electrode bar simultaneously.The lifting of pressure can make the combination between quartz sand particle more tight, greatly reduces the space reduced between particle and particle like this, thus reduces the probability that bubble occurs to a great extent, improve the drawing crystal forming rate of drawn monocrystalline silicon.In addition, the utility model also improves glass melting temperature, to remove on the one hand fast in domestic quartz sand raw material the metallic impurity such as lithium, aluminium, potassium, sodium, and solving raw material can only the drawback of dependence on import quartz sand, significantly reduces production cost.On the other hand, after in mould, temperature improves, the liquefied that product quartz crucible inner surface presents is more thorough, reduce the viscosity of liquid quartz, the bubble of liquid quartz inside, crucible internal skin is discharged fast, reach and remove bubble fast, the outer quartz sand particle of quartz crucible is combined closely, improve the intensity of product quartz crucible, improve quality product simultaneously, shorten the production cycle, save melting time, single finished product melting time is made to reduce to 9 minutes, improve production efficiency, utilization rate of raw materials brings up to more than 85%, reduce production cost, really reach energy-saving and cost-reducing object.
To sum up, the utility model has the advantage that intensity is high, long service life, power consumption are low, save energy, number of bubbles are few, with short production cycle, production cost is low.

Claims (4)

1. a quartz crucible forming mould, it is characterized in that: comprise metal alloy mould mould, outer mold, porous alloy base, universal stage, turning axle, the skin cover of described metal alloy mould has outer mold, porous alloy base is equipped with in the bottom of described metal alloy mould, described porous alloy base is placed on universal stage, turning axle is provided with below described universal stage, wherein, a cavity is formed between described metal alloy mould and described outer mold, described universal stage is equipped with vacuum pipe, described vacuum pipe communicates with described cavity and passes the centre hole of outer mold and metal alloy mould, described vacuum pipe accumulates a vacuum pipe in interior of rotating shaft and is connected with outside off-gas pump.
2. a kind of quartz crucible forming mould according to claim 1, is characterized in that: described metal alloy mould is provided with multiple micro-pore.
3. a kind of quartz crucible forming mould according to claim 1, is characterized in that: described outer mold eliminates the circulating chilled water device of original water jacket.
4. a kind of quartz crucible forming mould according to claim 3, is characterized in that: what described outer mold inside was filled is silica wool.
CN201420705792.8U 2014-11-24 2014-11-24 A kind of quartz crucible forming mould Expired - Fee Related CN204251495U (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Publications (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104402204A (en) * 2014-11-24 2015-03-11 许昌天戈硅业科技有限公司 Quartz crucible forming mould

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104402204A (en) * 2014-11-24 2015-03-11 许昌天戈硅业科技有限公司 Quartz crucible forming mould

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150408

Termination date: 20171124

CF01 Termination of patent right due to non-payment of annual fee